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ASTM D 4928 : 2012

Superseded
Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

View Superseded by
superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

Standard Test Method for Water in Crude Oils by Coulometric Karl Fischer Titration
Available format(s)

Hardcopy , PDF

Superseded date

31-08-2020

Language(s)

English

Published date

01-12-2012

1.1This test method covers the determination of water in the range from 0.02 to 5.00 mass or volume % in crude oils. Mercaptan (RSH) and sulfide (S or H2S) as sulfur are known to interfere with this test method, but at levels of less than 500 μg/g [ppm(m)], the interference from these compounds is insignificant (see Section 6).

1.2This test method can be used to determine water in the 0.005 to 0.02 mass % range, but the effects of the mercaptan and sulfide interference at these levels has not been determined. For the range 0.005 to 0.02 mass %, there is no precision or bias statement.

1.3This test method is intended for use with standard commercially available coulometric Karl Fischer reagent.

1.4The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.5This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific warning statements, see Section 8.

Committee
D 02
DocumentType
Test Method
Pages
6
PublisherName
American Society for Testing and Materials
Status
Superseded
SupersededBy
Supersedes

ASTM E 203 : 2016 Standard Test Method for Water Using Volumetric Karl Fischer Titration
ASTM D 7720 : 2011 : R2017 Standard Guide for Statistically Evaluating Measurand Alarm Limits when Using Oil Analysis to Monitor Equipment and Oil for Fitness and Contamination
ASTM D 3230 : 2019 Standard Test Method for Salts in Crude Oil (Electrometric Method)
ASTM D 482 : 2013 Standard Test Method for Ash from Petroleum Products
ASTM D 4177 : 2016 : EDT 1 Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
ASTM D 7059 : 2009 : R2017 Standard Test Method for Determination of Methanol in Crude Oils by Multidimensional Gas Chromatography
ASTM D 6470 : 1999 : R2015 Standard Test Method for Salt in Crude Oils (Potentiometric Method)
ASTM D 7829 : 2013 : R2018 Standard Guide for Sediment and Water Determination in Crude Oil

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