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ASTM D 7511 : 2012 : R2017 : EDT 1

Current
Current

The latest, up-to-date edition.

Standard Test Method for Total Cyanide by Segmented Flow Injection Analysis, In-Line Ultraviolet Digestion and Amperometric Detection
Available format(s)

Hardcopy , PDF

Language(s)

English

Published date

01-07-2017

CONTAINED IN VOL. 11.02, 2017 Specifies total cyanide in drinking and surface waters, as well as domestic and industrial wastes.

1.1This test method is used for determining total cyanide in drinking and surface waters, as well as domestic and industrial wastes. Cyanide ion (CN), hydrogen cyanide in water (HCN(aq)), and the cyano-complexes of zinc, copper, cadmium, mercury, nickel, silver, and iron may be determined by this test method. Cyanide ions from Au(I), Co(III), Pd(II), and Ru(II) complexes are only partially determined.

1.2The method detection limit (MDL) is 1.0 μg/L cyanide and the minimum level (ML) is 3 μg/L. The applicable range of the method is 3 to 500 μg/L cyanide using a 200-μL sample loop. Extend the range to analyze higher concentrations by sample dilution or changing the sample loop volume.

1.3This test method can be used by analysts experienced with equipment using segmented flow analysis (SFA) and flow injection analysis (FIA) or working under the close supervision of such qualified persons.

1.4The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.5This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific hazard statements are given in 8.5 and Section 9.

1.6This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

Committee
D 19
DocumentType
Test Method
Pages
10
ProductNote
Reconfirmed EDT 1
PublisherName
American Society for Testing and Materials
Status
Current
Supersedes

ASTM D 7572 : 2015 Standard Guide for Recovery of Aqueous Cyanides by Extraction from Mine Rock and Soil
ASTM D 7365 : 2009 : REV A : R2015 Standard Practice for Sampling, Preservation and Mitigating Interferences in Water Samples for Analysis of Cyanide
ASTM D 7728 : 2018 Standard Guide for Selection of ASTM Analytical Methods for Implementation of International Cyanide Management Code Guidance

ASTM D 7365 : 2007 Standard Practice for Sampling, Preservation and Mitigating Interferences in Water Samples for Analysis of Cyanide
ASTM D 3370 : 1995 : REV A : R2003 : EDT 1 Standard Practices for Sampling Water from Closed Conduits
ASTM D 1129 : 2013 : REDLINE Standard Terminology Relating to Water
ASTM D 1129 : 2003 Standard Terminology Relating to Water
ASTM D 2777 : 2013 : REDLINE Standard Practice for Determination of Precision and Bias of Applicable Test Methods of Committee D19 on Water
ASTM D 7365 : 2009 Standard Practice for Sampling, Preservation and Mitigating Interferences in Water Samples for Analysis of Cyanide
ASTM D 1129 : 2013 Standard Terminology Relating to Water
ASTM D 1129 : 2013 : R2020 Standard Terminology Relating to Water
ASTM D 2036 : 1991 Standard Test Methods for Cyanides in Water
ASTM D 5847 : 1999 : REV A : EDT 1 Standard Practice for Writing Quality Control Specifications for Standard Test Methods for Water Analysis
ASTM D 6696 : 2016 : REDLINE Standard Guide for Understanding Cyanide Species
ASTM D 2777 : 2012 Standard Practice for Determination of Precision and Bias of Applicable Test Methods of Committee D19 on Water
ASTM D 1129 : 2013 : R2020 : EDT 2 Standard Terminology Relating to Water
ASTM D 6696 : 2016 Standard Guide for Understanding Cyanide Species
ASTM D 1193 : 1977 : R1983 : EDT 1 Standard Specification for Reagent Water
ASTM D 5847 : 2002 : R2007 Standard Practice for Writing Quality Control Specifications for Standard Test Methods for Water Analysis
ASTM D 2036 : 2009 : R2022 Standard Test Methods for Cyanides in Water
ASTM D 6696 : 2010 Standard Guide for Understanding Cyanide Species
ASTM D 1129 : 2006 Standard Terminology Relating to Water
ASTM D 6696 : 2014 Standard Guide for Understanding Cyanide Species
ASTM D 2777 : 2003 Standard Practice for Determination of Precision and Bias of Applicable Methods of Committee D-19 on Water
ASTM D 2777 : 2021 Standard Practice for Determination of Precision and Bias of Applicable Test Methods of Committee D19 on Water
ASTM D 3370 : 2010 Standard Practices for Sampling Water from Closed Conduits
ASTM D 2777 : 2013 Standard Practice for Determination of Precision and Bias of Applicable Test Methods of Committee D19 on Water
ASTM D 7365 : 2009 : REV A Standard Practice for Sampling, Preservation and Mitigating Interferences in Water Samples for Analysis of Cyanide
ASTM D 6696 : 2005 : EDT 1 Standard Guide for Understanding Cyanide Species
ASTM D 5847 : 2002 : R2012 Standard Practice for Writing Quality Control Specifications for Standard Test Methods for Water Analysis
ASTM D 2777 : 1998 Standard Practice for Determination of Precision and Bias of Applicable Methods of Committee D-19 on Water
ASTM D 1129 : 2013 : R2020 : EDT 1 Standard Terminology Relating to Water
ASTM D 2036 : 2009 : R2015 Standard Test Methods for Cyanides in Water
ASTM D 3370 : 2008 Standard Practices for Sampling Water from Closed Conduits
ASTM D 1129 : 1999 : REV A Standard Terminology Relating to Water
ASTM D 2036 : 1998 Standard Test Methods for Cyanides in Water
ASTM D 3856 : 2011 Standard Guide for Management Systems in Laboratories Engaged in Analysis of Water
ASTM D 1129 : 2006 : REV A Standard Terminology Relating to Water
ASTM D 1193 : 2006 : R2011 Standard Specification for Reagent Water
ASTM D 5847 : 2002 : R2020 Standard Practice for Writing Quality Control Specifications for Standard Test Methods for Water Analysis
ASTM D 1129 : 2003 : REV A Standard Terminology Relating to Water
ASTM D 1129 : 2002 Standard Terminology Relating to Water
ASTM D 6696 : 2005 Standard Guide for Understanding Cyanide Species
ASTM D 2036 : 2009 Standard Test Methods for Cyanides in Water
ASTM D 6696 : 2016 : R2023 Standard Guide for Understanding Cyanide Species
ASTM D 1193 : 1991 Standard Specification for Reagent Water
ASTM D 3856 : 1995 : R2006 Standard Guide for Good Laboratory Practices in Laboratories Engaged in Sampling and Analysis of Water
ASTM D 1129 : 2004 Standard Terminology Relating to Water
ASTM D 5847 : 2022 Standard Practice for Writing Quality Control Specifications for Standard Test Methods for Water Analysis
ASTM D 2777 : 2008 Standard Practice for Determination of Precision and Bias of Applicable Test Methods of Committee D19 on Water
ASTM D 3856 : 2011 : R2015 Standard Guide for Management Systems in Laboratories Engaged in Analysis of Water (Withdrawn 2024)
ASTM D 2777 : 2006 Standard Practice for Determination of Precision and Bias of Applicable Test Methods of Committee D19 on Water
ASTM D 3856 : 1995 : R2000 Standard Guide for Good Laboratory Practices in Laboratories Engaged in Sampling and Analysis of Water
ASTM D 3370 : 2018 Standard Practices for Sampling Water from Flowing Process Streams
ASTM D 6696 : 2001 Standard Guide for Understanding Cyanide Species
ASTM D 1129 : 2002 : REV A Standard Terminology Relating to Water
ASTM D 5847 : 2002 Standard Practice for Writing Quality Control Specifications for Standard Test Methods for Water Analysis
ASTM D 3370 : 1976 Standard Practices for Sampling Water
ASTM D 7365 : 2009 : REV A : R2015 Standard Practice for Sampling, Preservation and Mitigating Interferences in Water Samples for Analysis of Cyanide
ASTM D 1193 : 1970 Standard Specification For Reagent Water
ASTM D 1193 : 2006 Standard Specification for Reagent Water
ASTM D 3370 : 1995 : REV A : R1999 : EDT 1 Standard Practices for Sampling Water from Closed Conduits
ASTM D 1193 : 1999 Standard Specification for Reagent Water
ASTM D 1129 : 2010 Standard Terminology Relating to Water
ASTM D 4210 : 1989 : R1996 : EDT 1 Standard Practice for Intralaboratory Quality Control Procedures and a Discussion on Reporting Low-Level Data (Withdrawn 2002)
ASTM D 3370 : 2007 Standard Practices for Sampling Water from Closed Conduits
ASTM D 2036 : 2006 Standard Test Methods for Cyanides in Water
ASTM D 1129 : 2006 : REV A : EDT 1 Standard Terminology Relating to Water
ASTM D 1129 : 2001 Standard Terminology Relating to Water
ASTM D 1129 : 2004 : EDT 1 Standard Terminology Relating to Water
ASTM D 1193 : 2006 : R2018 Standard Specification for Reagent Water
ASTM D 2777 : 2008 : EDT 1 Standard Practice for Determination of Precision and Bias of Applicable Test Methods of Committee D19 on Water
ASTM D 7365 : 2009 : REV A : R2022 Standard Practice for Sampling, Preservation and Mitigating Interferences in Water Samples for Analysis of Cyanide

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