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BS ISO 8260:2008

Current
Current

The latest, up-to-date edition.

Milk and milk products. Determination of organochlorine pesticides and polychlorobiphenyls. Method using capillary gas-liquid chromatography with electron- capture detection
Available format(s)

Hardcopy , PDF

Language(s)

English

Published date

31-12-2008

Foreword
Foreword
Introduction
1 Scope
2 Normative references
3 Terms and definitions
4 Principle
5 Reagents and materials
6 Apparatus
7 Sampling
8 Preparation of sample
   8.1 Milk
   8.2 Evaporated milk
   8.3 Sweetened condensed milk
   8.4 Powdered milk products
   8.5 Butter and butterfat
   8.6 Cheese
   8.7 Other milk products
9 Preparation of test sample
   9.1 Extraction of milk
   9.2 Extraction of sweetened condensed milk, powdered
        milk products, butter, butterfat and cheese
10 Procedure
   10.1 General
   10.2 Blank test
   10.3 Cryogenic extraction
   10.4 Clean-up
   10.5 Gas chromatography
   10.6 Blank result
11 Calculation and expression of results
   11.1 Calculation of the response factor
   11.2 Expression of the response factor
   11.3 Calculation of the organochlorine compound content
   11.4 Expression of the result
   11.5 Relative retention time
   11.6 Expression of the retention time
12 Precision
   12.1 General
   12.2 Repeatability
   12.3 Reproducibility
13 Test report
Annex A (informative) - Interlaboratory trial
Annex B (informative) - Example of a chromatogram
Bibliography

Describes a method for the determination of the contents of individual organochlorine pesticides (OCPs) and polychlorinated biphenyls (PCBs) in milk, evaporated milk, sweetened condensed milk, powdered milk products, butter and butterfat, cheese and other milk products.

Committee
AW/5
DevelopmentNote
Supersedes 07/30163272 DC. (01/2009)
DocumentType
Standard
Pages
26
PublisherName
British Standards Institution
Status
Current
Supersedes

Standards Relationship
ISO 8260:2008 Identical

ISO 707:2008 Milk and milk products — Guidance on sampling
ISO 14156:2001 Milk and milk products — Extraction methods for lipids and liposoluble compounds
ISO 3890-2:2009 Milk and milk products Determination of residues of organochlorine compounds (pesticides) Part 2: Test methods for crude extract purification and confirmation
ISO 5725-2:1994 Accuracy (trueness and precision) of measurement methods and results Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method

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