Pulps. Determination of limiting viscosity number in cupri-ethylenediamine (CED) solution

Available format(s)

Hardcopy , PDF

Language(s)

English

Published date

31-03-2010

Publisher

British Standards Institution

Foreword
Introduction
1 Scope
2 Normative references
3 Terms and definitions
4 Principle
5 Reagents and materials
6 Apparatus and materials
7 Calibration of viscometers
8 Sampling and preparation of sample
9 Procedure
10 Calculation
11 Precision
12 Test report
Annex A (normative) - Preparation and analysis of the
        cupri-ethylenediamine (CED) solution
Annex B (normative) - Values of [eta] x rho corresponding
        to different values of the viscosity ratio
        eta[ratio] (eta/eta[0])
Annex C (informative) - Calculation of degree of
        polymerization
Bibliography

Describes a method which yields a number that is an estimate of the limiting viscosity number of pulp in a dilute cupri-ethylenediamine (CED) solution.

This International Standard specifies a method which yields a number that is an estimate of the limiting viscosity number of pulp in a dilute cupri-ethylenediamine (CED) solution.

This International Standard is primarily applicable to CED-soluble samples of bleached chemical pulps, but can also be applied to any kind of pulp that dissolves completely in CED solution.

NOTE1 The results can be used to estimate the extent of cellulose degradation caused by cooking or bleaching. Results obtained with samples containing appreciable amounts of substances other than cellulose must be interpreted with caution, however.

NOTE2 In the strictest sense, viscosity measurement procedures are applicable only to the polysaccharide fraction of the sample. This notwithstanding, viscosity measurement can usually be used to obtain a result on unbleached pulps having lignin contents of up to 4%, because most of these pulps can be successfully dissolved in CED. However, the simple fact that an unbleached pulp can be dissolved in CED does not mean that the results are valid. In summary, viscosity results for pulps containing more than 0,5%of lignin are not acceptable for technical specification purposes.

Committee	PAI/11
DevelopmentNote	Supersedes BS 6306-1(1982) and 03/306734 DC. (03/2007) Supersedes 08/30190494 DC. (03/2010)
DocumentType	Standard
Pages	30
PublisherName	British Standards Institution
Status	Current
Supersedes	08/30190494 DC : DRAFT OCT 2008 03/306734 DC : DRAFT MAY 2003 BS ISO 5351:2004 BS 6306-1:1982

Standards	Relationship
ISO 5351:2010	Identical

ISO 638:2008	Paper, board and pulps Determination of dry matter content Oven-drying method
TAPPI T 230 : 2013	VISCOSITY OF PULP (CAPILLARY VISCOMETER METHOD)
ISO 7213:1981	Pulps Sampling for testing

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BS ISO 5351:2010

Current

Table of Contents

Abstract

Scope

General Product Information

International Equivalents

Standards Referencing This Book

Category

Subcategory

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