Water quality. Determination of selected polybrominated diphenyl ethers in sediment and sewage sludge. Method using extraction and gas chromatography/mass spectrometry

Available format(s)

Hardcopy , PDF

Language(s)

English

Published date

30-06-2009

Publisher

British Standards Institution

Introduction
1 Scope
2 Normative references
3 Principle
4 Interferences
5 Reagents and standards
6 Apparatus
7 Sampling and sample pre-treatment
8 Procedure
9 Calibration
10 Test report
Annex A (informative) - Clean-up procedures
Annex B (informative) - Examples for separation conditions
in gas chromatography and mass spectrometry
Annex C (informative) - Typical ions and time windows for
electron impact ionization detection
Annex D (informative) - Examples of chromatograms and spectra
Annex E (informative) - Precision data
Bibliography

Defines a method for the determination of selected polybrominated diphenyl ethers (PBDE) in sediment and sludge using gas chromatography/mass spectrometry (GC-MS) in the electron impact (EI) or negative ion chemical ionization (NCI) mode.

Committee	EH/3/2
DevelopmentNote	Also numbered as BS 6068-2.99(2006). Renumbers and supersedes BS ISO 22032. 2009 version incorporates corrigendum to BS ISO 22032. Supersedes 04/30091620 DC. (06/2009)
DocumentType	Standard
Pages	36
PublisherName	British Standards Institution
Status	Current
Supersedes	BS ISO 22032 : 2006 04/30091620 DC : DRAFT NOV 2004

Standards	Relationship
ISO 22032:2006	Identical
EN ISO 22032:2009	Identical

ISO 5667-13:2011	Water quality Sampling Part 13: Guidance on sampling of sludges
ISO/TR 13530:1997	Water quality Guide to analytical quality control for water analysis
EN 12880:2000	Characterization of sludges - Determination of dry residue and water content
DIN 32645:2008-11	CHEMICAL ANALYSIS - DECISION LIMIT, DETECTION LIMIT AND DETERMINATION LIMIT UNDER REPEATABILITY CONDITIONS - TERMS, METHODS, EVALUATION
ISO 3696:1987	Water for analytical laboratory use — Specification and test methods
ISO 8466-1:1990	Water quality Calibration and evaluation of analytical methods and estimation of performance characteristics Part 1: Statistical evaluation of the linear calibration function

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BS EN ISO 22032:2009

Water quality. Determination of selected polybrominated diphenyl ethers in sediment and sewage sludge. Method using extraction and gas chromatography/mass spectrometry

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Abstract

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