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BS EN ISO 4259:2006

Superseded
Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

View Superseded by
superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

Petroleum products. Determination and application of precision data in relation to methods of test
Available format(s)

Hardcopy , PDF

Superseded date

31-01-2018

Language(s)

English

Published date

31-01-2007

Foreword
Introduction
1 Scope
2 Normative references
3 Terms and definitions
4 Stages in the planning of an inter-laboratory test
   programme for the determination of the precision of
   a test method
   4.1 General
   4.2 Preparing a draft method of test
   4.3 Planning a pilot programme with at least two
       laboratories
   4.4 Planning the inter-laboratory programme
   4.5 Executing the inter-laboratory programme
5 Inspection of inter-laboratory results for uniformity
   and for outliers
   5.1 General
   5.2 Transformation of data
   5.3 Tests for outliers
   5.4 Rejection of complete data from a sample
   5.5 Estimating missing or rejected values
   5.6 Rejection test for outlying laboratories
   5.7 Confirmation of selected transformation
6 Analysis of variance, calculation and expression of
   precision estimates
   6.1 General
   6.2 Analysis of variance
   6.3 Expectation of mean squares and calculation of
       precision estimates
   6.4 Expression of precision estimates of a method of test
7 Significance of repeatability (r) and reproducibility (R)
   7.1 General
   7.2 Repeatability, r
   7.3 Reproducibility, R
8 Specifications
   8.1 Aim of specifications
   8.2 Construction of specifications limits in relation
       to precision
9 Quality control against specifications
   9.1 General
   9.2 Testing margin at the supplier
   9.3 Testing margin at the recipient
10 Dispute procedure
Annex A (normative) Determination of number of samples
                      required
Annex B (informative) Derivation of equation for calculating
                      the number of samples required
Annex C (normative) Notation and tests
Annex D (normative) Example results of test for determination
                      of bromine number and statistical tables
Annex E (normative) Types of dependence and corresponding
                      transformations
Annex F (normative) Weighted linear regression analysis
Annex G (normative) Rules for rounding off results
Annex H (informative) Explanation of equations given in Clause 7
Annex I (informative) Specifications that relate to a specified
                      degree of criticality
Bibliography

Describes calculation of precision estimates and application to specifications, also contains definitions of relevant statistical terms, procedures for adoption in planning of an inter-laboratory test programme for determination of precision of a test method, calculation method for precision for results of programme and procedure for interpreting laboratory results relating to precision of methods and to limits laid down by specifications.

Committee
PTI/13
DevelopmentNote
Also numbered as BS 2000-367(2006). Supersedes 04/30112885 DC (02/2007)
DocumentType
Standard
Pages
74
PublisherName
British Standards Institution
Status
Superseded
SupersededBy
Supersedes

10/30218583 DC : 0 BS 2869 - FUEL OILS FOR AGRICULTURAL, DOMESTIC AND INDUSTRIAL ENGINES AND BOILERS - SPECIFICATION
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BS MA 100:1996 Specification for petroleum fuels for marine oil engines and boilers
DEFSTAN 91-56/2(1997) : 1997 GREASE, SILICONE, METAL TO RUBBER - NATO CODE: G-394 - JOINT SERVICE DESIGNATION: XG-315
14/30283904 DC : 0 BS 4250 - SPECIFICATION FOR COMMERCIAL BUTANE AND COMMERCIAL PROPANE
DEFSTAN 91-27/2(1997) : 1997 GREASE, AUTOMOTIVE AND ARTILLERY - NATO CODE: G-403 - JOINT SERVICE DESIGNATION: XG-279
DEFSTAN 91-106/1(1997) : 1997 GREASE, MULTI-PURPOSE, ELEVATED TEMPERATURE RANGE - JOINT SERVICE DESIGNATION: XG-294
DEFSTAN 91-22/3(1997) : 1997 LUBRICATING OIL, DIESEL ENGINE: SEVERE SERVICE, GRADE 40 - NATO CODE: 0-278 - JOINT SERVICE DESIGNATION: OMD-113
BS 4475:2000 Specification for straight mineral lubricating oils
BS 489:1999 Specification for turbine lubricants
DEFSTAN 91-53/2(1997) : 1997 GREASE, MULTI-PURPOSE, LOW TEMPERATURE RANGE - NATO CODE: G-354 - JOINT SERVICE DESIGNATION: XG-287
17/30351591 DC : 0 BS 2869 - FUEL OILS FOR AGRICULTURAL, DOMESTIC AND INDUSTRIAL ENGINES AND BOILERS - SPECIFICATION
DEFSTAN 91-111/2(2015) : 2015 GREASE, PUMPABLE, CALCIUM BASE JOINT SERVICE DESIGNATION: XG-380
BS 7800:1998 Specification for high octane (super) unleaded petrol (gasoline) for motor vehicles
BS 7800:2006 Automotive fuel. High octane (super) unleaded petrol. Specification
BS 4250:1997 Specification for commercial butane and commercial propane
BS 4040:1997 Specification for leaded petrol (gasoline) for motor vehicles
BS 4250:2014 Specification for commercial butane and commercial propane
BS 7800:2000 Automotive fuel. High octane (super) unleaded petrol. Specification
BS 4040:2001 Specification for leaded petrol (gasoline) for motor vehicles
DEFSTAN 91-48/2(1997) : 1997 HYDRAULIC FLUID, PETROLEUM: SUPERCLEAN NATO CODE: H-515 JOINT SERVICE DESIGNATION: OM-15 HYDRAULIC FLUID, PETROLEUM: NORMAL NATO CODE: H-520 JOINT SERVICE DESIGNATION: OM-18
DEFSTAN 91-34/3(2015) : 2015 GREASE, SEA WATER RESISTING NATO CODE: G-460 JOINT SERVICE DESIGNATION: XG-286
DEFSTAN 91-25/3(1997) : 1997 LUBRICATING OIL, STEAM TURBINE AND GEAR: LIGHT SERVICE NATO CODE: 0-240 JOINT SERVICE DESIGNATION: OM-100
DEFSTAN 91-105/1(1997) : 1997 GREASE, MULTI-PURPOSE, HEAVY DUTY - NATO CODE: G-421 - JOINT SERVICE DESIGNATION: XG-291
DEFSTAN 91-22/6(2014) : 2014 LUBRICATING OIL, DIESEL ENGINE: SEVERE SERVICE, GRADE 40 NATO CODE: O-278 JOINT SERVICE DESIGNATION: OMD-113
97/124012 DC : DRAFT OCT 1997
DEFSTAN 91-110/1(1997) : 1997 HYDRAULIC FLUID, FIRE RESISTANT AQUEOUS POLYGLYCOL JOINT SERVICE DESIGNATION: OX-40
DEFSTAN 91-38/2(2015) : 2015 PETROLATUM, TECHNICAL JOINT SERVICE DESIGNATION: PX-6 PETROLATUM, TECHNICAL NATO CODE NO: S-743 JOINT SERVICE DESIGNATION: PX-7
BS 2869:2017 Fuel oils for agricultural, domestic and industrial engines and boilers Specification
BS 2869(2010) : 2010 FUEL OILS FOR AGRICULTURAL, DOMESTIC AND INDUSTRIAL ENGINES AND BOILERS - SPECIFICATION
BS 2869:1998 Specification for fuel oils for agricultural, domestic and industrial engines and boilers

ISO 3534-2:2006 Statistics Vocabulary and symbols Part 2: Applied statistics
ISO 5725-2:1994 Accuracy (trueness and precision) of measurement methods and results Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method

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