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ASTM C 1347 : 2002

Superseded

Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

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superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

Standard Practice for Preparation and Dissolution of Uranium Materials for Analysis

Available format(s)

Hardcopy , PDF

Superseded date

11-11-2014

Language(s)

English

Published date

10-08-2002

1.1 This practice covers dissolution treatments for uranium materials that are applicable to the test methods used for characterizing these materials for uranium elemental, isotopic, and impurities determinations. Dissolution treatments for the major uranium materials assayed for uranium or analyzed for other components are listed.

1.2 The treatments, in order of presentation, are as follows:

Procedure TitleSection
Dissolution of Uranium Metal and Oxide with Nitric Acid8.1
Dissolution of Uranium Oxides with Nitric Acid and Residue Treatment8.2
Dissolution of Uranium-Aluminum Alloys in Hydrochloric Acid with Residue Treatment8.3
Dissolution of Uranium Scrap and Ash by Leaching with Nitric Acid and Treatment of Residue by Carbonate Fusion8.4
Dissolution of Refractory Uranium-Containing Material by Carbonate Fusion8.5
Dissolution of Uranium-Aluminum Alloys Uranium Scrap and Ash, and RefractoryUranium-Containing Materials by Microwave Treatment8.6

1.3 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.

1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific hazards statements are given in Section 7.

Committee
C 26
DocumentType
Standard Practice
Pages
8
PublisherName
American Society for Testing and Materials
Status
Superseded
SupersededBy

ASTM C 1647 : 2013 Standard Practice for Removal of Uranium or Plutonium, or both, for Impurity Assay in Uranium or Plutonium Materials
ASTM C 1845 : 2016 Standard Practice for The Separation of Lanthanide Elements from Uranium Matrices Using High Pressure Ion Chromatography (HPIC) for Isotopic Analyses by Inductively Coupled Plasma Mass Spectrometry (ICP-MS)
ASTM C 1413 : 2018 Standard Test Method for Isotopic Analysis of Hydrolyzed Uranium Hexafluoride and Uranyl Nitrate Solutions by Thermal Ionization Mass Spectrometry
ASTM C 1462 : 2000 : R2013 Standard Specification for Uranium Metal Enriched to More than 15 % and Less Than 20 % 235U
ASTM C 1474 : 2019 Standard Test Method for Analysis of Isotopic Composition of Uranium in Nuclear-Grade Fuel Material by Quadrupole Inductively Coupled Plasma-Mass Spectrometry
ASTM C 1672 : 2017 Standard Test Method for Determination of Uranium or Plutonium Isotopic Composition or Concentration by the Total Evaporation Method Using a Thermal Ionization Mass Spectrometer
ASTM C 1816 : 2016 Standard Practice for The Ion Exchange Separation of Small Volume Samples Containing Uranium, Americium, and Plutonium Prior to Isotopic Abundance and Content Analysis
ASTM C 968 : 2012 Standard Test Methods for Analysis of Sintered Gadolinium Oxide-Uranium Dioxide Pellets
ASTM C 1128 : 2018 Standard Guide for Preparation of Working Reference Materials for Use in Analysis of Nuclear Fuel Cycle Materials
ASTM C 1287 : 2018 Standard Test Method for Determination of Impurities in Nuclear Grade Uranium Compounds by Inductively Coupled Plasma Mass Spectrometry
ASTM D 7876 : 2013 : R2018 Standard Practice for Practice for Sample Decomposition Using Microwave Heating (With or Without Prior Ashing) for Atomic Spectroscopic Elemental Determination in Petroleum Products and Lubricants
ASTM C 1267 : 2017 Standard Test Method for Uranium by Iron (II) Reduction in Phosphoric Acid Followed by Chromium (VI) Titration in the Presence of Vanadium
ASTM C 1517 : 2016 Standard Test Method for Determination of Metallic Impurities in Uranium Metal or Compounds by DC-Arc Emission Spectroscopy
ASTM C 1625 : 2012 Standard Test Method for Uranium and Plutonium Concentrations and Isotopic Abundances by Thermal Ionization Mass Spectrometry
ASTM C 1590 : 2004 : R2014 Standard Practice for Alternate Actinide Calibration for Inductively Coupled Plasma-Mass Spectrometry
ASTM C 1411 : 2014 Standard Practice for The Ion Exchange Separation of Uranium and Plutonium Prior to Isotopic Analysis
ASTM C 1832 : 2016 Standard Test Method for Determination of Uranium Isotopic Composition by the Modified Total Evaporation (MTE) Method Using a Thermal Ionization Mass Spectrometer
ASTM C 1871 : 2018 : REV A Standard Test Method for Determination of Uranium Isotopic Composition by the Double Spike Method Using a Thermal Ionization Mass Spectrometer
ASTM C 1022 : 2017 Standard Test Methods for Chemical and Atomic Absorption Analysis of Uranium-Ore Concentrate
ASTM C 696 : 2011 Standard Test Methods for Chemical, Mass Spectrometric, and Spectrochemical Analysis of Nuclear-Grade Uranium Dioxide Powders and Pellets

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