Standard Test Method for Determination of Major and Minor Elements in Coal, Coke, and Solid Residues from Combustion of Coal and Coke by Inductively Coupled Plasma—Atomic Emission Spectrometry

Available format(s)

Hardcopy , PDF

Language(s)

English

Published date

20-10-2021

Publisher

American Society for Testing and Materials

1.1This test method covers a procedure for the analysis of the commonly determined major and minor elements in coal, coke, and solid residues from combustion of coal and coke. These residues may be laboratory ash, bottom ash, fly ash, flue gas desulfurization sludge, and other combustion process residues.

Note 1:There are two interlaboratory studies associated with this test method. The first was conducted in 1997 ( RR:D05-1035)2 and the second was conducted in 2007 ( RR:D05-1032).3 Sulfur trioxide was only included in the 2007 study, and that study only included combustion residues derived from ash and no combustion residues derived from coke.

1.2Units—The values stated in SI units are to be regarded as standard. The values given in parentheses after SI units are provided for information only and are not considered standard.

1.3This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.

1.4This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

Committee	D 05
DocumentType	Test Method
Pages	12
PublisherName	American Society for Testing and Materials
Status	Current
Supersedes	ASTM D 6349 : 2013

ASTM D 1857/D1857M : 2018	Standard Test Method for Fusibility of Coal and Coke Ash
ASTM D 7348 : 2013	Standard Test Methods for Loss on Ignition (LOI) of Solid Combustion Residues
ASTM D 8088 : 2016	Standard Practice for Determination of the Six Major Rare Earth Elements in Fluid Catalytic Cracking Catalysts, Zeolites, Additives, and Related Materials by Inductively Coupled Plasma Optical Emission Spectroscopy
ASTM D 5016 : 2016	Standard Test Method for Total Sulfur in Coal and Coke Combustion Residues Using a High-Temperature Tube Furnace Combustion Method with Infrared Absorption
ASTM D 3174 : 2012 : R2018 : EDT 1	Standard Test Method for Ash in the Analysis Sample of Coal and Coke from Coal
ASTM D 7260 : 2020	Standard Practice for Optimization, Calibration, and Validation of Inductively Coupled Plasma-Atomic Emission Spectrometry (ICP-AES) for Elemental Analysis of Petroleum Products and Lubricants

ASTM D 8146 : 2022	Standard Guide for Evaluating Test Method Capability and Fitness for Use
ASTM D 7582 : 2015 : R2023	Standard Test Methods for Proximate Analysis of Coal and Coke by Macro Thermogravimetric Analysis
ASTM D 8146 : 2018	Standard Guide for Evaluating Test Method Capability and Fitness for Use
ASTM D 3180 : 2015	Standard Practice for Calculating Coal and Coke Analyses from As-Determined to Different Bases
ASTM E 691 : 2020	Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
ASTM E 691 : 2023	Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
ASTM D 7582 : 2015	Standard Test Methods for Proximate Analysis of Coal and Coke by Macro Thermogravimetric Analysis
ASTM D 121 : 2015 : R2024	Standard Terminology of Coal and Coke
ASTM E 691 : 2022	Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
ASTM D 7348 : 2021	Standard Test Methods for Loss on Ignition (LOI) of Solid Combustion Residues
ASTM D 121 : 2015	Standard Terminology of Coal and Coke
ASTM E 691 : 2021	Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
ASTM D 3180 : 2015 : R2023	Standard Practice for Calculating Coal and Coke Analyses from As-Determined to Different Bases