Stationary source emissions. Determination of gas and particle-phase polycyclic aromatic hydrocarbons Sample preparation, clean-up and determination

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Hardcopy , PDF

Language(s)

English

Published date

27-11-2003

Publisher

British Standards Institution

Foreword
Introduction
1 Scope
2 Normative references
3 Terms and definitions
4 Principle
   4.1 Sampling
   4.2 Analysis
5 Safety measures
6 Procedures
   6.1 HPLC method
   6.2 GC-MS method
7 Limitations and interferences
   7.1 Limitations
   7.2 Interferences
Annex A (informative) - Maximum UV absorption wavelength and
                        recommended combinations of
                        excitation-emission wavelengths for HPLC
Annex B (informative) - Formulae and physical properties of selected
                        PAH
Annex C (informative) - Characteristic ions for GC-MS detection of
                        selected PAH, recovery, and surrogate
                        recovery standards
Annex D (informative) - Applicability of internal standards for
                        GC-MS detection of selected PAH
Annex E (normative) - Summary of performance characteristics
                        of the HPLC method
Bibliography

Gives procedures for sample preparation, clean-up and analysis for the determination of gas and particle-phase polycyclic aromatic hydrocarbons (PAH) in stack and waste gases.

This part of ISO 11338 specifies procedures for sample preparation, clean-up and analysis for the determination of gas and particle-phase polycyclic aromatic hydrocarbons (PAH) in stack and waste gases. The analytical methods are capable of detecting sub-microgram concentrations of PAH per cubic metre of sample, depending on the type of PAH and the flue gas volume sampled.

The methods described in this part of ISO 11338 are based on either high performance liquid chromatography (HPLC) or gas chromatography-mass spectrometry (GC-MS).

NOTE ISO 11338-1 describes three methods and specifies minimum requirements for the sampling of PAH in stack and waste gases.

Committee	EH/2/1
DevelopmentNote	Supersedes 99/563634 DC (12/2003)
DocumentType	Standard
Pages	32
PublisherName	British Standards Institution
Status	Current
Supersedes	99/563634 DC : JUL 99

Standards	Relationship
ISO 11338-2:2003	Identical

VDI 3873 Blatt 1:1992-11	Emission measurement; measurement of Polycyclic Aromatic Hydrocarbons (PAH) in stationary industrial plants; dilution method (RWTUeV method); gas-chromatographic determination
ISO 12884:2000	Ambient air Determination of total (gas and particle-phase) polycyclic aromatic hydrocarbons Collection on sorbent-backed filters with gas chromatographic/mass spectrometric analyses
ISO 11338-1:2003	Stationary source emissions Determination of gas and particle-phase polycyclic aromatic hydrocarbons Part 1: Sampling
ISO 4225:1994	Air quality General aspects Vocabulary
VDI 3872 Blatt 1:1989-05	Emission measurement; measurement of polycyclic aromatic hydrocarbons(PAH); measurement of PAH in the exhaust gas from gasoline and diesel; engines of passenger cars; gas chromatographic determination
VDI 3872 Blatt 2:1995-12	Emission measurement - Measurement of polycyclic aromatic hydrocarbons (PAHs) - Measurement of PAHs in the diluted exhaust gas from gasoline and diesel engines of passenger cars gas chromatographic determination - Dilution tunnel method

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BS ISO 11338-2:2003

Stationary source emissions. Determination of gas and particle-phase polycyclic aromatic hydrocarbons Sample preparation, clean-up and determination

Table of Contents

Abstract

Scope

General Product Information

International Equivalents

Standards Referencing This Book

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