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ASTM D 4165 : 2006 : R2012

Superseded
Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

View Superseded by
superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

Standard Test Method for Cyanogen Chloride in Water
Available format(s)

Hardcopy , PDF

Superseded date

23-01-2020

Language(s)

English

Published date

15-06-2012

This test method covers the determination of cyanogen chloride in water.

1.1 This test method covers the determination of cyanogen chloride in water. Cyanogen chloride is normally present only at very low concentrations; it is a very labile and sparsely soluble gaseous compound. Water samples may contain cyanogen chloride after the chlorination of waste waters containing cyanide or thiocyanate compounds.

1.2 Cyanogen chloride is unstable. A quick test using a spot plate or comparator as soon as the sample is collected may be the best test, reducing the loss of cyanogen chloride during the time lapse between sampling and analysis. (See Fig. 1 for a typical decay curve for cyanogen chloride in a solution.)

1.3 This test method has been used successfully with reagent water. The analyst is responsible for determining whether the test method is applicable to the water matrix being tested. Reference is made to Test Method D of Test Methods D2036 which is based on similar chemical reactions and has been evaluated by collaborative testing in this matrix.

1.4 The lower limit of detectability is 0.005 mg CN /L.

1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific hazard statements are given in Note 1 and Note 2 and Section 9.


FIG. 1 Cyanogen Chloride Stability

Committee
D 19
DocumentType
Test Method
Pages
4
ProductNote
Reconfirmed 2012
PublisherName
American Society for Testing and Materials
Status
Superseded
SupersededBy
Supersedes

ASTM D 3694 : 1996 : R2017 Standard Practices for Preparation of Sample Containers and for Preservation of Organic Constituents

ASTM D 3370 : 1995 : REV A : R2003 : EDT 1 Standard Practices for Sampling Water from Closed Conduits
ASTM D 1129 : 2013 : REDLINE Standard Terminology Relating to Water
ASTM D 1129 : 2003 Standard Terminology Relating to Water
ASTM D 1129 : 2013 Standard Terminology Relating to Water
ASTM D 2036 : 1991 Standard Test Methods for Cyanides in Water
ASTM D 5847 : 1999 : REV A : EDT 1 Standard Practice for Writing Quality Control Specifications for Standard Test Methods for Water Analysis
ASTM D 1193 : 1977 : R1983 : EDT 1 Standard Specification for Reagent Water
ASTM D 5847 : 2002 : R2007 Standard Practice for Writing Quality Control Specifications for Standard Test Methods for Water Analysis
ASTM D 1129 : 2006 Standard Terminology Relating to Water
ASTM D 3370 : 2010 Standard Practices for Sampling Water from Closed Conduits
ASTM E 275 : 2008 Describing and Measuring Performance of Ultraviolet and Visible Spectrophotometers
ASTM D 5847 : 2002 : R2012 Standard Practice for Writing Quality Control Specifications for Standard Test Methods for Water Analysis
ASTM D 2036 : 2009 : R2015 Standard Test Methods for Cyanides in Water
ASTM D 3370 : 2008 Standard Practices for Sampling Water from Closed Conduits
ASTM D 1129 : 1999 : REV A Standard Terminology Relating to Water
ASTM D 2036 : 1998 Standard Test Methods for Cyanides in Water
ASTM D 3856 : 2011 Standard Guide for Management Systems in Laboratories Engaged in Analysis of Water
ASTM D 1129 : 2006 : REV A Standard Terminology Relating to Water
ASTM D 1193 : 2006 : R2011 Standard Specification for Reagent Water
ASTM D 1129 : 2003 : REV A Standard Terminology Relating to Water
ASTM D 1129 : 2002 Standard Terminology Relating to Water
ASTM D 2036 : 2009 Standard Test Methods for Cyanides in Water
ASTM D 1193 : 1991 Standard Specification for Reagent Water
ASTM D 3856 : 1995 : R2006 Standard Guide for Good Laboratory Practices in Laboratories Engaged in Sampling and Analysis of Water
ASTM D 1129 : 2004 Standard Terminology Relating to Water
ASTM D 3856 : 2011 : R2015 Standard Guide for Management Systems in Laboratories Engaged in Analysis of Water (Withdrawn 2024)
ASTM D 3856 : 1995 : R2000 Standard Guide for Good Laboratory Practices in Laboratories Engaged in Sampling and Analysis of Water
ASTM D 3370 : 2018 Standard Practices for Sampling Water from Flowing Process Streams
ASTM D 1129 : 2002 : REV A Standard Terminology Relating to Water
ASTM D 5847 : 2002 Standard Practice for Writing Quality Control Specifications for Standard Test Methods for Water Analysis
ASTM D 3370 : 1976 Standard Practices for Sampling Water
ASTM D 1193 : 1970 Standard Specification For Reagent Water
ASTM D 1193 : 2006 Standard Specification for Reagent Water
ASTM D 3370 : 1995 : REV A : R1999 : EDT 1 Standard Practices for Sampling Water from Closed Conduits
ASTM D 1193 : 1999 Standard Specification for Reagent Water
ASTM D 1129 : 2010 Standard Terminology Relating to Water
ASTM D 4210 : 1989 : R1996 : EDT 1 Standard Practice for Intralaboratory Quality Control Procedures and a Discussion on Reporting Low-Level Data (Withdrawn 2002)
ASTM D 3370 : 2007 Standard Practices for Sampling Water from Closed Conduits
ASTM D 2036 : 2006 Standard Test Methods for Cyanides in Water
ASTM D 1129 : 2006 : REV A : EDT 1 Standard Terminology Relating to Water
ASTM D 1129 : 2001 Standard Terminology Relating to Water
ASTM D 1129 : 2004 : EDT 1 Standard Terminology Relating to Water
ASTM D 1193 : 2006 : R2018 Standard Specification for Reagent Water

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