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CEN/TR 10345:2013

Current
Current

The latest, up-to-date edition.

Guideline for statistical data treatment of inter laboratory tests for validation of analytical methods
Published date

04-12-2013

Foreword
1 Scope
2 Normative references
3 Principle
4 Preliminary rules
5 Procedure
6 Report
7 General remarks
Annex A (normative) - Steps for the validation of
        a draft Standard
Annex B (normative) - Synoptic of the operations
        described in Annex A
Annex C (informative) - Examples
Bibliography

This Technical Report is a guideline to carry out the statistical evaluation of data from an inter laboratory test for method validation.Its purpose is to detail the methodology of ISO 5725 1:1994, ISO 5725 2:1994 and ISO 5725 3:1994 for the treatment of the data collected under the conditions used within the ECISS/TC 102 working groups.NOTEThe present document is not a simplification of the ISO 5725 standard, which is the only reference document.

Committee
CEN/TC 459/SC 2
DocumentType
Technical Report
PublisherName
Comite Europeen de Normalisation
Status
Current

BS EN 10351:2011 Chemical analysis of ferrous materials. Inductively coupled plasma optical emission spectrometric analysis of unalloyed and low alloyed steels. Determination of Mn, P, Cu, Ni, Cr, Mo, V, Co, Al (total) and Sn [Routine method]
DIN EN 10351:2011-05 Chemical analysis of ferrous materials - Inductively coupled plasma optical emission spectrometric analysis of unalloyed and low alloyed steels - Determination of Mn, P, Cu, Ni, Cr, Mo, V, Co, Al (total) and Sn [Routine method]
UNE-EN 10351:2012 Chemical analysis of ferrous materials - Inductively coupled plasma optical emission spectrometric analysis of unalloyed and low alloyed steels - Determination of Mn, P, Cu, Ni, Cr, Mo, V, Co, Al (total) and Sn [Routine method]
EN 10361:2015 Alloyed steels - Determination of nickel content - Inductively coupled plasma optical emission spectrometric method
EN 10351:2011 Chemical analysis of ferrous materials - Inductively coupled plasma optical emission spectrometric analysis of unalloyed and low alloyed steels - Determination of Mn, P, Cu, Ni, Cr, Mo, V, Co, Al (total) and Sn [Routine method]
EN 10355:2013 Chemical analysis of ferrous materials - Inductively coupled plasma optical emission spectrometric analysis of unalloyed and low alloyed steels - Determination of Si, Mn, P, Cu, Ni, Cr, Mo and Sn, following dissolution with nitric and sulphuric acids [Routine method]
11/30252539 DC : 0 BS EN 10355 - CHEMICAL ANALYSIS OF FERROUS MATERIALS - INDUCTIVELY COUPLED PLASMA OPTICAL EMISSION SPECTROMETRIC ANALYSIS OF UNALLOYED AND LOW ALLOYED STEELS - DETERMINATION OF SI, MN, P, CU, NI, CR, MO, SN [ROUTINE METHOD]
BS EN 10361:2015 Alloyed steels. Determination of nickel content. Inductively coupled plasma optical emission spectrometric method
UNI EN 10351 : 2011 CHEMICAL ANALYSIS OF FERROUS MATERIALS - INDUCTIVELY COUPLED PLASMA OPTICAL EMISSION SPECTROMETRIC ANALYSIS OF UNALLOYED AND LOW ALLOYED STEELS - DETERMINATION OF MN, P, CU, NI, CR, MO, V, CO, AL (TOTAL) AND SN [ROUTINE METHOD]
I.S. EN 10351:2011 CHEMICAL ANALYSIS OF FERROUS MATERIALS - INDUCTIVELY COUPLED PLASMA OPTICAL EMISSION SPECTROMETRIC ANALYSIS OF UNALLOYED AND LOW ALLOYED STEELS - DETERMINATION OF MN, P, CU, NI, CR, MO, V, CO, AL (TOTAL) AND SN [ROUTINE METHOD]
CEN/TR 10261:2013 Iron and steel - European standards for the determination of chemical composition
NF EN 10351 : 2011 CHEMICAL ANALYSIS OF FERROUS MATERIALS - INDUCTIVELY COUPLED PLASMA OPTICAL EMISSION SPECTROMETRIC ANALYSIS OF UNALLOYED AND LOW ALLOYED STEELS - DETERMINATION OF MN, P, CU, NI, CR, MO, V, CO, AL (TOTAL) AND SN [ROUTINE METHOD]
DIN EN 10355:2013-11 Chemical analysis of ferrous materials - Inductively coupled plasma optical emission spectrometric analysis of unalloyed and low alloyed steels - Determination of Si, Mn, P, Cu, Ni, Cr, Mo and Sn, following dissolution with nitric and sulphuric acids [Routine method]
DIN EN 10355 E : 2013 CHEMICAL ANALYSIS OF FERROUS MATERIALS - INDUCTIVELY COUPLED PLASMA OPTICAL EMISSION SPECTROMETRIC ANALYSIS OF UNALLOYED AND LOW ALLOYED STEELS - DETERMINATION OF SI, MN, P, CU, NI, CR, MO AND SN, FOLLOWING DISSOLUTION WITH NITRIC AND SULPHURIC ACIDS [ROUTINE METHOD]
UNE-EN 10355:2014 Chemical analysis of ferrous materials - Inductively coupled plasma optical emission spectrometric analysis of unalloyed and low alloyed steels - Determination of Si, Mn, P, Cu, Ni, Cr, Mo and Sn, following dissolution with nitric and sulphuric acids [Routine method]
I.S. EN 10361:2015 ALLOYED STEELS - DETERMINATION OF NICKEL CONTENT - INDUCTIVELY COUPLED PLASMA OPTICAL EMISSION SPECTROMETRIC METHOD
ISO/TS 18223:2015 Nickel alloys — Determination of Nickel content — Inductively coupled plasma atomic emission spectrometric method
DIN EN 10361:2016-02 ALLOYED STEELS - DETERMINATION OF NICKEL CONTENT - INDUCTIVELY COUPLED PLASMA OPTICAL EMISSION SPECTROMETRIC METHOD
DIN EN 10361 E : 2016 ALLOYED STEELS - DETERMINATION OF NICKEL CONTENT - INDUCTIVELY COUPLED PLASMA OPTICAL EMISSION SPECTROMETRIC METHOD
BS EN 10355:2013 Chemical analysis of ferrous materials. Inductively coupled plasma optical emission spectrometric analysis of unalloyed and low alloyed steels. Determination of Si, Mn, P, Cu, Ni, Cr, Mo and Sn, following dissolution with nitric and sulphuric acids [Routine method]
UNI EN 10355 : 2013 CHEMICAL ANALYSIS OF FERROUS MATERIALS - INDUCTIVELY COUPLED PLASMA OPTICAL EMISSION SPECTROMETRIC ANALYSIS OF UNALLOYED AND LOW ALLOYED STEELS - DETERMINATION OF SI, MN, P, CU, NI, CR, MO AND SN, FOLLOWING DISSOLUTION WITH NITRIC AND SULPHURIC ACIDS [ROUTINE METHOD]
PD CEN/TR 10261:2013 Iron and steel. European standards for the determination of chemical composition
09/30203049 DC : 0 BS EN 10351 - CHEMICAL ANALYSIS OF FERROUS MATERIALS - INDUCTIVELY COUPLED PLASMA OPTICAL EMISSION SPECTROMETRIC ANALYSIS OF LOW ALLOYED STEELS - DETERMINATION OF MN, P, CU, NI, CR, MO, V, CO, AL (TOTAL) AND SN (ROUTINE METHOD)
13/30291170 DC : 0 BS EN 10361 - ALLOYED STEELS - DETERMINATION OF NICKEL CONTENT - INDUCTIVELY COUPLED PLASMA OPTICAL EMISSION SPECTROMETRIC METHOD
UNE-EN 10361:2016 Alloyed steels - Determination of nickel content - Inductively coupled plasma optical emission spectrometric method
I.S. EN 10355:2013 CHEMICAL ANALYSIS OF FERROUS MATERIALS - INDUCTIVELY COUPLED PLASMA OPTICAL EMISSION SPECTROMETRIC ANALYSIS OF UNALLOYED AND LOW ALLOYED STEELS - DETERMINATION OF SI, MN, P, CU, NI, CR, MO AND SN, FOLLOWING DISSOLUTION WITH NITRIC AND SULPHURIC ACIDS [ROUTINE METHOD]

ISO 5725-1:1994 Accuracy (trueness and precision) of measurement methods and results — Part 1: General principles and definitions
ISO/TR 22971:2005 Accuracy (trueness and precision) of measurement methods and results Practical guidance for the use of ISO 5725-2:1994 in designing, implementing and statistically analysing interlaboratory repeatability and reproducibility results
ISO 5725-3:1994 Accuracy (trueness and precision) of measurement methods and results — Part 3: Intermediate measures of the precision of a standard measurement method
ISO 5725-2:1994 Accuracy (trueness and precision) of measurement methods and results Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method
NFX 06 050 : 1995 APPLICATION OF STATISTICS - STUDY OF THE NORMALITY OF A DISTRIBUTION
ISO 3534-1:2006 Statistics — Vocabulary and symbols — Part 1: General statistical terms and terms used in probability

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