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ASTM D 6047 : 2017

Superseded
Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

View Superseded by
superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

Standard Test Methods for Rubber, Raw—Determination of 5-Ethylidenenorbornene (ENB) or Dicyclopentadiene (DCPD) in Ethylene-Propylene-Diene (EPDM) Terpolymers
Available format(s)

Hardcopy , PDF

Superseded date

21-01-2022

Language(s)

English

Published date

25-10-2017

Publisher

American Society for Testing and Materials

1.1These test methods cover the determination of the content of 5-ethylidenenorbornene (ENB) or Dicyclopentadiene (DCPD) in ethylene-propylene-diene (EPDM) terpolymers. They are applicable to diene contents in the 0.1 to 10 mass % range.

1.2ENB and DCPD are dienes introduced in ethylene/propylene rubbers to generate specific cure properties. Since high precision for diene content determination has become very important, a Fourier Transform Infrared Spectroscopic (FTIR) method was developed. Diene determination was performed in the past by a refractive index technique.

Note 1:The procedures for % ENB and % DCPD differ only in the location in the infrared (IR) of the IR peak being quantified.

1.3The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.4This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.

1.5This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

Committee
D 11
DocumentType
Test Method
Pages
8
PublisherName
American Society for Testing and Materials
Status
Superseded
SupersededBy
Supersedes

ASTM E 1421 : 1999 : R2021 Standard Practice for Describing and Measuring Performance of Fourier Transform Mid-Infrared (FT-MIR) Spectrometers: Level Zero and Level One Tests
ASTM D 3900 : 2005 : REV A Standard Test Methods for Rubber-Determination of Ethylene Units in Ethylene-Propylene Copolymers (EPM) and in Ethylene-Propylene-Diene Terpolymers (EPDM) by Infrared Spectrometry
ASTM E 1421 : 1999 : R2004 Standard Practice for Describing and Measuring Performance of Fourier Transform Mid-Infrared (FT-MIR) Spectrometers: Level Zero and Level One Tests
ASTM D 4483 : 1999 Standard Practice for Determining Precision for Test Method Standards in the Rubber and Carbon Black Industries
ASTM D 4483 : 2020 Standard Practice for Evaluating Precision for Test Method Standards in the Rubber and Carbon Black Manufacturing Industries
ASTM D 3568 : 2003 : R2013 Standard Test Methods for Rubber—Evaluation of EPDM (Ethylene Propylene Diene Terpolymers) Including Mixtures With Oil
ASTM D 4483 : 2005 : REV A Standard Practice for Evaluating Precision for Test Method Standards in the Rubber and Carbon Black Manufacturing Industries
ASTM E 932 : 1989 : R2013 Standard Practice for Describing and Measuring Performance of Dispersive Infrared Spectrometers
ASTM D 3900 : 2017 Standard Test Methods for Rubber—Determination of Ethylene Units in Ethylene-Propylene Copolymers (EPM) and in Ethylene-Propylene-Diene Terpolymers (EPDM) by Infrared Spectrometry
ASTM D 3568 : 1998 Standard Test Methods for Rubber-Evaluation of EPDM (Ethylene Propylene Diene Terpolymers) Including Mixtures With Oil
ASTM D 3900 : 2015 Standard Test Methods for Rubber—Determination of Ethylene Units in Ethylene-Propylene Copolymers (EPM) and in Ethylene-Propylene-Diene Terpolymers (EPDM) by Infrared Spectrometry
ASTM D 3900 : 1995 : R2000 Standard Test Methods for Rubber Raw-Determination of Ethylene Units in EPM (Ethylene-Propylene Copolymers) and EPDM (Ethylene-Propylene-Diene Terpolymers)
ASTM E 1421 : 1999 : R2009 Standard Practice for Describing and Measuring Performance of Fourier Transform Mid-Infrared (FT-MIR) Spectrometers: Level Zero and Level One Tests
ASTM E 1421 : 1999 : R2015 : EDT 1 Standard Practice for Describing and Measuring Performance of Fourier Transform Mid-Infrared (FT-MIR) Spectrometers: Level Zero and Level One Tests
ASTM D 3900 : 2005 Standard Test Methods for Rubber-Determination of Ethylene Units in Ethylene-Propylene Copolymers (EPM) and in Ethylene-Propylene-Diene Terpolymers (EPDM) by Infrared Spectrometry
ASTM E 932 : 1989 : R2021 Standard Practice for Describing and Measuring Performance of Dispersive Infrared Spectrometers
ASTM E 1421 : 1999 Standard Practice for Describing and Measuring Performance of Fourier Transform Mid-Infrared (FT-MIR) Spectrometers Level Zero and Level One Tests
ASTM D 3568 : 2003 Standard Test Methods for Rubber—Evaluation of EPDM (Ethylene Propylene Diene Terpolymers) Including Mixtures With Oil
ASTM D 3568 : 2003 : R2009 Standard Test Methods for Rubber—Evaluation of EPDM (Ethylene Propylene Diene Terpolymers) Including Mixtures With Oil
ASTM D 3900 : 2017 : R2021 Standard Test Methods for Rubber—Determination of Ethylene Units in Ethylene-Propylene Copolymers (EPM) and in Ethylene-Propylene-Diene Terpolymers (EPDM) by Infrared Spectrometry
ASTM D 3900 : 1995 : R2004 : EDT 1 Standard Test Methods for Rubber-Determination of Ethylene Units in Ethylene-Propylene Copolymers (EPM) and in Ethylene-Propylene-Diene Terpolymers (EPDM) by Infrared Spectrometry
ASTM D 1416 : 1989 Test Methods for Rubber from Synthetic Sources--Chemical Analysis (Withdrawn 1996)
ASTM D 4483 : 2005 Standard Practice for Evaluating Precision for Test Method Standards in the Rubber and Carbon Black Manufacturing Industries
ASTM D 3900 : 2005 : REV A : R2010 Standard Test Methods for Rubber-Determination of Ethylene Units in Ethylene-Propylene Copolymers (EPM) and in Ethylene-Propylene-Diene Terpolymers (EPDM) by Infrared Spectrometry
ASTM D 3568 : 2003 : R2018 Standard Test Methods for Rubber—Evaluation of EPDM (Ethylene Propylene Diene Terpolymers) Including Mixtures With Oil
ASTM D 4483 : 2014 : REV A Standard Practice for Evaluating Precision for Test Method Standards in the Rubber and Carbon Black Manufacturing Industries
ASTM D 4483 : 2014 Standard Practice for Evaluating Precision for Test Method Standards in the Rubber and Carbon Black Manufacturing Industries
ASTM D 4483 : 2018 Standard Practice for Evaluating Precision for Test Method Standards in the Rubber and Carbon Black Manufacturing Industries
ASTM D 4483 : 2005 : REV A : R2011 Standard Practice for Evaluating Precision for Test Method Standards in the Rubber and Carbon Black Manufacturing Industries

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