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ASTM E 1899 : 2016

Superseded
Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

View Superseded by
superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

Standard Test Method for Hydroxyl Groups Using Reaction with p-Toluenesulfonyl Isocyanate (TSI) and Potentiometric Titration with Tetrabutylammonium Hydroxide
Available format(s)

Hardcopy , PDF

Superseded date

17-06-2023

Language(s)

English

Published date

22-02-2019

This test method covers the determination of hydroxyl groups attached to primary and secondary carbon atoms in aliphatic and cyclic compounds and phenols

1.1This test method covers the determination of hydroxyl groups attached to primary and secondary carbon atoms in aliphatic and cyclic compounds and phenols. It is not suitable for determination of hydroxyl groups attached to tertiary carbon atoms. This test method is applicable to polyacetals, temperature sensitive materials, high solids polymer polyols, and rigid polyols. Other available test methods listed in Note 1 are not suitable for many of the sample types listed above.

1.1.1This test method is currently recommended for neutral refined products. Successful application has been made, however, to some in-process samples that contain an excess of acidic species. Proper validation must be performed, of course, to show that the acidic species either does not interfere, or that the acidic species interference has been obviated.

Note 1:Other methods for determination of hydroxyl groups are given in Test Methods D817, D871, D1957, D2195, D4252, D4273, D4274, E222, E326, and E335.

1.2Review the current appropriate Safety Data Sheets (SDS) for detailed information concerning toxicity, first aid procedures, and safety precautions.

1.3The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.4This standard does not purport to address all of the safety concerns, if any, associated, with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific hazards see Section 9.

Committee
D 16
DocumentType
Test Method
Pages
5
PublisherName
American Society for Testing and Materials
Status
Superseded
SupersededBy
Supersedes

ASTM D 6342 : 2022 Standard Practice for Polyurethane Raw Materials: Determining Hydroxyl Number of Polyols by Near Infrared (NIR) Spectroscopy
ASTM E 1547 : 2009 : R2023 Standard Terminology Relating to Industrial and Specialty Chemicals
ASTM E 1547 : 2009 : R2017 Standard Terminology Relating to Industrial and Specialty Chemicals
ASTM D 6342 : 2012 : R2017 : EDT 1 Standard Practice for Polyurethane Raw Materials: Determining Hydroxyl Number of Polyols by Near Infrared (NIR) Spectroscopy

ASTM D 4252 : 1989 : R2009 Standard Test Methods for Chemical Analysis of Alcohol Ethoxylates and Alkylphenol Ethoxylates
ASTM D 2195 : 2000 Standard Test Methods for Pentaerythritol
ASTM D 4274 : 2005 Standard Test Methods for Testing Polyurethane Raw Materials: Determination of Hydroxyl Numbers of Polyols
ASTM D 4274 : 2011 Standard Test Methods for Testing Polyurethane Raw Materials: Determination of Hydroxyl Numbers of Polyols
ASTM E 222 : 2017 Standard Test Methods for Hydroxyl Groups Using Acetic Anhydride Acetylation
ASTM D 4273 : 2023 Standard Test Method for Polyurethane Raw Materials: Determination of Primary Hydroxyl Content of Polyether Polyols
ASTM E 222 : 2023 Standard Test Methods for Hydroxyl Groups Using Acetic Anhydride Acetylation
ASTM D 2195 : 2005 Standard Test Methods for Pentaerythritol (Withdrawn 2011)
ASTM D 1957 : 1986 : R1995 : EDT 1 Standard Test Method for Hydroxyl Value of Fatty Oils and Acids
ASTM D 1193 : 1977 : R1983 : EDT 1 Standard Specification for Reagent Water
ASTM D 1193 : 2006 : R2011 Standard Specification for Reagent Water
ASTM E 300 : 2003 : R2022 Standard Practice for Sampling Industrial Chemicals
ASTM D 4273 : 2011 Standard Test Method for Polyurethane Raw Materials: Determination of Primary Hydroxyl Content of Polyether Polyols
ASTM D 4252 : 1989 : R2017 Standard Test Methods for Chemical Analysis of Alcohol Ethoxylates and Alkylphenol Ethoxylates
ASTM D 1193 : 1991 Standard Specification for Reagent Water
ASTM D 1957 : 1986 : R2001 Standard Test Method for Hydroxyl Value of Fatty Oils and Acids (Withdrawn 2007)
ASTM D 4252 : 1989 : R2003 Standard Test Methods for Chemical Analysis of Alcohol Ethoxylates and Alkylphenol Ethoxylates
ASTM D 4252 : 1989 : R1995 : EDT 1 Standard Test Methods for Chemical Analysis of Alcohol Ethoxylates and Alkylphenol Ethoxylates
ASTM D 4273 : 2018 Standard Test Method for Polyurethane Raw Materials: Determination of Primary Hydroxyl Content of Polyether Polyols
ASTM D 4273 : 1999 Standard Test Methods for Polyurethane Raw Materials Determination of Primary Hydroxyl Content of Polyether Polyols
ASTM D 4273 : 2005 Standard Test Methods for Polyurethane Raw Materials Determination of Primary Hydroxyl Content of Polyether Polyols
ASTM E 326 : 1996 Test Method for Hydroxyl Groups by Phthalic Anhydride Esterification (Withdrawn 2001)
ASTM E 300 : 2003 : R2017 Standard Practice for Sampling Industrial Chemicals
ASTM D 1193 : 1970 Standard Specification For Reagent Water
ASTM D 4274 : 2016 Standard Test Methods for Testing Polyurethane Raw Materials: Determination of Hydroxyl Numbers of Polyols
ASTM D 1193 : 2006 Standard Specification for Reagent Water
ASTM D 1193 : 1999 Standard Specification for Reagent Water
ASTM D 1193 : 2006 : R2018 Standard Specification for Reagent Water
ASTM D 4274 : 2021 Standard Test Methods for Testing Polyurethane Raw Materials: Determination of Hydroxyl Numbers of Polyols
ASTM D 4274 : 1999 Standard Test Methods for Testing Polyurethane Raw Materials Determination of Hydroxyl Numbers of Polyols
ASTM E 335 : 1996 Standard Test Method for Hydroxyl Groups by Pyromellitic Dianhydride Esterification (Withdrawn 2003)
ASTM D 4274 : 2023 Standard Test Methods for Testing Polyurethane Raw Materials: Determination of Hydroxyl Numbers of Polyols

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