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AS 1038.10.1-2003

Withdrawn
Withdrawn

A Withdrawn Standard is one, which is removed from sale, and its unique number can no longer be used. The Standard can be withdrawn and not replaced, or it can be withdrawn and replaced by a Standard with a different number.

Coal and coke - Analysis and testing Determination of trace elements - Coal, coke and fly-ash - Determination of eleven trace elements - Flame atomic absorption spectrometric method (Reconfirmed 2013)
Available format(s)

Hardcopy , PDF 1 User , PDF 3 Users , PDF 5 Users , PDF 9 Users

Withdrawn date

10-11-2023

Language(s)

English

Published date

05-03-2003

Publisher

Standards Australia

Preview

This Standard has been reconfirmed. To view or download the Reconfirmation Notice please click here.

1 - AS 1038.10.1-2003 COAL AND COKE-ANALYSIS AND TESTING - DETERMINATION OF TRACE ELEMENTS-COAL, COKE AND FLY-ASH-...
4 - PREFACE
5 - CONTENTS
6 - 1 SCOPE
6 - 2 REFERENCED DOCUMENTS
6 - 3 DEFINITIONS
7 - 4 PRINCIPLE
7 - 5 SAFETY
7 - 6 REAGENTS
7 - 6.1 General
7 - 6.2 Solutions
7 - 6.2.1 Nitric acid
7 - 6.2.2 Nitric acid
7 - 6.2.3 Nitric acid
7 - 6.2.4 Hydrochloric acid
7 - 6.2.5 Aqua regia solution
7 - 6.2.6 Hydrofluoric acid
7 - 6.2.7 Boric acid solution
8 - 6.2.8 Sodium buffer solution
8 - 6.2.9 Hydrogen peroxide
8 - 6.3 Standard solutions
8 - 6.3.1 Standard barium solution
8 - 6.3.2 Standard beryllium solution
8 - 6.3.3 Standard chromium solution
8 - 6.3.4 Standard copper solution
8 - 6.3.5 Standard lithium solution
8 - 6.3.6 Standard manganese solution
8 - 6.3.7 Standard nickel solution
8 - 6.3.8 Standard lead solution
8 - 6.3.9 Standard strontium solution
8 - 6.3.10 Standard vanadium solution
9 - 6.3.11 Standard zinc solution
9 - 6.3.12 Unbuffered blank calibration solution (Solution 1U)
9 - 6.3.13 Buffered blank calibration solution (Solution 1B)
9 - 6.3.14 Unbuffered composite calibration solution (Solution 6U)
9 - 6.3.15 Buffered composite calibration solution (Solution 6B)
9 - 6.3.16 Unbuffered calibration solutions
9 - 6.3.17 Buffered calibration solutions.
11 - 6.3.18 Synthetic coal ash solutions
12 - 7 APPARATUS
12 - 7.1 Atomic absorption/emission spectrometer
12 - 7.2 Muffle furnace
12 - 7.3 Bottles for ash dissolution and storage of AAS measurement solutions
12 - 7.4 Plastics volumetric flasks
12 - 7.5 Plastics burettes
12 - 7.6 Polyethylene dispensing bottles
12 - 7.7 Plastics bottles
12 - 7.8 Plastics measuring cylinder
12 - 7.9 Water bath
12 - 7.10 Weighing devices
13 - 7.11 Ashing dishes
13 - 7.12 Aluminium boat or heavy duty aluminium foil
13 - 8 SAMPLE
13 - 8.1 General
13 - 8.2 Preparation of ash
13 - 8.2.1 Equilibration of sample
13 - 8.2.2 Mass of test portion
14 - 8.2.3 Ashing procedure
15 - 9 PROCEDURE
15 - 9.1 Duplicate determinations
15 - 9.2 Blank tests
15 - 9.3 Check test
15 - 9.4 Dissolution of test portion
15 - 9.5 Measurement
15 - 9.5.1 General
16 - 9.5.2 Background correction
16 - 9.5.3 Minimization of interference
17 - 9.5.4 Samples with element contents outside the range
17 - 10 CALCULATION
18 - 11 REPORTING OF RESULTS
18 - 12 ACCEPTANCE OF RESULTS
18 - 13 PRECISION
19 - 14 TEST REPORT
20 - APPENDIX A - PRECISION DATA FOR DETERMINATION OF ELEVEN TRACEELEMENTS IN COAL, COKE AND FLY-ASH

This Standard sets out a method for the preparation of the ash and a flame atomic absorption spectrometric method for the determination of barium, beryllium, chromium, copper, lead, lithium, manganese, nickel, strontium, vanadium and zinc in ash prepared in the laboratory from higher rank coal, coke and fly-ash. The Standard also provides an optional flame atomic emission spectrometric method for the determination of barium, as it gives improved sensitivity over flame atomic absorption spectrometry and it is not possible to determine barium by the latter technique with some instruments.

This Standard sets out a method for the preparation of the ash and a flame atomic absorption spectrometric method for the determination of barium, beryllium, chromium, copper, lead, lithium, manganese, nickel, strontium, vanadium and zinc in ash prepared in the laboratory from higher rank coal, coke and fly-ash. The Standard also provides an optional flame atomic emission spectrometric method for the determination of barium, as it gives improved sensitivity over flame atomic absorption spectrometry and it is not possible to determine barium by the latter technique with some instruments. NOTE: Two approaches, gravimetric and volumetric, have been specified for solution preparation, both give the same results provided that, in the volumetric approach, plastics volumetric ware is used.

Committee
MN-001
DocumentType
Standard
ISBN
0 7337 5092 3
Pages
19
ProductNote
Reconfirmed 06-08-2013
PublisherName
Standards Australia
Status
Withdrawn
Supersedes

First published as AS 1038.10.1-1986.Second edition 2003.Reconfirmed 2013. Originated as AS 1038.10.1-1986. Second edition 2003.

AS/NZS 2243.5:2004 Safety in laboratories Non-ionizing radiations - Electromagnetic, sound and ultrasound
AS 2243.9-1991 Safety in laboratories - Recirculating fume cabinets
AS 2508.3.009-1982 Safe storage and handling information card - Hydrocarbon solvents
AS 2508.8.009-1990 Safe storage and handling information card - Sulfuric acid (Oleum)
AS 1038.4-2006 Coal and coke - Analysis and testing Coke - Proximate analysis
AS 2508.3.013-1984 Safe storage and handling information card - Methyl ethyl ketone (MEK)
AS 2508.6.002-1985 Safe storage and handling information card - Cyanides (sodium and potassium)
AS 2508.3.005-1982 Safe storage and handling information cards for hazardous materials - Benzene (benzol)
AS 2508.3.027-1983 Safe storage and handling information card - Diacetone alcohol
AS 2508.3.033-1984 Safe storage and handling information card - Isoprene, inhibited
AS 2508.6.004-1984 Safe storage and handling information card - Cadmium compounds (other than selenide and sulphide)
AS 2508.2.007-2001 Safe storage and handling information card - Liquefied petroleum gas
AS 2508.8.005-1992 Safe storage and handling information card - Acetic acid (containing more than 10 percent but not more than 80 percent acid, by mass, in water)
AS 2508.2.006-1995 Safe storage and handling information card - Ethylene oxide
AS 2243.10-1993 Safety in laboratories - Storage of chemicals
AS 2508.6.011-1988 Safe storage and handling information card - Tetrachloroethylene (Perchloroethylene, Per or Perc)
AS 1038.16-2005 Coal and coke - Analysis and testing Assessment and reporting of results (Reconfirmed 2016)
AS 2508.6.019-1995 Safe storage and handling information card - Lead alkyls
AS/NZS 2243.3:2002 Safety in laboratories Microbiological aspects and containment facilities
AS 2508.3.007-1995 Safe storage and handling information card - Carbon disulphide
AS 2508.6.020-1991 Safe storage and handling information card - Selenious acid, selenates and selenites
AS/NZS 2243.8:2006 Safety in laboratories - Fume cupboards
AS 2508.3.032-1984 Safe storage and handling information card - Glycol ether acetates
AS 2508.6.009-1990 Safe storage and handling information card - 1,1,1-trichloroethane (Methylchloroform)
AS 1038.4-1995 Coal and coke - Analysis and testing Coke - Proximate analysis
AS 2508.8.017-1988 Safe storage and handling information card - Aluminium chloride (Anhydrous)
AS 2508.3.016-1982 Safe storage and handling information card - Methyl isobutyl ketone (MIBK)
AS 2508.6.022-1986 Safe storage and handling information card - Copper-chrome-arsenic
AS 2508.3.029-1983 Safe storage and handling information card - Glycol ethers (flammable)
AS 2508.3.030-1983 Safe storage and handling information card - Cyclohexane
AS 2508.6.024-1984 Safe storage and handling information card - Pentachlorophenol
AS 2508.6.003-1984 Safe storage and handling information card - Aniline (aminobenzene)
AS 2508.6.006-1982 Safe storage and handling information card - Beryllium and compounds
AS 4264.2-1996 Coal and coke - Sampling Coke - Sampling procedures (Reconfirmed 2013)
AS 2418-1995 Coal and coke - Glossary of terms (Reconfirmed 2013) (Reconfirmed 2023)
AS 2508.6.012-1988 Safe storage and handling information card - Diphenyl methane-4, 4-Diisocyanate [Methylene bis-(Phenylene) Diisocyanate] (MDI)
AS 2508.3.021-1983 Safe storage and handling information card - Cyclohexanone
AS 2508.6.010-1983 Safe storage and handling information card - Toluene diisocyanate (TDI)
AS/NZS 2243.9:2003 Safety in laboratories - Recirculating fume cabinets
AS 2508.5.002-1990 Safe storage and handling information card - Ammonium nitrate
AS 2243.3-1991 Safety in laboratories - Microbiology
AS 2508.6.001-1988 Safe storage and handling information card - Carbon tetrachloride (tetrachloromethane)
AS 2508.2.010-1984 Safe storage and handling information card - Sulphur dioxide (liquefied)
AS 2508.8.010-1990 Safe storage and handling information cards for hazardous materials - Sulfuric acid (up to 98% m/m)
AS 2508.3.017-1983 Safe storage and handling information card - Ethanol/methylated spirits
AS 2508.5.001-1989 Safe storage and handling information card - Hydrogen peroxide
AS 2508.6.018-1989 Safe storage and handling information card - Lead arsenate and Lead aresenite
AS 2508.2.001-1992 Safe storage and handling information card - Acetylene (Dissolved) (Ethyne)
AS 2508.3.008-1983 Safe storage and handling information cards for hazardous materials - Acrylonitrile (inhibited)
AS 2508.8.018-1995 Safe storage and handling information card - Formaldehyde solutions (with not less than 25 percent formaldehyde)
AS 2508.8.013-1991 Safe storage and handling information card - Hydrofluoric acid (aqueous)
AS 2508.3.026-1995 Safe storage and handling information card - Propylene oxide
AS 2508.8.007-1990 Safe storage and handling information card - Nitric acid
AS 2508.5.003-1990 Safe storage and handling information card - Calcium hypochlorite
AS 2508.6.015-1983 Safe storage and handling information card - Methylene chloride (Dichloromethane)
AS 1038.3-2000 Coal and coke - Analysis and testing - Proximate analysis of higher rank coal
AS 2134.1-1999 Recommended practice for chemical analysis by atomic absorption spectrometry Flame atomic absorption spectrometry (Reconfirmed 2016)
AS 2243.1-1990 Safety in laboratories - General
AS 2508.5.005-1992 Safe storage and handling information card - Methyl ethyl ketone peroxide (MEKP) (not more than 50% in solution with not more than 10% available oxygen)
AS 2508.10.001-2000 Safe storage and handling information card - Agricultural and veterinary chemicals (Packaged products only)
AS 2508.3.015-1992 Safe storage and handling information card - Toluene (toluol)
AS 2508.3.012-1982 Safe storage and handling information card - Styrene (vinyl benzene, styrene monomer)
AS 2508.3.010-1995 Safe storage and handling information card - Amines (isopropylamine, diethylamine, triethylamine)
AS 2508.2.005-1984 Safe storage and handling information card - Chlorine (compressed)
AS 2508.8.008-1992 Safe storage and handling information card - Maleic anhydride
AS 2243.8-1992 Safety in laboratories - Fume cupboards
AS 2508.6.013-1991 Safe storage and handling information card - Trichloroethylene
AS 2508.8.002-1986 Safe storage and handling information card - Hydrochloric acid (muriatic acid, spirits of salts)
AS 2508.8.004-1992 Safe storage and handling information card - Acetic acid (containing more than 80 percent acid, by mass, in water)
AS 2508.2.011-1984 Safe storage and handling information card - Butadiene (inhibited)
AS 2508.3.024-1995 Safe storage and handling information card - Dimethylamine solution
AS 2850-1986 Chemical analysis - Interlaboratory test programs - For determining precision of analytical method(s) - Guide to the planning and conduct
AS 2508.3.031-1983 Safe storage and handling information card - Tetrahydrofuran (THF)
AS 2508.3.002-1982 Safe storage and handling information card - Acetates (ethyl acetate, propyl acetates, butyl acetates, amyl acetate)
AS 2243.2-1990 Safety in laboratories - Chemical aspects
AS 2508.3.004-1982 Safe storage and handling information card - Acrylates (methyl, ethyl)
AS 2508.8.003-1990 Safe storage and handling information card - Sodium hypochlorite Hypochlorite solutions
AS 2508.6.008-1989 Safe storage and handling information card - Ammonium thioglycolate
AS 2508.8.015-1988 Safe storage and handling information card - Dilute ammonia solution containing 10 percent up to 35 percent m/m ammonia
AS 2508.6.005-1984 Safe storage and handling information card - Fluorides (ammonium, potassium, magnesium or sodium fluoride)
AS 2508.3.034-1984 Safe storage and handling information card - Pentanes
AS 2508.2.013-1992 Safe storage and handling information card - Ethylene (ethene)
AS 2508.3.011-1992 Safe storage and handling information card - Methanol (methyl alcohol)
AS 2508.8.016-1988 Safe storage and handling information card - Phosphoric acid (Orthophosphoric acid)
AS 2508.2.004-1995 Safe storage and handling information card - Ammonia (anhydrous)
AS 2508.2.002-1992 Safe storage and handling information card - Hydrogen (compressed)
AS 2508.6.014-1989 Safe storage and handling information card - Cyanides, inorganic (other than Sodium and Potassium Cyanides for which refer to AS 2508.6.002)
AS 2508.3.001-1982 Safe storage and handling information card - Acetone
AS 2508.3.028-1983 Safe storage and handling information card - Ethylene dichloride (1,2-dichloroethane, ethylene chloride (EDC))
AS 2508.8.001-1995 Safe storage and handling information card - Acetic anhydride
AS 2508.6.023-1989 Safe storage and handling information card - Phenylmercuric compounds
AS 2508.6.026-1984 Safe storage and handling information card - Formaldehyde solutions - Flashpoint above 61 degrees Celsius
AS/NZS 2243.2:2006 Safety in laboratories Chemical aspects
AS 2243.7-1991 Safety in laboratories - Electrical aspects
AS 2508.2.003-1995 Safe storage and handling information card - Vinyl chloride (inhibited)
AS 2508.8.011-1995 Safe storage and handling information card - Methacrylic acid (inhibited)
AS 2508.3.020-1983 Safe storage and handling information card - Ethyl benzene
AS 2508.3.023-1983 Safe storage and handling information card - Vinyl acetate (vinyl acetate monomer)
AS 2508.3.022-1983 Safe storage and handling information card - Cumene (isopropyl-benzene)
AS 2508.6.028-1988 Safe storage and handling information card - Chloropicrin
AS 2508.8.012-1991 Safe storage and handling information card - Hydrogen fluoride (Anhydrous)(Anhydrous hydrofluoric acid)
AS 2508.6.016-1995 Safe storage and handling information card - Phenol (carbolic acid), cresols and cresylic acid
AS 2508.4.001-1982 Safe storage and handling information card - Calcium carbide
AS 2508.3.003-1982 Safe storage and handling information card - Acrylates (butyl, isobutyl)
AS 2508.3.005-1995 Safe storage and handling information card - Benzene
AS 2508.6.021-1984 Safe storage and handling information card - Sodium pentachlorophenate
AS 2508.3.006-1995 Safe storage and handling information card - Butanols, propanols, amyl alcohols
AS 2508.6.025-1984 Safe storage and handling information card - Arsenic acid
AS 2508.6.007-1995 Safe storage and handling information card - Epichlorohydrin (Ech or 1-Chloro-2,3-epoxypropane)
AS/NZS 2243.10:2004 Safety in laboratories Storage of chemicals
AS/NZS 2243.1:2005 Safety in laboratories Planning and operational aspects
AS 2508.6.027-1984 Safe storage and handling information card - Tributyltin-oxide
AS 2508.3.014-1992 Safe storage and handling information card - Xylenes (xylols)
AS 2508.2.009-1984 Safe storage and handling information card - Oxygen (refrigerated liquid)
AS 2243.4-1998 Safety in laboratories - Ionizing radiations
AS 2508.3.025-1983 Safe storage and handling information cards for hazardous materials - Chlorobenzene (monochlorobenzene)
AS 2508.2.012-1985 Safe storage and handling information card - Non-flammable, inert, compressed gases (includes: argon, helium, krypton, neon, nitrogen and xenon)
AS 2508.3.018-1983 Safe storage and handling information card - Methyl isobutyl carbinol
AS 2243.6-1990 Safety in laboratories - Mechanical aspects
AS 2508.2.008-1984 Safe storage and handling information card - Oxygen (compressed)
AS 2508.8.006-1992 Safe storage and handling information card - Sodium hydroxide (solid and solution) (caustic soda)
AS 2508.5.004-1991 Safe storage and handling information card - Benzoyl peroxide
AS 2508.8.014-1985 Safe storage and handling information card - Mercury metal
AS 1038.16-1996 Coal and coke - Analysis and testing - Assessment and reporting of results
AS 2508.6.017-1989 Safe storage and handling information card - Lead acetate
AS 2508.3.019-1983 Safe storage and handling information card - Methacrylates, HFP
AS 2243.5-1993 Safety in laboratories - Non-ionizing radiations
AS 4264.1-1995 Coal and coke - Sampling Higher rank coal - Sampling procedures

AS 1038.16-2005 Coal and coke - Analysis and testing Assessment and reporting of results (Reconfirmed 2016)
AS 2519-1993 Guide to the technical evaluation of higher rank coal deposits (Reconfirmed 2013) (Reconfirmed 2023)
AS 2418-1995 Coal and coke - Glossary of terms (Reconfirmed 2013) (Reconfirmed 2023)

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