ASTM D 4951 : 2014
Superseded
Superseded
A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.
View Superseded by
superseded
A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.
Standard Test Method for Determination of Additive Elements in Lubricating Oils by Inductively Coupled Plasma Atomic Emission Spectrometry
Available format(s)
Hardcopy , PDF
Superseded date
11-11-2014
Language(s)
English
Published date
01-10-2014
1.1This test method covers the quantitative determination of barium, boron, calcium, copper, magnesium, molybdenum, phosphorus, sulfur, and zinc in unused lubricating oils and additive packages.
1.2The precision statements are valid for dilutions in which the mass % sample in solvent is held constant in the range of 1 to 5 mass % oil.
1.3The precision tables define the concentration ranges covered in the interlaboratory study. However, both lower and higher concentrations can be determined by this test method. The low concentration limits are dependent on the sensitivity of the ICP instrument and the dilution factor. The high concentration limits are determined by the product of the maximum concentration defined by the linear calibration curve and the sample dilution factor.
1.4Sulfur can be determined if the instrument can operate at a wavelength of 180 nm.
1.5The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.6This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
| Committee |
D 02
|
| DocumentType |
Test Method
|
| Pages |
8
|
| PublisherName |
American Society for Testing and Materials
|
| Status |
Superseded
|
| SupersededBy | |
| Supersedes |
| ASTM D 4857 : 2012 | Standard Test Method for Determination of the Ability of Lubricants to Minimize Ring Sticking and Piston Deposits in Two-Stroke-Cycle Gasoline Engines Other Than Outboards (Withdrawn 2021) |
| ASTM D 6751 : 2019 | Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels |
| ASTM D 7303 : 2017 | Standard Test Method for Determination of Metals in Lubricating Greases by Inductively Coupled Plasma Atomic Emission Spectrometry |
| ASTM D 7876 : 2013 : R2018 | Standard Practice for Practice for Sample Decomposition Using Microwave Heating (With or Without Prior Ashing) for Atomic Spectroscopic Elemental Determination in Petroleum Products and Lubricants |
| ASTM D 6443 : 2014 : R2019 : EDT 1 | Standard Test Method for Determination of Calcium, Chlorine, Copper, Magnesium, Phosphorus, Sulfur, and Zinc in Unused Lubricating Oils and Additives by Wavelength Dispersive X-ray Fluorescence Spectrometry (Mathematical Correction Procedure) |
| ASTM D 6074 : 2015 | Standard Guide for Characterizing Hydrocarbon Lubricant Base Oils |
| ASTM E 2097 : 2000 : R2014 | Standard Guide for Determining the Impact of Extractables from Non-Metallic Materials on the Safety of Biotechnology Products (Withdrawn 2022) |
| ASTM D 7260 : 2019 | Standard Practice for Optimization, Calibration, and Validation of Inductively Coupled Plasma-Atomic Emission Spectrometry (ICP-AES) for Elemental Analysis of Petroleum Products and Lubricants |
| ASTM D 7455 : 2019 | Standard Practice for Sample Preparation of Petroleum and Lubricant Products for Elemental Analysis |
| ASTM D 7578 : 2018 | Standard Guide for Calibration Requirements for Elemental Analysis of Petroleum Products and Lubricants |
| ASTM D 7040 : 2004 : R2015 | Standard Test Method for Determination of Low Levels of Phosphorus in ILSAC GF 4 and Similar Grade Engine Oils by Inductively Coupled Plasma Atomic Emission Spectrometry |
| ASTM D 4057 : 2019 | Standard Practice for Manual Sampling of Petroleum and Petroleum Products |
| ASTM D 1552 : 2003 | Standard Test Method for Sulfur in Petroleum Products (High-Temperature Method) |
| ASTM D 6299 : 2010 | Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance |
| ASTM D 6299 : 2013 : EDT 1 | Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance |
| ASTM D 5185 : 1997 | Standard Test Method for Determination of Additive Elements, Wear Metals, and Contaminants in Used Lubricating Oils and Determination of Selected Elements in Base Oils by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES) |
| ASTM D 6299 : 2017 : REV A | Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance |
| ASTM D 4927 : 2010 | Standard Test Methods for Elemental Analysis of Lubricant and Additive Components—Barium, Calcium, Phosphorus, Sulfur, and Zinc by Wavelength-Dispersive X-Ray Fluorescence Spectroscopy |
| ASTM D 6299 : 2017 : REV B | Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance |
| ASTM D 6299 : 2009 | Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance |
| ASTM D 1552 : 2008 : R2014 | Standard Test Method for Sulfur in Petroleum Products (High-Temperature Method) |
| ASTM D 4057 : 2012 : R2018 | Standard Practice for Manual Sampling of Petroleum and Petroleum Products |
| ASTM D 6299 : 2013 | Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance |
| ASTM D 4927 : 2002 | Standard Test Methods for Elemental Analysis of Lubricant and Additive Components—Barium, Calcium, Phosphorus, Sulfur, and Zinc by Wavelength-Dispersive X-Ray Fluorescence Spectroscopy |
| ASTM D 1552 : 1990 : EDT 1 | Standard Test Method for Sulfur in Petroleum Products (High-Temperature Method) |
| ASTM D 4628 : 2014 | Standard Test Method for Analysis of Barium, Calcium, Magnesium, and Zinc in Unused Lubricating Oils by Atomic Absorption Spectrometry |
| ASTM D 1552 : 2016 | Standard Test Method for Sulfur in Petroleum Products by High Temperature Combustion and Infrared (IR) Detection or Thermal Conducitivity Detection (TCD) |
| ASTM D 4927 : 2005 | Standard Test Methods for Elemental Analysis of Lubricant and Additive Components—Barium, Calcium, Phosphorus, Sulfur, and Zinc by Wavelength-Dispersive X-Ray Fluorescence Spectroscopy |
| ASTM D 6299 : 2010 : EDT 1 | Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance |
| ASTM D 4927 : 1996 | Standard Test Methods for Elemental Analysis of Lubricant and Additive Components—Barium, Calcium, Phosphorus, Sulfur, and Zinc by Wavelength-Dispersive X-Ray Fluorescence Spectroscopy |
| ASTM D 5185 : 2005 | Standard Test Method for Determination of Additive Elements, Wear Metals, and Contaminants in Used Lubricating Oils and Determination of Selected Elements in Base Oils by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES) |
| ASTM D 4057 : 1981 : EDT 2 | Standard Practice for Manual Sampling of Petroleum and Petroleum Products |
| ASTM D 5185 : 2002 | Standard Test Method for Determination of Additive Elements, Wear Metals, and Contaminants in Used Lubricating Oils and Determination of Selected Elements in Base Oils by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES) |
| ASTM D 4628 : 2005 | Standard Test Method for Analysis of Barium, Calcium, Magnesium, and Zinc In Unused Lubricating Oils By Atomic Absorption Spectrometry |
| ASTM D 1552 : 2000 | Standard Test Method for Sulfur in Petroleum Products (High-Temperature Method) |
| ASTM D 4628 : 2002 | Standard Test Method for Analysis of Barium, Calcium, Magnesium, and Zinc In Unused Lubricating Oils By Atomic Absorption Spectrometry |
| ASTM D 5185 : 2018 | Standard Test Method for Multielement Determination of Used and Unused Lubricating Oils and Base Oils by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES) |
| ASTM D 4628 : 2016 | Standard Test Method for Analysis of Barium, Calcium, Magnesium, and Zinc in Unused Lubricating Oils by Atomic Absorption Spectrometry |
| ASTM D 4307 : 1999 : R2004 | Standard Practice for Preparation of Liquid Blends for Use as Analytical Standards |
| ASTM D 5185 : 2013 : EDT 1 | Standard Test Method for Multielement Determination of Used and Unused Lubricating Oils and Base Oils by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES) |
| ASTM D 6299 : 2000 | Standard Practice for Applying Statistical Quality Assurance Techniques to Evaluate Analytical Measurement System Performance |
| ASTM D 6299 : 2010 : EDT 2 | Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance |
| ASTM D 6299 : 2016 | Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance |
| ASTM D 4628 : 2005 : R2011 : EDT 1 | Standard Test Method for Analysis of Barium, Calcium, Magnesium, and Zinc in Unused Lubricating Oils by Atomic Absorption Spectrometry |
| ASTM D 4057 : 2006 | Standard Practice for Manual Sampling of Petroleum and Petroleum Products |
| ASTM D 4057 : 2012 | Standard Practice for Manual Sampling of Petroleum and Petroleum Products |
| ASTM D 6299 : 2000 : REV A | Standard Practice for Applying Statistical Quality Assurance Techniques to Evaluate Analytical Measurement System Performance |
| ASTM D 4927 : 2015 | Standard Test Methods for Elemental Analysis of Lubricant and Additive Components—Barium, Calcium, Phosphorus, Sulfur, and Zinc by Wavelength-Dispersive X-Ray Fluorescence Spectroscopy |
| ASTM D 5185 : 2013 | Standard Test Method for Multielement Determination of Used and Unused Lubricating Oils and Base Oils by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES) |
| ASTM D 4307 : 1999 | Standard Practice for Preparation of Liquid Blends for Use as Analytical Standards |
| ASTM D 4927 : 2001 | Standard Test Methods for Elemental Analysis of Lubricant and Additive Components—Barium, Calcium, Phosphorus, Sulfur, and Zinc by Wavelength-Dispersive X-Ray Fluorescence Spectroscopy |
| ASTM D 1552 : 2016 : EDT 1 | Standard Test Method for Sulfur in Petroleum Products by High Temperature Combustion and Infrared (IR) Detection or Thermal Conductivity Detection (TCD) |
| ASTM D 1552 : 2007 | Standard Test Method for Sulfur in Petroleum Products (High-Temperature Method) |
| ASTM D 1552 : 1995 | Standard Test Method for Sulfur in Petroleum Products (High-Temperature Method) |
| ASTM D 1552 : 2015 | Standard Test Method for Sulfur in Petroleum Products by High Temperature Combustion and IR Detection |
| ASTM D 4307 : 2017 | Standard Practice for Preparation of Liquid Blends for Use as Analytical Standards |
| ASTM D 1552 : 2001 | Standard Test Method for Sulfur in Petroleum Products (High-Temperature Method) |
| ASTM D 6299 : 2008 | Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance |
| ASTM D 1552 : 2008 : R2014 : EDT 1 | Standard Test Method for Sulfur in Petroleum Products (High-Temperature Method) |
| ASTM D 4927 : 2014 | Standard Test Methods for Elemental Analysis of Lubricant and Additive Components—Barium, Calcium, Phosphorus, Sulfur, and Zinc by Wavelength-Dispersive X-Ray Fluorescence Spectroscopy |
| ASTM D 6299 : 2002 : EDT 1 | Standard Practice for Applying Statistical Quality Assurance Techniques to Evaluate Analytical Measurement System Performance |
| ASTM D 4307 : 1999 : R2010 | Standard Practice for Preparation of Liquid Blends for Use as Analytical Standards |
| ASTM D 5185 : 2009 | Standard Test Method for Determination of Additive Elements, Wear Metals, and Contaminants in Used Lubricating Oils and Determination of Selected Elements in Base Oils by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES) |
| ASTM D 1552 : 2008 | Standard Test Method for Sulfur in Petroleum Products (High-Temperature Method) |
| ASTM D 5185 : 2002 : EDT 1 | Standard Test Method for Determination of Additive Elements, Wear Metals, and Contaminants in Used Lubricating Oils and Determination of Selected Elements in Base Oils by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES) |
| ASTM D 4628 : 1997 | Standard Test Method for Analysis of Barium, Calcium, Magnesium, and Zinc In Unused Lubricating Oils By Atomic Absorption Spectrometry |
| ASTM D 5185 : 2002 : EDT 2 | Standard Test Method for Determination of Additive Elements, Wear Metals, and Contaminants in Used Lubricating Oils and Determination of Selected Elements in Base Oils by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES) |
| ASTM D 6299 : 2007 | Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance |
| ASTM D 6299 : 2007 : EDT 1 | Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance |
| ASTM D 4057 : 1995 : R2000 | Standard Practice for Manual Sampling of Petroleum and Petroleum Products |
| ASTM D 6299 : 2017 | Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance |
| ASTM D 4307 : 1999 : R2015 | Standard Practice for Preparation of Liquid Blends for Use as Analytical Standards |
| ASTM D 4057 : 2006 : R2011 | Standard Practice for Manual Sampling of Petroleum and Petroleum Products |
| ASTM D 1552 : 1983 | Standard Test Method for Sulfur in Petroleum Products (High-Temperature Method) |
| ASTM D 6299 : 2002 | Standard Practice for Applying Statistical Quality Assurance Techniques to Evaluate Analytical Measurement System Performance |
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