Standard Test Method for Measurement of Effects of Automotive Engine Oils on Fuel Economy of Passenger Cars and Light-Duty Trucks in Sequence VIB Spark Ignition Engine (Withdrawn 2022)

Available format(s)

Hardcopy , PDF

Language(s)

English

Published date

07-06-2013

Publisher

American Society for Testing and Materials

1.1This test method covers an engine test procedure for the measurement of the effects of automotive engine oils on the fuel economy of passenger cars and light-duty trucks with gross vehicle weight of 3856 kg or less. The tests are conducted on a dynamometer test stand using a specified spark-ignition engine with a displacement of 4.6-L. It applies to multiviscosity grade oils used in these applications.

1.2This test method also provides for the running of an abbreviated length test that is referred to as the VIBSJ. The procedure for VIBSJ is identical to the Sequence VIB with the exception of the items specifically listed in Annex A13. The procedure modifications listed in Annex A13 refer to the corresponding section of the Sequence VIB test method.

1.3The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.3.1Exceptions—Where there is no direct SI equivalent such as screw threads, National Pipe Threads/diameters, tubing size, or single source supply equipment specifications. Brake Specific Fuel Consumption is measured in kilograms per kilowatthour. In Figs. A2.4, A2.5, and A2.8, inch-pound units are to be regarded as standard.

1.4This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

1.5This test method is arranged as follows:

Subject	Section
Introduction
Scope	1
Referenced Documents	2
Terminology	3
Summary of Test Method	4
Significance and Use	5
Apparatus	6
General	6.1
Test Engine Configuration	6.2
Laboratory Ambient Conditions	6.3
Engine Speed and Torque Control	6.4
Dynamometer	6.4.1
Dynamometer Torque	6.4.2
Engine Cooling System	6.5
External Oil System	6.6
Fuel System	6.7
Fuel Flow Measurement	6.7.2
Fuel Temperature and Pressure Control to the Fuel Flowmeter	6.7.3
Fuel Temperature and Pressure Control to Engine Fuel Rail	6.7.4
Fuel Supply Pumps	6.7.5
Fuel Filtering	6.7.6
Engine Intake Air Supply	6.8
Intake Air Humidity	6.8.1
Intake Air Filtration	6.8.2
Intake Air Pressure Relief	6.8.3
Temperature Measurement	6.9
Thermocouple Location	6.9.5
AFR Determination	6.10
Exhaust and Exhaust Back Pressure Systems	6.11
Exhaust Manifolds	6.11.1
Laboratory Exhaust System	6.11.2
Exhaust Back Pressure	6.11.3
Pressure Measurement and Pressure Sensor Locations	6.12
Engine Oil	6.12.2
Fuel to Fuel Flowmeter	6.12.3
Fuel to Engine Fuel Rail	6.12.4
Exhaust Back Pressure	6.12.5
Intake Air	6.12.6
Intake Manifold Vacuum/Absolute Pressure	6.12.7
Coolant Flow Differential Pressure	6.12.8
Crankcase Pressure	6.12.9
Engine Hardware and Related Apparatus	6.13
Test Engine Configuration	6.13.1
ECM/EEC (Engine Control) Module	6.13.2
Thermostat/Orifice Plate	6.13.3
Intake Manifold	6.13.4
Flywheel	6.13.5
Wiring Harnesses	6.13.6
EGR Block-Off Plate	6.13.7
Oil Pan	6.13.8
Oil Pump Screen and Pickup Tube	6.13.9
Idle Speed Control Solenoid (ISC) Block-Off Plate	6.13.10
Engine Water Pump	6.13.11
Thermostat Housing	6.13.12
Oil Filter Adapter	6.13.13
Fuel Rail	6.13.14
Miscellaneous Apparatus Related to Engine Operation	6.14
Timing Light	6.14.1
Reagents and Materials	7
Engine Oil	7.1
Test Fuel	7.2
Engine Coolant	7.3
Cleaning Materials	7.4
Preparation of Apparatus	8
Test Stand Preparation	8.2
Engine Preparation	9
Cleaning of Engine Parts	9.2
Engine Assembly Procedure	9.3
General Assembly Instructions	9.3.1
Bolt Torque Specifications	9.3.2
Sealing Compounds	9.3.3
Harmonic Balancer	9.3.5
Oil Pan	9.3.6
Intake Manifold	9.3.7
Camshaft Covers	9.3.8
Thermostat	9.3.9
Thermostat Housing	9.3.10
Coolant Inlet	9.3.11
Oil Filter Adapter	9.3.12
Dipstick Tube	9.3.13
Water Pump	9.3.14
Sensors, Switches, Valves, and Positioners	9.3.15
Ignition System	9.3.16
Fuel Injection System	9.3.17
Intake Air System	9.3.18
Engine Management System (Spark and Fuel Control)	9.3.19
Accessory Drive Units	9.3.20
Exhaust Manifolds	9.3.21
Engine Flywheel and Guards	9.3.22
Lifting of Assembled Engines	9.3.23
Engine Mounts	9.3.24
Calibration	10
Stand/Engine Calibration	10.1
Procedure	10.1.1
Reporting of Reference Results	10.1.2
Analysis of Reference/Calibration Oils	10.1.3
Instrument Calibration	10.2
Engine Torque Measurement System	10.2.1
Fuel Flow Measurement System	10.2.2
Coolant Flow Measurement System	10.2.3
Thermocouple and Temperature Measurement System	10.2.4
Humidity Measurement System	10.2.5
Other Instrumentation	10.2.6
Test Procedure	11
Preparation for Initial Start-up of New Engine	11.1
External Oil System	11.1.1
Flush Effectiveness Demonstration	11.1.2
Preparation for Oil Charge	11.1.3
Oil Charge for Coolant Flush	11.1.4
Engine Coolant Charge for Coolant Flush	11.1.5
Initial Engine Start-up	11.2
Coolant Flush	11.3
New Engine Break-In	11.4
Oil Charge for Break-In	11.4.2
Break-In Operating Conditions	11.4.3
Routine Test Operation	11.5
Start-Up and Shutdown Procedures	11.5.8
Flying Flush Oil Exchange Procedures	11.5.9
Test Operating Stages	11.5.10
Stabilization to Stage Conditions	11.5.11
Stabilized BSFC Measurement Cycle	11.5.12
Data Logging	11.5.13
BC Oil Flush Procedure for BC Oil Before Test Oil	11.5.14
BSFC Measurement of BC Oil Before Test Oil	11.5.15
Test Oil Flush Procedure	11.5.16
Test Oil Aging	11.5.17
BSFC Measurement of Aged (Phase I) Test Oil	11.5.18
Aging Phase II	11.5.19
BSFC Measurement of Aged (Phase II) Test Oil	11.5.21
BC Oil Flush Procedure for BC Oil After Test Oil	11.5.22
BSFC Measurement for BC Oil After Test Oil	11.5.23
General Test Data Logging Forms	11.5.24
Diagnostic Review Procedures	11.5.25
Determination of Test Results	12
FEI1 and FEI2 Calculations	12.1
Final Test Report	13
Validity Statement	13.1
Report Format	13.2
Precision and Bias	14
Precision	14.1
Validity	14.2
Test Stand Calibration Status	14.2.1
Validity Interpretation of Deviant Operational Conditions	14.2.2
Bias	14.3
Keywords	15

Annexes
Role of ASTM TMC	Annex A1
Detailed Specifications and Drawings of Apparatus	Annex A2
Oil Heater Cerrobase Refill Procedure	Annex A3
Engine Part Number Listing	Annex A4
Flying Flush Checklists	Annex A5
Safety Precautions	Annex A6
Report Format	Annex A7
Statistical Equations for Mean and Standard Deviations	Annex A8
Oil Sump Full Level Determination Consumption Measurement Calibration Procedure	Annex A9
Fuel Injector Evaluation	Annex A10
Pre-test Maintenance Checklist	Annex A11
Blow-by Ventilation System Requirements	Annex A12
VIBSJ Abbreviated Length Test Requirements	Annex A13

Appendix
Procurement of Test Materials	Appendix X1

Committee	D 02
DocumentType	Test Method
Pages	61
PublisherName	American Society for Testing and Materials
Status	Current
Supersedes	ASTM D 6837 : 2010

ASTM D 7589 : 2016	Standard Test Method for Measurement of Effects of Automotive Engine Oils on Fuel Economy of Passenger Cars and Light-Duty Trucks in Sequence VID Spark Ignition Engine<rangeref></rangeref >
ASTM D 4485 : 2020	Standard Specification for Performance of Active API Service Category Engine Oils
ASTM D 8226 : 2021 : REV A	Standard Test Method for Measurement of Effects of Automotive Engine Oils on Fuel Economy of Passenger Cars and Light-Duty Trucks in Sequence VIF Spark Ignition Engine<rangeref></rangeref >
ASTM D 8114 : 2021 : REV A	Standard Test Method for Measurement of Effects of Automotive Engine Oils on Fuel Economy of Passenger Cars and Light-Duty Trucks in Sequence VIE Spark Ignition

ASTM D 4175 : 2020	Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
ASTM D 4175 : 2014	Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
ASTM D 4485 : 2003 : REV A	Standard Specification for Performance of Engine Oils
ASTM D 4175 : 2009 : REV A : EDT 1	Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
ASTM D 2699 : 2016	Standard Test Method for Research Octane Number of Spark-Ignition Engine Fuel
ASTM D 2699 : 2011	Standard Test Method for Research Octane Number of Spark-Ignition Engine Fuel
ASTM D 3338 : 1992	Standard Test Method for Estimation of Net Heat of Combustion of Aviation Fuels
ASTM D 4175 : 2008 : REV B : EDT 1	Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
ASTM D 4485 : 2006	Standard Specification for Performance of Engine Oils
ASTM D 4175 : 2005	Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
ASTM D 4485 : 2011 : REV C	Standard Specification for Performance of Active API Service Category Engine Oils
ASTM D 2699 : 1999	Standard Test Method for Research Octane Number of Spark-Ignition Engine Fuel
ASTM D 1319 : 1989	Standard Test Method for Hydrocarbon Types in Liquid Petroleum Products by Fluorescent Indicator Absorption
ASTM D 4175 : 2005 : EDT 2	Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
ASTM D 1319 : 2008	Standard Test Method for Hydrocarbon Types in Liquid Petroleum Products by Fluorescent Indicator Adsorption
ASTM D 6750 : 2017	Standard Test Methods for Evaluation of Engine Oils in a High-Speed, Single-Cylinder Diesel Engine—1K Procedure (0.4 % Fuel Sulfur) and 1N Procedure (0.04 % Fuel Sulfur)
ASTM D 2699 : 2004	Standard Test Method for Research Octane Number of Spark-Ignition Engine Fuel
ASTM D 4485 : 2001	Standard Specification for Performance of Engine Oils
ASTM D 2699 : 2007	Standard Test Method for Research Octane Number of Spark-Ignition Engine Fuel
ASTM D 3231 : 1999	Standard Test Method for Phosphorus in Gasoline
ASTM D 2699 : 2013 : REV A	Standard Test Method for Research Octane Number of Spark-Ignition Engine Fuel
ASTM D 4175 : 2015 : REV C	Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
ASTM D 3231 : 2013	Standard Test Method for Phosphorus in Gasoline
ASTM D 4175 : 2020 : REV B	Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
ASTM D 4175 : 2017 : REV A : EDT 1	Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
ASTM D 2699 : 2017	Standard Test Method for Research Octane Number of Spark-Ignition Engine Fuel
ASTM D 6750 : 2006	Standard Test Methods for Evaluation of Engine Oils in a High-Speed, Single-Cylinder Diesel Engine-1K Procedure (0.4 % Fuel Sulfur) and 1N Procedure (0.04 % Fuel Sulfur)
ASTM D 6750 : 2014	Standard Test Methods for Evaluation of Engine Oils in a High-Speed, Single-Cylinder Diesel Engine—1K Procedure(0.4 % Fuel Sulfur) and 1N Procedure(0.04 % Fuel Sulfur)
ASTM D 4485 : 2003	Standard Specification for Performance of Engine Oils
ASTM D 4485 : 2008	Standard Specification for Performance of Engine Oils
ASTM D 4485 : 2015	Standard Specification for Performance of Active API Service Category Engine Oils
ASTM D 1319 : 2018	Standard Test Method for Hydrocarbon Types in Liquid Petroleum Products by Fluorescent Indicator Adsorption
ASTM D 4485 : 2005 : REV A	Standard Specification for Performance of Engine Oils
ASTM D 4175 : 2008 : REV A	Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
ASTM D 4175 : 2020 : REV A	Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
ASTM D 4294 : 2010	Standard Test Method for Sulfur in Petroleum and Petroleum Products by Energy Dispersive X-ray Fluorescence Spectrometry
ASTM D 6750 : 2016	Standard Test Methods for Evaluation of Engine Oils in a High-Speed, Single-Cylinder Diesel Engine—1K Procedure (0.4 % Fuel Sulfur) and 1N Procedure (0.04 % Fuel Sulfur)
ASTM D 1319 : 2014	Standard Test Method for Hydrocarbon Types in Liquid Petroleum Products by Fluorescent Indicator Adsorption
ASTM D 4175 : 2017 : REV B	Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
ASTM D 4175 : 2009	Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
ASTM D 4485 : 2011 : REV A	Standard Specification for Performance of Active API Service Category Engine Oils
ASTM D 6557 : 2004	Standard Test Method for Evaluation of Rust Preventive Characteristics of Automotive Engine Oils
ASTM D 3338 : 2000	Standard Test Method for Estimation of Net Heat of Combustion of Aviation Fuels
ASTM E 29 : 2002	Standard Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications
ASTM D 3338 : 2004	Standard Test Method for Estimation of Net Heat of Combustion of Aviation Fuels
ASTM D 2699 : 1992	Standard Test Method for Knock Characteristics of Motor Fuels by the Research Method
ASTM D 240 : 1992 : R1997 : EDT 2	Standard Test Method for Heat of Combustion of Liquid Hydrocarbon Fuels by Bomb Calorimeter
ASTM D 6750 : 2019	Standard Test Methods for Evaluation of Engine Oils in a High-Speed, Single-Cylinder Diesel Engine—1K Procedure (0.4 % Fuel Sulfur) and 1N Procedure (0.04 % Fuel Sulfur)
ASTM D 3237 : 2006 : EDT 1	Standard Test Method for Lead in Gasoline by Atomic Absorption Spectroscopy
ASTM D 1319 : 1999	Standard Test Method for Hydrocarbon Types in Liquid Petroleum Products by Fluorescent Indicator Adsorption
ASTM D 4485 : 2018	Standard Specification for Performance of Active API Service Category Engine Oils
ASTM D 4175 : 2009 : REV A : EDT 4	Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
ASTM D 6557 : 2000	Standard Test Method for Evaluation of Rust Preventive Characteristics of Automotive Engine Oils
ASTM D 4175 : 2009 : REV A : EDT 3	Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
ASTM D 2699 : 2001 : REV A	Standard Test Method for Research Octane Number of Spark-Ignition Engine Fuel
ASTM D 235 : 2022	Standard Specification for Mineral Spirits (Petroleum Spirits) (Hydrocarbon Dry Cleaning Solvent)
ASTM D 2699 : 2003 : REV A	Standard Test Method for Research Octane Number of Spark-Ignition Engine Fuel
ASTM D 6750 : 2018	Standard Test Methods for Evaluation of Engine Oils in a High-Speed, Single-Cylinder Diesel Engine—1K Procedure (0.4 % Fuel Sulfur) and 1N Procedure (0.04 % Fuel Sulfur)
ASTM D 4485 : 2011 : REV B	Standard Specification for Performance of Active API Service Category Engine Oils
ASTM D 4485 : 2016	Standard Specification for Performance of Active API Service Category Engine Oils
ASTM D 4175 : 2018	Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
ASTM D 4485 : 2007	Standard Specification for Performance of Engine Oils
ASTM D 4485 : 2010	Standard Specification for Performance of Engine Oils
ASTM D 2699 : 2009	Standard Test Method for Research Octane Number of Spark-Ignition Engine Fuel
ASTM D 4485 : 2001 : REV A	Standard Specification for Performance of Engine Oils
ASTM D 4175 : 2001 : EDT 1	Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
ASTM D 4175 : 2020 : REV B : EDT 1	Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
ASTM D 1319 : 2002 : REV A	Standard Test Method for Hydrocarbon Types in Liquid Petroleum Products by Fluorescent Indicator Adsorption
ASTM D 6750 : 2005	Standard Test Methods for Evaluation of Engine Oils in a High-Speed, Single-Cylinder Diesel Engine-1K Procedure (0.4 % Fuel Sulfur) and 1N Procedure (0.04 % Fuel Sulfur)
ASTM D 4175 : 2001	Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
ASTM D 4175 : 2005 : EDT 1	Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
ASTM D 6557 : 2010 : REV A	Standard Test Method for Evaluation of Rust Preventive Characteristics of Automotive Engine Oils
ASTM D 2699 : 2012	Standard Test Method for Research Octane Number of Spark-Ignition Engine Fuel
ASTM D 3231 : 2018	Standard Test Method for Phosphorus in Gasoline
ASTM D 4175 : 2002	Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
ASTM D 3237 : 2002	Standard Test Method for Lead In Gasoline By Atomic Absorption Spectroscopy
ASTM D 6750 : 2013	Standard Test Methods for Evaluation of Engine Oils in a High-Speed, Single-Cylinder Diesel Engine—1K Procedure (0.4 % Fuel Sulfur) and 1N Procedure (0.04 % Fuel Sulfur)
ASTM D 4485 : 2004	Standard Specification for Performance of Engine Oils
ASTM D 2699 : 2016 : EDT 1	Standard Test Method for Research Octane Number of Spark-Ignition Engine Fuel
ASTM D 445 : 1988	Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and the Calculation of Dynamic Viscosity)
ASTM D 3231 : 2002	Standard Test Method for Phosphorus in Gasoline
ASTM D 4294 : 2008	Standard Test Method for Sulfur in Petroleum and Petroleum Products by Energy Dispersive X-ray Fluorescence Spectrometry
ASTM D 2699 : 2011 : EDT 1	Standard Test Method for Research Octane Number of Spark-Ignition Engine Fuel
ASTM D 4175 : 2015	Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
ASTM D 4485 : 2000	Standard Specification for Performance of Engine Oils
ASTM D 4175 : 2002 : REV A : EDT 2	Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
ASTM D 2699 : 2012 : REV A	Standard Test Method for Research Octane Number of Spark-Ignition Engine Fuel
ASTM D 2699 : 2008	Standard Test Method for Research Octane Number of Spark-Ignition Engine Fuel
ASTM D 1319 : 2003	Standard Test Method for Hydrocarbon Types in Liquid Petroleum Products by Fluorescent Indicator Adsorption
ASTM D 6557 : 2008	Standard Test Method for Evaluation of Rust Preventive Characteristics of Automotive Engine Oils
ASTM D 6750 : 2015 : REV A	Standard Test Methods for Evaluation of Engine Oils in a High-Speed, Single-Cylinder Diesel Engine—1K Procedure (0.4 % Fuel Sulfur) and 1N Procedure (0.04 % Fuel Sulfur)
ASTM D 4485 : 2015 : REV A	Standard Specification for Performance of Active API Service Category Engine Oils
ASTM D 6557 : 2013	Standard Test Method for Evaluation of Rust Preventive Characteristics of Automotive Engine Oils
ASTM D 2699 : 2019 : EDT 1	Standard Test Method for Research Octane Number of Spark-Ignition Engine Fuel
ASTM D 4294 : 2008 : REV A	Standard Test Method for Sulfur in Petroleum and Petroleum Products by Energy Dispersive X-ray Fluorescence Spectrometry
ASTM D 1319 : 2010	Standard Test Method for Hydrocarbon Types in Liquid Petroleum Products by Fluorescent Indicator Adsorption
ASTM D 4175 : 2009 : REV A : EDT 5	Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
ASTM D 4175 : 2016 : REV C	Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
ASTM D 4175 : 2015 : REV B	Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
ASTM D 2699 : 2003	Standard Test Method for Research Octane Number of Spark-Ignition Engine Fuel
ASTM D 6750 : 2010 : REV A	Standard Test Methods for Evaluation of Engine Oils in a High-Speed, Single-Cylinder Diesel Engine<span class='unicode'>—</span>1K Procedure (0.4 % Fuel Sulfur) and 1N Procedure (0.04 % Fuel Sulfur)
ASTM D 4294 : 2002	Standard Test Method for Sulfur in Petroleum Products by Energy-Dispersive X-Ray Fluorescence Spectroscopy
ASTM D 2699 : 2018 : REV A	Standard Test Method for Research Octane Number of Spark-Ignition Engine Fuel
ASTM D 4175 : 2015 : REV A	Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
ASTM D 4485 : 2006 : REV A	Standard Specification for Performance of Engine Oils
ASTM D 445 : 2019 : REV A	Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity)
ASTM D 4175 : 2009 : REV A	Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
ASTM D 4175 : 2016 : REV B	Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
ASTM D 4175 : 2002 : REV A : EDT 1	Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
ASTM D 4175 : 2008	Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
ASTM D 2699 : 2007 : REV A	Standard Test Method for Research Octane Number of Spark-Ignition Engine Fuel
ASTM D 4175 : 2002 : REV A	Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
ASTM D 4294 : 2016 : EDT 1	Standard Test Method for Sulfur in Petroleum and Petroleum Products by Energy Dispersive X-ray Fluorescence Spectrometry
ASTM D 4175 : 2000 : EDT 1	Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
ASTM D 4175 : 2016 : REV A	Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
ASTM D 3237 : 2006	Standard Test Method for Lead in Gasoline by Atomic Absorption Spectroscopy
ASTM D 4294 : 2008 : REV A : EDT 1	Standard Test Method for Sulfur in Petroleum and Petroleum Products by Energy Dispersive X-ray Fluorescence Spectrometry
ASTM D 4294 : 1998	Standard Test Method for Sulfur in Petroleum Products by Energy-Dispersive X-Ray Fluorescence Spectroscopy
ASTM D 2699 : 2004 : REV A	Standard Test Method for Research Octane Number of Spark-Ignition Engine Fuel
ASTM D 2699 : 2015	Standard Test Method for Research Octane Number of Spark-Ignition Engine Fuel
ASTM D 235 : 2002 : R2012	Standard Specification for Mineral Spirits (Petroleum Spirits) (Hydrocarbon Dry Cleaning Solvent) (Withdrawn 2021)
ASTM D 2699 : 2013 : REV B	Standard Test Method for Research Octane Number of Spark-Ignition Engine Fuel
ASTM D 4175 : 2019 : EDT 1	Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
ASTM D 4485 : 2018 : REV A	Standard Specification for Performance of Active API Service Category Engine Oils
ASTM D 4485 : 2005	Standard Specification for Performance of Engine Oils
ASTM D 4294 : 2021	Standard Test Method for Sulfur in Petroleum and Petroleum Products by Energy Dispersive X-ray Fluorescence Spectrometry
ASTM D 2699 : 2001	Standard Test Method for Research Octane Number of Spark-Ignition Engine Fuel
ASTM D 6750 : 2009	Standard Test Methods for Evaluation of Engine Oils in a High-Speed, Single-Cylinder Diesel Engine<span class='unicode'>—</span>1K Procedure (0.4 % Fuel Sulfur) and 1N Procedure (0.04 % Fuel Sulfur)
ASTM D 2699 : 2006	Standard Test Method for Research Octane Number of Spark-Ignition Engine Fuel
ASTM D 445 : 2001	Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (the Calculation of Dynamic Viscosity)
ASTM D 2699 : 2021	Standard Test Method for Research Octane Number of Spark-Ignition Engine Fuel
ASTM D 445 : 2021	Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity)
ASTM D 4485 : 2014	Standard Specification for Performance of Active API Service Category Engine Oils
ASTM D 2699 : 2015 : REV A	Standard Test Method for Research Octane Number of Spark-Ignition Engine Fuel
ASTM D 6557 : 2009	Standard Test Method for Evaluation of Rust Preventive Characteristics of Automotive Engine Oils
ASTM D 4485 : 2002	Standard Specification for Performance of Engine Oils
ASTM D 6557 : 2018	Standard Test Method for Evaluation of Rust Preventive Characteristics of Automotive Engine Oils
ASTM D 4175 : 2017 : REV A	Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
ASTM D 4485 : 2005 : EDT 1	Standard Specification for Performance of Engine Oils
ASTM D 6750 : 2015	Standard Test Methods for Evaluation of Engine Oils in a High-Speed, Single-Cylinder Diesel Engine—1K Procedure (0.4â€‰% Fuel Sulfur) and 1N Procedure (0.04â€‰% Fuel Sulfur)
ASTM D 2699 : 2002	Standard Test Method for Research Octane Number of Spark-Ignition Engine Fuel
ASTM D 4175 : 2009 : REV A : EDT 2	Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
ASTM D 4294 : 2003	Standard Test Method for Sulfur in Petroleum and Petroleum Products by Energy-Dispersive X-Ray Fluorescence Spectrometry
ASTM D 3231 : 2007	Standard Test Method for Phosphorus in Gasoline
ASTM D 3237 : 2017	Standard Test Method for Lead in Gasoline by Atomic Absorption Spectroscopy
ASTM D 4175 : 2018 : EDT 1	Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
ASTM D 4175 : 2016	Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
ASTM D 1319 : 2015	Standard Test Method for Hydrocarbon Types in Liquid Petroleum Products by Fluorescent Indicator Adsorption
ASTM D 4294 : 2016	Standard Test Method for Sulfur in Petroleum and Petroleum Products by Energy Dispersive X-ray Fluorescence Spectrometry
ASTM D 2699 : 2009 : EDT 1	Standard Test Method for Research Octane Number of Spark-Ignition Engine Fuel
ASTM D 2699 : 2004 : EDT 1	Standard Test Method for Research Octane Number of Spark-Ignition Engine Fuel
ASTM D 2699 : 2006 : REV A	Standard Test Method for Research Octane Number of Spark-Ignition Engine Fuel
ASTM D 3237 : 1997	Standard Test Method for Lead In Gasoline By Atomic Absorption Spectroscopy
ASTM D 1319 : 2013	Standard Test Method for Hydrocarbon Types in Liquid Petroleum Products by Fluorescent Indicator Adsorption
ASTM D 6750 : 2010 : REV B	Standard Test Methods for Evaluation of Engine Oils in a High-Speed, Single-Cylinder Diesel Engine<span class='unicode'>—</span>1K Procedure (0.4 % Fuel Sulfur) and 1N Procedure (0.04 % Fuel Sulfur)
ASTM D 6557 : 2003	Standard Test Method for Evaluation of Rust Preventive Characteristics of Automotive Engine Oils
ASTM D 3338 : 2005	Standard Test Method for Estimation of Net Heat of Combustion of Aviation Fuels
ASTM D 3231 : 1989	Standard Test Method for Phosphorus in Gasoline
ASTM D 445 : 2021 : EDT 1	Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity)
ASTM D 6750 : 2005 : REV A	Standard Test Methods for Evaluation of Engine Oils in a High-Speed, Single-Cylinder Diesel Engine-1K Procedure (0.4 % Fuel Sulfur) and 1N Procedure (0.04 % Fuel Sulfur)
ASTM D 6750 : 2008	Standard Test Methods for Evaluation of Engine Oils in a High-Speed, Single-Cylinder Diesel Engine<span class='unicode'>—</span>1K Procedure (0.4 % Fuel Sulfur) and 1N Procedure (0.04 % Fuel Sulfur)
ASTM D 2699 : 2018	Standard Test Method for Research Octane Number of Spark-Ignition Engine Fuel
ASTM D 4175 : 2017	Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
ASTM D 6557 : 2010	Standard Test Method for Evaluation of Rust Preventive Characteristics of Automotive Engine Oils
ASTM D 4175 : 2019	Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
ASTM D 3338 : 2008	Standard Test Method for Estimation of Net Heat of Combustion of Aviation Fuels
ASTM D 3338 : 1995	Standard Test Method for Estimation of Net Heat of Combustion of Aviation Fuels
ASTM D 2699 : 2013	Standard Test Method for Research Octane Number of Spark-Ignition Engine Fuel
ASTM D 4485 : 2009	Standard Specification for Performance of Engine Oils
ASTM D 4485 : 2019	Standard Specification for Performance of Active API Service Category Engine Oils
ASTM D 6750 : 2010	Standard Test Methods for Evaluation of Engine Oils in a High-Speed, Single-Cylinder Diesel Engine<span class='unicode'>—</span>1K Procedure (0.4 % Fuel Sulfur) and 1N Procedure (0.04 % Fuel Sulfur)
ASTM D 6750 : 2002	Standard Test Methods for Evaluation of Engine Oils in A High-Speed, Single-Cylinder Diesel Engine -1K Procedure (0.4 % Fuel Sulfur) and 1N Procedure (0.04 % Fuel Sulfur)
ASTM D 4175 : 2015 : REV B : EDT 1	Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
ASTM D 6750 : 2004	Standard Test Methods for Evaluation of Engine Oils in A High-Speed, Single-Cylinder Diesel Engine -1K Procedure (0.4 % Fuel Sulfur) and 1N Procedure (0.04 % Fuel Sulfur)
ASTM D 4485 : 2010 : REV A	Standard Specification for Performance of Engine Oils
ASTM D 4485 : 2011	Standard Specification for Performance of Engine Oils
ASTM D 2699 : 2010	Standard Test Method for Research Octane Number of Spark-Ignition Engine Fuel
ASTM D 3231 : 2011	Standard Test Method for Phosphorus in Gasoline
ASTM D 3237 : 2012	Standard Test Method for Lead in Gasoline by Atomic Absorption Spectroscopy
ASTM D 1319 : 2019	Standard Test Method for Hydrocarbon Types in Liquid Petroleum Products by Fluorescent Indicator Adsorption
ASTM D 2699 : 2019	Standard Test Method for Research Octane Number of Spark-Ignition Engine Fuel
ASTM D 4294 : 1990 : R1998 : EDT 1	Standard Test Method for Sulfur in Petroleum Products by Energy-Dispersive X-Ray Fluorescence Spectroscopy
ASTM D 1319 : 2002	Standard Test Method for Hydrocarbon Types in Liquid Petroleum Products by Fluorescent Indicator Adsorption
ASTM D 4175 : 2008 : REV B	Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
ASTM D 4485 : 2007 : REV A	Standard Specification for Performance of Engine Oils