Foodstuffs. Vegetable oils and foodstuff on basis of vegetable oils. Determination of mineral oil saturated hydrocarbons (MOSH) and mineral oil aromatic hydrocarbons (MOAH) with on-line HPLC-GC-FID analysis

Available format(s)

Hardcopy , PDF

Language(s)

English

Published date

13-07-2017

Publisher

British Standards Institution

European foreword
1 Scope
2 Normative references
3 Terms and definitions
4 Principle
5 Reagents
6 Apparatus
7 Sample storage
8 Preparation of the test sample
9 Preparation of the analytical sample
10 Liquid chromatography and gas chromatography
11 Precision
12 Test report
Annex A (informative) - Examples of chromatograms
Annex B (informative) - Precision data
Bibliography

Defines a highly efficient method for the determination of saturated and aromatic hydrocarbons (from C10 to C50) in vegetable fats and oils and foodstuff on basis of vegetable oils for which it has been interlaboratory validated, with online-HPLC-GC-FID.

This European Standard specifies a highly efficient method for the determination of saturated and aromatic hydrocarbons (from C10 to C50) in vegetable fats and oils and foodstuff on basis of vegetable oils for which it has been interlaboratory validated, with online-HPLC-GC-FID [1], [2] and [3]. This standard is not intended to be applied to other matrices. The method can be used for the analysis of mineral oil saturated hydrocarbons (MOSH) and/or mineral oil aromatic hydrocarbons (MOAH). The method has been tested in an interlaboratory study via the analysis of both naturally contaminated and spiked vegetable oil samples and mayonnaise and margarine samples, ranging from 4 mg/kg to 197 mg/kg for MOSH, and from 2 mg/kg to 51 mg/kg for MOAH. According to the results of the interlaboratory studies, the method has been proven suitable for MOSH- and MOAH mass concentrations each above 10 mg/kg. In case of suspected interferences from natural sources, the mineral origin of the MOSH and MOAH fraction can be verified by examination of the pattern by GC-MS.

Committee	AW/275
DevelopmentNote	Supersedes 16/30272448 DC. (07/2017)
DocumentType	Standard
Pages	40
PublisherName	British Standards Institution
Status	Current
Supersedes	16/30272448 DC : DRAFT APR 2016

Standards	Relationship
EN 16995:2017	Identical

ISO 5555:2001	Animal and vegetable fats and oils — Sampling
EN ISO 661:2005/AC:2006	ANIMAL AND VEGETABLE FATS AND OILS - PREPARATION OF TEST SAMPLE
ISO 5725-2:1994	Accuracy (trueness and precision) of measurement methods and results Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method
ISO 661:2003	Animal and vegetable fats and oils Preparation of test sample

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BS EN 16995:2017

Current

Table of Contents

Abstract

Scope

General Product Information

International Equivalents

Standards Referencing This Book

Category

Subcategory

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