Surface chemical analysis. X-ray photoelectron spectroscopy. Repeatability and constancy of intensity scale

Available format(s)

Hardcopy , PDF

Language(s)

English

Published date

11-09-2005

Publisher

British Standards Institution

Foreword
Introduction
1 Scope
2 Symbols and abbreviations
3 Outline of method
4 Method for evaluating the repeatability and constancy of
  the intensity scale
  4.1 Obtaining the reference sample
  4.2 Mounting the sample
  4.3 Cleaning the sample
  4.4 Choosing the spectrometer settings for which intensity
       stability is to be determined
  4.5 Operating the instrument
  4.6 Options for initial or subsequent evaluation measurements
  4.7 Measurements for the intensity and repeatability
  4.8 Calculating the peak area intensities, intensity ratios
       and uncertainties
  4.9 Procedure for the regular evaluation of the constancy
       of the intensity scale
  4.10 Next evaluation
Annex A (informative) Example of calculations and measurements
        of the intensity repeatability for a commercial X-ray
        photoelectron spectrometer using unmonochromated
        Mg K[Alpha] X-rays
Bibliography

Specifies a method for evaluating the repeatability and constancy of the intensity scale of X-ray photoelectron spectrometers, for general analytical purposes, using unmonochromated Al or Mg X-rays or monochromated Al X-rays.

This International Standard specifies a method for evaluating the repeatability and constancy of the intensity scale of X-ray photoelectron spectrometers, for general analytical purposes, using unmonochromated Al or Mg X-rays or monochromated Al X-rays. It is only applicable to instruments that incorporate an ion gun for sputter cleaning. It is not intended to be a calibration of the intensity/energy response function. That calibration may be made by the instrument manufacturer or other organization. The present procedure provides data to evaluate and confirm the accuracy with which the intensity/energy response function remains constant with instrument usage. Guidance is given on some of the instrument settings that may affect this constancy.

Committee	CII/60
DevelopmentNote	Supersedes 04/30109361 DC. (09/2005) Reviewed and confirmed by BSI, March 2016. (03/2016)
DocumentType	Standard
Pages	22
PublisherName	British Standards Institution
Status	Current
Supersedes	04/30109361 DC : DRAFT FEB 2004

Standards	Relationship
ISO 24237:2005	Identical

ISO 18118:2015	Surface chemical analysis — Auger electron spectroscopy and X-ray photoelectron spectroscopy — Guide to the use of experimentally determined relative sensitivity factors for the quantitative analysis of homogeneous materials
ISO 7873:1993	Control charts for arithmetic average with warning limits
ISO 15472:2010	Surface chemical analysis X-ray photoelectron spectrometers Calibration of energy scales
ISO 7870:1993	Control charts General guide and introduction

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BS ISO 24237:2005

Current

Table of Contents

Abstract

Scope

General Product Information

International Equivalents

Standards Referencing This Book

Category

Subcategory

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