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CEN/TR 15160:2005

Current
Current

The latest, up-to-date edition.

Petroleum and related products - Applicability of diesel fuel test methods for Fatty Acid Methyl Esters (FAME) - Information and results on round robin tests
Published date

03-08-2005

Foreword
Introduction
1 Summary
2 Background
3 Basis of the work
4 Details of the round robin
5 Results
6 Conclusion
Annex A (informative) List of participants in working group
                      26 activities
Annex B (informative) Report of the result of the round robin
                      on 'determination of flash point using the
                      rapid equilibrium close cup method'
                      (prEN ISO/DIS 3679)
Annex C (informative) Report of the result of the round robin
                      series on 'distillation of petroleum
                      products at reduced pressure' (ASTM D 1160)
Annex D (informative) Preliminary study on applicability of
                      'distillation of petroleum products at
                      atmospheric pressure' (EN ISO 3405) on
                      blends of FAME in diesel fuel
Annex E (informative) Report of the results of the round robin
                      on 'determination of carbon residue via
                      the micro method' (EN ISO 10370)
Annex F (informative) Report of the result of the round robin
                      series on 'corrosiveness to copper via
                      the copper strip test' (EN ISO 2160)
Annex G (informative) Report of the result of the round robin
                      series on 'determination of fatty acid
                      methyl esters (FAME) in middle distillates
                      via infrared spectroscopy' (prEN 14078)
Annex H (informative) Influence of FAME origin on the measure of
                      FAME content in mineral oil using
                      prEN 14078 ('Determination of fatty acid
                      methyl esters (FAME) in middle distillates
                      via infrared spectroscopy method')

(no Scope)



1Summary

One task under the European Mandate M/245 was to investigate the applicability of existing petroleum test method standards for fatty acid methyl esters (FAME). For this task CEN/TC 19 has founded a separate working group 26, which has validated 24 methods via round robins, including the development of new test methods.

The work of CEN/TC 19/WG 26 was aimed at the drafting of amendments for existing ISO standards (with test methods for fossil fuels). These amendments include the extension of the scope of the standards to biodiesel as well as the new precision data for biodiesel. To get these new precision data (repeatability & reproducibility), WG 26 has done a major effort to validate all relevant test methods on request of the Task Force of WG 24 and WG 25 dealing with the specifications.

2Background

CEN has been asked by the Commission (Mandate M/245) to elaborate standards for fatty acid methyl esters (FAME) to be used as sole fuel for heating and diesel engines and as an additive to mineral oil based fuels. This work has been divided amongst two Technical Committees, of which CEN/TC 19 was responsible for determining the applicability of already existing petroleum type test method standards to both pure FAME and to blends. This included comparing precision data, generating new reproducibility and repeatability figures and developing new test method standards if necessary.

Committee
CEN/TC 19
DocumentType
Technical Report
PublisherName
Comite Europeen de Normalisation
Status
Current

Standards Relationship
PD CEN/TR 15160:2005 Identical
NEN NPR CEN/TR 15160 : 2005 Identical
I.S. CEN/TR 15160:2005 Identical
UNI CEN/TR 15160 : 2005 Identical

09/30205523 DC : 0 BS EN 14214 - AUTOMOTIVE FUELS - FATTY ACID METHYL ESTERS (FAME) FOR DIESEL ENGINES - REQUIREMENTS AND TEST METHODS
EN 16734:2016 Automotive fuels - Automotive B10 diesel fuel - Requirements and test methods
BS EN 16734 : 2016 AUTOMOTIVE FUELS - AUTOMOTIVE B10 DIESEL FUEL - REQUIREMENTS AND TEST METHODS
I.S. EN 16734:2016 AUTOMOTIVE FUELS - AUTOMOTIVE B10 DIESEL FUEL - REQUIREMENTS AND TEST METHODS
16/30294369 DC : 0 BS ISO 8217 - PETROLEUM PRODUCTS - FUELS (CLASS F) - SPECIFICATIONS OF MARINE FUELS
14/30298209 DC : 0 BS EN 16734 - AUTOMOTIVE FUELS - AUTOMOTIVE B10 DIESEL FUEL - REQUIREMENTS AND TEST METHODS
ISO 8217:2017 Petroleum products Fuels (class F) Specifications of marine fuels
BS EN 14214:2012 LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS
DIN EN 14214:2014-06 LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS
I.S. EN ISO 3679:2015 DETERMINATION OF FLASH NO-FLASH AND FLASH POINT - RAPID EQUILIBRIUM CLOSED CUP METHOD (ISO 3679:2015)
DIN EN 14214 E : 2003 LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS
BS ISO 8217:2017 Petroleum products. Fuels (class F). Specifications of marine fuels
BS 2000-523(2015) : 2015 DETERMINATION OF FLASH NO-FLASH AND FLASH POINT - RAPID EQUILIBRIUM CLOSED CUP METHOD
18/30358429 DC : DRAFT APR 2018 BS EN ISO 3015 - PETROLEUM AND RELATED PRODUCTS FROM NATURAL OR SYNTHETIC SOURCES - DETERMINATION OF CLOUD POINT
PREN 590 : DRAFT 2011 AUTOMOTIVE FUELS - DIESEL - REQUIREMENTS AND TEST METHODS
I.S. EN 14214:2012 LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS
UNE-EN 16734:2017 Automotive fuels - Automotive B10 diesel fuel - Requirements and test methods
UNI EN 14214 : 2014 LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS
DIN EN ISO 3679:2015-06 Determination of flash no-flash and flash point - Rapid equilibrium closed cup method (ISO 3679:2015)
EN 14214:2012+A1:2014/AC:2014 LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS
PREN 14214 : DRAFT 2009 AUTOMOTIVE FUELS - FATTY ACID METHYL ESTERS (FAME) FOR DIESEL ENGINES - REQUIREMENTS AND TEST METHODS
13/30285144 DC : 0 BS ISO 3679 - DETERMINATION OF FLASH POINT - RAPID EQUILIBRIUM CLOSED CUP METHOD
ISO 3679:2015 Determination of flash no-flash and flash point — Rapid equilibrium closed cup method
BS EN ISO 3679:2015 Determination of flash no-flash and flash point. Rapid equilibrium closed cup method
UNE-EN ISO 3679:2015 Determination of flash no-flash and flash point - Rapid equilibrium closed cup method (ISO 3679:2015)
EN ISO 3679:2015 Determination of flash no-flash and flash point - Rapid equilibrium closed cup method (ISO 3679:2015)
11/30249539 DC : 0 BS EN 590 - AUTOMOTIVE FUELS - DIESEL - REQUIREMENTS AND TEST METHODS
DIN EN 590:2017-10 Automotive fuels - Diesel - Requirements and test methods (includes Amendment :2017)
UNE-EN 14214:2013 Liquid petroleum products - Fatty acid methyl esters (FAME) for use in diesel engines and heating applications - Requirements and test methods
UNE-EN 590:2014 Automotive fuels - Diesel - Requirements and test methods
DIN EN 14214:2003-11 LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS

ISO 3016:1994 Petroleum products Determination of pour point
ISO 2719:2016 Determination of flash point Pensky-Martens closed cup method
ISO 13759:1996 Petroleum products — Determination of alkyl nitrate in diesel fuels — Spectrometric method
ISO 12937:2000 Petroleum products — Determination of water — Coulometric Karl Fischer titration method
ISO 3675:1998 Crude petroleum and liquid petroleum products Laboratory determination of density Hydrometer method
EN ISO 3104:1996 Petroleum products - Transparent and opaque liquids - Determination of kinematic viscosity and calculation of dynamic viscosity (ISO 3104:1994)
ISO 3987:2010 Petroleum products — Determination of sulfated ash in lubricating oils and additives
ISO 5165:1998 Petroleum products Determination of the ignition quality of diesel fuels Cetane engine method
EN 116:2015 Diesel and domestic heating fuels - Determination of cold filter plugging point - Stepwise cooling bath method
EN ISO 12185:1996 Crude petroleum and petroleum products - Determination of density - Oscillating U-tube method (ISO 12185:1996)
EN ISO 14596:2007 Petroleum products - Determination of sulfur content - Wavelength-dispersive X-ray fluorescence spectrometry (ISO 14596:2007)
ISO 2160:1998 Petroleum products Corrosiveness to copper Copper strip test
ISO 12156-1:2016 Diesel fuel Assessment of lubricity using the high-frequency reciprocating rig (HFRR) Part 1: Test method
EN ISO 10370:2014 Petroleum products - Determination of carbon residue - Micro method (ISO 10370:2014)
EN ISO 3675:1998 Crude petroleum and liquid petroleum products - Laboratory determination of density - Hydrometer method (ISO 3675:1998)
EN ISO 12205 : 1996 Petroleum products - Determination of the oxidation stability of middle-distillate fuels (ISO 12205:1995)
ISO 3679:2015 Determination of flash no-flash and flash point — Rapid equilibrium closed cup method
EN ISO 3405:2011 Petroleum products - Determination of distillation characteristics at atmospheric pressure (ISO 3405:2011)
ISO 10370:2014 Petroleum products — Determination of carbon residue — Micro method
ISO 12185:1996 Crude petroleum and petroleum products — Determination of density — Oscillating U-tube method
ISO 12205:1995 Petroleum products — Determination of the oxidation stability of middle-distillate fuels
PREN 14078 : DRAFT 2013 LIQUID PETROLEUM PRODUCTS - DETERMINATION OF FATTY ACID METHYL ESTER (FAME) CONTENT IN MIDDLE DISTILLATES - INFRARED SPECTROMETRY METHOD
ISO 6245:2001 Petroleum products — Determination of ash
ISO 4259:2006 Petroleum products Determination and application of precision data in relation to methods of test
EN 12662:2014 Liquid petroleum products - Determination of total contamination in middle distillates, diesel fuels and fatty acid methyl esters
EN ISO 12937:2000 Petroleum products - Determination of water - Coulometric Karl Fischer titration method (ISO 12937:2000)
EN 23015:1994 Petroleum products - Determination of cloud point (ISO 3015:1992)
EN 12634:1998 Petroleum products and lubricants - Determination of acid number - Non-aqueous potentiometric titration method
EN 22719 : 1993 PETROLEUM PRODUCTS AND LUBRICANTS - DETERMINATION OF FLASH POINT - PENSKY-MARTENS CLOSED CUP METHOD
ISO 3405:2011 Petroleum products Determination of distillation characteristics at atmospheric pressure
EN ISO 13759:1996 Petroleum products - Determination of alkyl nitrate in diesel fuels - Spectrometric method (ISO 13759:1996)
EN ISO 3679:2015 Determination of flash no-flash and flash point - Rapid equilibrium closed cup method (ISO 3679:2015)
ISO 14596:2007 Petroleum products — Determination of sulfur content — Wavelength-dispersive X-ray fluorescence spectrometry
EN ISO 2160:1998 Petroleum products - Corrosiveness to copper - Copper strip test (ISO 2160:1998)
ISO 3015:1992 Petroleum products — Determination of cloud point
EN ISO 4259:2006 Petroleum products - Determination and application of precision data in relation to methods of test (ISO 4259:2006)

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