Tobacco. Determination of tobacco specific nitrosamines. Method using buffer extraction

Available format(s)

Hardcopy , PDF

Language(s)

English

Published date

31-03-2009

Publisher

British Standards Institution

Foreword
Introduction
1 Scope
2 Normative references
3 Terms and definitions
4 Principle
5 Reagents
6 Apparatus
7 Preparation of extraction solution and standards
   7.1 Preparation of buffer extraction solution
   7.2 Preparation of internal standard
   7.3 Preparation of calibration standards
   7.4 Setting up of the gas chromatograph and detector
   7.5 Tobacco extraction and isolation of TSNAs
   7.6 Extract concentration
8 Data analysis and calculation of results
9 Repeatability and reproducibility
10 Test report
Annex A (informative) - Typical chromatograms and
        calibration curves
Bibliography

Describes the procedure for the determination of the tobacco specific nitrosamines (TSNAs): N-nitrosonornicotine (NNN), N-nitrosoanatabine (NAT), N-nitrosoanabasine (NAB) and 4-(methylnitrosamino)-1-(3-pyridyl)-1-butanone (NNK) in ground leaf tobacco, manufactured tobacco and tobacco products.

This International Standard specifies the procedure for the determination of the tobacco specific nitrosamines (TSNAs): N-nitrosonornicotine (NNN), N-nitrosoanatabine (NAT), N-nitrosoanabasine (NAB) and 4-(methylnitrosamino)-1-(3-pyridyl)-1-butanone (NNK) in ground leaf tobacco, manufactured tobacco and tobacco products. The determination is by means of gas chromatography.

Committee	AW/40
DevelopmentNote	Supersedes 07/30160967 DC. (03/2009)
DocumentType	Standard
Pages	20
PublisherName	British Standards Institution
Status	Current
Supersedes	07/30160967 DC : 0

Standards	Relationship
ISO 22303:2008	Identical

ISO 1042:1998	Laboratory glassware One-mark volumetric flasks
ISO/TS 22304:2008	Tobacco Determination of tobacco specific nitrosamines Method using alkaline dichloromethane extraction
ISO 3696:1987	Water for analytical laboratory use — Specification and test methods

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BS ISO 22303:2008

Current

Table of Contents

Abstract

Scope

General Product Information

International Equivalents

Standards Referencing This Book

Category

Subcategory

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