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ASTM E 2787 : 2011 : R2016

Superseded
Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

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superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

Standard Test Method for Determination of Thiodiglycol in Soil Using Pressurized Fluid Extraction Followed by Single Reaction Monitoring Liquid Chromatography/Tandem Mass Spectrometry (LC/MS/MS)
Available format(s)

Hardcopy , PDF

Superseded date

14-05-2021

Language(s)

English

Published date

25-09-2017

CONTAINED IN VOL. 15.08, 2017 Defines the determination of thiodiglycol (TDG) in soil using pressurized fluid extraction (PFE). A commercially available PFE system was used, followed by analysis using liquid chromatography (LC), and detected with tandem mass spectrometry (MS/MS).

1.1This procedure covers the determination of thiodiglycol (TDG) in soil using pressurized fluid extraction (PFE). A commercially available PFE system2 was used, followed by analysis using liquid chromatography (LC), and detected with tandem mass spectrometry (MS/MS). TDG is qualitatively and quantitatively determined by this method. This method adheres to single reaction monitoring (SRM) mass spectrometry.

1.2The Method Detection Limit (MDL) and Reporting Range for TDG are listed in Table 1.

1.2.1The MDL is determined following the Code of Federal Regulations, 40 CFR Part 136, Appendix B.

1.2.2The reporting limit (RL) is calculated from the concentration of the Level 1 calibration standard as shown in Table 4. The RL for this method is 200 ppb. Reporting range concentrations are calculated from Table 4 concentrations assuming a 5 μL injection of the lowest level calibration standard, 5 g sample, and a 2 mL final extract volume.

1.3Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.4This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Committee
D 34
DocumentType
Test Method
Pages
9
ProductNote
Reconfirmed 2016
PublisherName
American Society for Testing and Materials
Status
Superseded
SupersededBy
Supersedes

CFR 40(PTS100-149) : JUL 94 PROTECTION OF ENVIRONMENT - ENVIRONMENTAL PROTECTION AGENCY
ASTM D 653 : 2007 Standard Terminology Relating to Soil, Rock, and Contained Fluids
ASTM D 3740 : 2012-06 PRACTICE FOR MINIMUM REQUIREMENTS FOR AGENCIES ENGAGED IN TESTING AND/OR INSPECTION OF SOIL AND ROCK AS USED IN ENGINEERING DESIGN AND CONSTRUCTION
ASTM D 653 : 2020 : EDT 1 Standard Terminology Relating to Soil, Rock, and Contained Fluids
ASTM D 653 : 2021 Standard Terminology Relating to Soil, Rock, and Contained Fluids
ASTM E 2554 : 2013-05 PRACTICE FOR ESTIMATING AND MONITORING THE UNCERTAINTY OF TEST RESULTS OF A TEST METHOD USING CONTROL CHART TECHNIQUES
ASTM D 653 : 2014 : REDLINE Standard Terminology Relating to Soil, Rock, and Contained Fluids

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