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BS 3406-5:1983

Superseded
Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

View Superseded by
superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

Methods for determination of particle size distribution Recommendations for electrical sensing zone method (the Coulter principle)
Available format(s)

Hardcopy , PDF

Superseded date

15-06-2000

Language(s)

English

Published date

30-09-1983

Foreword
Cooperating organizations
Recommendations
0. Introduction
1. Scope
2. Definitions
3. Symbols and abbreviations
4. Health and safety
5. Principle
5.1 General operation
5.2 Response theory
5.3 Effect of particle shape and orientation
5.4 Effect of coincident particle passage
5.5 Pulse shape
5.6 Size limits
6. Operational procedures
6.1 Instrument location
6.2 Choice of electrolyte solution
6.3 Electrolyte solution preparation
6.4 Sample preparation and dispersion
6.5 Choice of orifice(s) and monometer setting(s)
6.6 Stability of dispersion
6.7 Clearing an orifice blockage
6.8 Analytical procedure
6.9 Background counts
6.10 Calibration
6.11 Multiple orifice method for wide size range samples
6.12 Calculation of results
6.13 Extrapolation
6.14 Determination of mass percentage detected
7. Reporting of results
Appendices
A. Comparison with other methods
B. List of suitable elecrolyte solutions
C. Instrument checks
D. Measurement of the immersed density of particles
    of powder when dispersed in electrolyte solution
E. Example of calibration by mass integration
F. Example of determination of percentage mass
    analysed
G. Large orifice technique (orifice diameter >560 mu m)
H. Bibliography
Tables
1. Background counts
2. Suggested manometer settings
3. Stability of suspension
4. Typical coincidence correction chart
5. Recommended number of counts
6. Suitable orifice diameter combinations
7. Data sheet: normal calculation
8. Data sheet: worked example without corrections
9. Data sheet: large orifice analysis
10. Data sheet: small orifice analysis
11. Worked example (for a 2-orifice analysis)
12. Recommended electrolyte solutions
13. Density of pure water, pw
14. Data for calibration by mass integration
Figures
1. Schematic drawing of a simple form of analyser
2. Pulses
3. Current density at orifice
4. Pulses resulting from axial and non-axial passage
     of particles
5. 2-orifice overlap
6. Example of constant vacuum supply

Gives recommendations on a specific method, the electrical sensing zone method, for the determination of the particle size of powders, and facilitates comparison between size analyses made in different laboratories.

Committee
LBI/37
DevelopmentNote
Supersedes 92/78236 DC. (10/2007)
DocumentType
Standard
Pages
44
PublisherName
British Standards Institution
Status
Superseded
SupersededBy
Supersedes

ISO 9934-2:2015 Non-destructive testing — Magnetic particle testing — Part 2: Detection media
DEFSTAN 13-163/1(1995) : 1995 BX 4
BS 3406-7:1988 Methods for determination of particle size distribution Recommendations for single particle light interaction methods
I.S. EN ISO 9934-2:2015 NON-DESTRUCTIVE TESTING - MAGNETIC PARTICLE TESTING - PART 2: DETECTION MEDIA (ISO 9934-2:2015)
BS 3406-4:1993 Methods for determination of particle size distribution Guide to microscope and image analysis methods
13/30281192 DC : 0 BS EN ISO 9934-2 - NON-DESTRUCTIVE TESTING - MAGNETIC PARTICLE TESTING - PART 2: DETECTION MEDIA
15/30284298 DC : 0 BS ISO 12103-1 - ROAD VEHICLES - TEST CONTAMINANTS FOR FILTER EVALUATION - PART 1: ARIZONA TEST DUST
BS ISO 12103-1:2016 Road vehicles. Test contaminants for filter evaluation Arizona test dust
ISO 12103-1:2016 Road vehicles — Test contaminants for filter evaluation — Part 1: Arizona test dust
DIN EN ISO 9934-2:2015-12 NON-DESTRUCTIVE TESTING - MAGNETIC PARTICLE TESTING - PART 2: DETECTION MEDIA (ISO 9934-2:2015)
BS ISO 12103-2:1997 Road vehicles. Test dust for filter evaluation Aluminium oxide test dust
UNE-EN ISO 9934-2:2016 Non-destructive testing - Magnetic particle testing - Part 2: Detection media (ISO 9934-2:2015)
BS EN ISO 9934-2:2015 Non-destructive testing. Magnetic particle testing Detection media
EN ISO 9934-2:2015 Non-destructive testing - Magnetic particle testing - Part 2: Detection media (ISO 9934-2:2015)

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$478.43
Including GST where applicable

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