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ASTM D 3524 : 2014

Superseded
Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

View Superseded by
superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

Standard Test Method for Diesel Fuel Diluent in Used Diesel Engine Oils by Gas Chromatography
Available format(s)

Hardcopy , PDF

Superseded date

25-11-2020

Language(s)

English

Published date

15-05-2014

CONTAINED IN VOL. 05.02, 2015 Describes the use of gas chromatography to determine the amount of diesel fuel in used engine lubricating oil.

1.1This test method covers the use of gas chromatography to determine the amount of diesel fuel in used engine lubricating oil. This test is limited to SAE 30 oil. The diesel fuel diluent is analyzed at concentrations up to 12 mass %.

Note 1This test method may be applicable to higher viscosity grade oils. However, such oils were not included in the program used to develop the precision statement.

1.2This test method is limited to gas chromatographs equipped with flame ionization detectors and temperature programmable ovens.

Note 2The use of other detectors and instrumentation has been reported. However, the precision statement applies only when the instrumentation specified is employed.

1.3There is some overlap of the boiling ranges of diesel fuel and SAE 30 engine oils. Moreover, the boiling range of SAE 30 oils from various sources can vary appreciably. As a result, the calibration can be altered by as much as 2 %, in terms of fuel dilution. When testing unknown or mixed brands of used engine oil, it should be realized that the precision of the method may be poorer than the precision obtained when calibrating with a new oil representative of the used oil being tested.

1.4The values stated in SI units are to be regarded as the standard. The values stated in inch-pound units are for information only.

1.5This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory requirements prior to use.

Committee
D 02
DocumentType
Test Method
Pages
6
PublisherName
American Society for Testing and Materials
Status
Superseded
SupersededBy
Supersedes

ASTM D 8048 : 2017-05 TEST METHOD FOR EVALUATION OF DIESEL ENGINE OILS IN T-13 DIESEL ENGINE
ASTM D 5290 : 1991 Standard Test Method for Measurement of Oil Consumption, Piston Deposits and Wear in a Heavy-Duty High Speed Diesel Engine-NTC-400 Procedure (Withdrawn 1997)
SAE J 357 : 2016 PHYSICAL AND CHEMICAL PROPERTIES OF ENGINE OILS
ASTM D 6681 : 2017 Standard Test Method for Evaluation of Engine Oils in a High Speed, Single-Cylinder Diesel Engine—Caterpillar 1P Test Procedure
ASTM D 8048 : 2019 Standard Test Method for Evaluation of Diesel Engine Oils in T-13 Diesel Engine
ASTM D 6224 : 2016 Standard Practice for In-Service Monitoring of Lubricating Oil for Auxiliary Power Plant Equipment
ASTM D 7593 : 2014 : REDLINE Standard Test Method for Determination of Fuel Dilution for In-Service Engine Oils by Gas Chromatography
ASTM D 6681 : 2017 : REDLINE Standard Test Method for Evaluation of Engine Oils in a High Speed, Single-Cylinder Diesel Engine—Caterpillar 1P Test Procedure
ASTM D 7156 : 2017 : REDLINE Standard Test Method for Evaluation of Diesel Engine Oils in the T-11 Exhaust Gas Recirculation Diesel Engine
ASTM D 7593 : 2014 Standard Test Method for Determination of Fuel Dilution for In-Service Engine Oils by Gas Chromatography
ASTM D 6750 : 2019 Standard Test Methods for Evaluation of Engine Oils in a High-Speed, Single-Cylinder Diesel Engine—1K Procedure (0.4 % Fuel Sulfur) and 1N Procedure (0.04 % Fuel Sulfur)
ASTM D 8047 : 2018 Standard Test Method for Evaluation of Engine Oil Aeration Resistance in a Caterpillar C13 Direct-Injected Turbocharged Automotive Diesel Engine
ASTM D 8074 : 2018 Standard Test Method for Evaluation of Diesel Engine Oils in DD13 Diesel Engine
ASTM D 7156 : 2017 Standard Test Method for Evaluation of Diesel Engine Oils in the T-11 Exhaust Gas Recirculation Diesel Engine
ASTM D 6923 : 2018 Standard Test Method for Evaluation of Engine Oils in a High Speed, Single-Cylinder Diesel Engine—Caterpillar 1R Test Procedure
08/30190684 DC : DRAFT OCT 2008 BS ISO 18436-5 - CONDITION MONITORING AND DIAGNOSTICS OF MACHINES - REQUIREMENTS FOR QUALIFICATION AND ASSESSMENT OF PERSONNEL - PART 5: LUBRICANT LABORATORY TECHNICIAN/ANALYST
BS ISO 18436-5:2012 Condition monitoring and diagnostics of machines. Requirements for qualification and assessment of personnel Lubricant laboratory technician/analyst
UNI ISO 18436-5 : 2013 CONDITION MONITORING AND DIAGNOSTICS OF MACHINES - REQUIREMENTS FOR QUALIFICATION AND ASSESSMENT OF PERSONNEL - PART 5: LUBRICANT LABORATORY TECHNICIAN/ANALYST
ASTM D 8074 : 2016 Standard Test Method for Evaluation of Diesel Engine Oils in DD13 Diesel Engine
ASTM D 6224 : 2016 : REDLINE Standard Practice for In-Service Monitoring of Lubricating Oil for Auxiliary Power Plant Equipment
ISO 18436-5:2012 Condition monitoring and diagnostics of machines — Requirements for qualification and assessment of personnel — Part 5: Lubricant laboratory technician/analyst

ASTM E 1510 : 1995 : R2013 : EDT 1 Standard Practice for Installing Fused Silica Open Tubular Capillary Columns in Gas Chromatographs
ASTM E 260 : 1996 Standard Practice for Packed Column Gas Chromatography
ASTM D 4626 : 1995 : R2005 Standard Practice for Calculation of Gas Chromatographic Response Factors
ASTM E 1510 : 1995 : R2000 Standard Practice for Installing Fused Silica Open Tubular Capillary Columns in Gas Chromatographs
ASTM E 1510 : 1995 : R2005 Standard Practice for Installing Fused Silica Open Tubular Capillary Columns in Gas Chromatographs
ASTM E 1510 : 1995 Standard Practice for Installing Fused Silica Open Tubular Capillary Columns in Gas Chromatographs
ASTM D 4626 : 1995 : R2019 Standard Practice for Calculation of Gas Chromatographic Response Factors
ASTM D 4626 : 1995 : R2015 Standard Practice for Calculation of Gas Chromatographic Response Factors
ASTM D 4626 : 1995 : R2000 Standard Practice for Calculation of Gas Chromatographic Response Factors
ASTM D 4626 : 1995 : R2010 Standard Practice for Calculation of Gas Chromatographic Response Factors

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