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ASTM D 5765 : 2016

Current
Current

The latest, up-to-date edition.

Standard Practice for Solvent Extraction of Total Petroleum Hydrocarbons from Soils and Sediments Using Closed Vessel Microwave Heating
Available format(s)

Hardcopy , PDF

Language(s)

English

Published date

01-01-2016

Publisher

American Society for Testing and Materials

This practice covers the solvent extraction of total petroleum hydrocarbon (TPH) from soils and sediments, using closed vessel microwave heating, for subsequent determination by gravimetric or gas chromatographic techniques.

1.1This practice covers the solvent extraction of total petroleum hydrocarbon (TPH) from soils and sediments, using closed vessel microwave heating, for subsequent determination by gravimetric or gas chromatographic techniques.

1.2This practice is recommended only for solid samples that can pass through a ten mesh screen (approximately 2 mm openings).

1.3The solvent extract obtained by this practice may be analyzed for total or specific nonvolatile and semivolatile petroleum hydrocarbons but may require sample clean-up procedures prior to specific compound analysis.

1.4This practice is limited to solvents that are recommended for use in microwave solvent extraction systems.

1.5The values stated in SI units are to be regarded as standard.

1.5.1Exception—The inch-pound values given for units of pressure are to be regarded as standard; SI unit conversions are shown in parentheses.

1.6This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific hazard statements are given in Section 9.

Committee
D 19
DocumentType
Standard Practice
Pages
3
PublisherName
American Society for Testing and Materials
Status
Current
Supersedes

ASTM D 7876 : 2013 : R2018 Standard Practice for Practice for Sample Decomposition Using Microwave Heating (With or Without Prior Ashing) for Atomic Spectroscopic Elemental Determination in Petroleum Products and Lubricants

ASTM D 3694 : 1996 : R2011 Standard Practices for Preparation of Sample Containers and for Preservation of Organic Constituents
ASTM D 1129 : 2003 Standard Terminology Relating to Water
ASTM D 3974 : 1981 : R2008 Standard Practices for Extraction of Trace Elements from Sediments
ASTM D 5368 : 1993 : R2006 Standard Test Methods for Gravimetric Determination of Total Solvent Extractable Content (TSEC) of Solid Waste Samples
ASTM D 1129 : 2013 Standard Terminology Relating to Water
ASTM D 1129 : 2013 : R2020 Standard Terminology Relating to Water
ASTM D 3694 : 1996 Standard Practices for Preparation of Sample Containers and for Preservation of Organic Constituents
ASTM D 3976 : 1992 : R2005 Standard Practice for Preparation of Sediment Samples for Chemical Analysis
ASTM D 1129 : 2013 : R2020 : EDT 2 Standard Terminology Relating to Water
ASTM D 3976 : 1992 : R2001 Standard Practice for Preparation of Sediment Samples for Chemical Analysis
ASTM D 1129 : 2006 Standard Terminology Relating to Water
ASTM D 3976 : 1992 : R2010 Standard Practice for Preparation of Sediment Samples for Chemical Analysis
ASTM D 3974 : 2009 : R2023 Standard Practices for Extraction of Trace Elements from Sediments
ASTM D 3974 : 2009 Standard Practices for Extraction of Trace Elements from Sediments
ASTM D 3974 : 2009 : R2015 Standard Practices for Extraction of Trace Elements from Sediments
ASTM D 3976 : 1992 : R1996 Standard Practice for Preparation of Sediment Samples for Chemical Analysis
ASTM D 3694 : 1996 : R2017 Standard Practices for Preparation of Sample Containers and for Preservation of Organic Constituents
ASTM D 1129 : 2013 : R2020 : EDT 1 Standard Terminology Relating to Water
ASTM D 1129 : 1999 : REV A Standard Terminology Relating to Water
ASTM D 3856 : 2011 Standard Guide for Management Systems in Laboratories Engaged in Analysis of Water
ASTM D 1129 : 2006 : REV A Standard Terminology Relating to Water
ASTM D 3974 : 1981 : R2003 : EDT 1 Standard Practices for Extraction of Trace Elements from Sediments
ASTM D 1129 : 2003 : REV A Standard Terminology Relating to Water
ASTM D 3694 : 1996 : R2004 Standard Practices for Preparation of Sample Containers and for Preservation of Organic Constituents
ASTM D 1129 : 2002 Standard Terminology Relating to Water
ASTM D 5368 : 2013 Standard Test Methods for Gravimetric Determination of Total Solvent Extractable Content (TSEC) of Solid Waste Samples (Withdrawn 2014)
ASTM D 3856 : 1995 : R2006 Standard Guide for Good Laboratory Practices in Laboratories Engaged in Sampling and Analysis of Water
ASTM D 3974 : 1981 : R1999 Standard Practices for Extraction of Trace Elements from Sediments
ASTM D 5368 : 1993 Standard Test Methods for Gravimetric Determination of Total Solvent Extractable Content (TSEC) of Solid Waste Samples
ASTM D 1129 : 2004 Standard Terminology Relating to Water
ASTM D 3976 : 2022 Standard Practice for Preparation of Sediment Samples for Chemical Analysis
ASTM D 3976 : 1992 : R2015 Standard Practice for Preparation of Sediment Samples for Chemical Analysis
ASTM D 3856 : 2011 : R2015 Standard Guide for Management Systems in Laboratories Engaged in Analysis of Water (Withdrawn 2024)
ASTM D 3856 : 1995 : R2000 Standard Guide for Good Laboratory Practices in Laboratories Engaged in Sampling and Analysis of Water
ASTM D 5368 : 1993 : R2001 Standard Test Methods for Gravimetric Determination of Total Solvent Extractable Content (TSEC) of Solid Waste Samples
ASTM D 1129 : 2002 : REV A Standard Terminology Relating to Water
ASTM D 1129 : 2010 Standard Terminology Relating to Water
ASTM D 1129 : 2006 : REV A : EDT 1 Standard Terminology Relating to Water
ASTM D 1129 : 2001 Standard Terminology Relating to Water
ASTM D 1129 : 2004 : EDT 1 Standard Terminology Relating to Water

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