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CEN/TS 14405 : 2004

Superseded
Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

View Superseded by
superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

CHARACTERIZATION OF WASTE - LEACHING BEHAVIOUR TESTS - UP-FLOW PERCOLATION TEST (UNDER SPECIFIED CONDITIONS)
Superseded date

01-03-2017

Published date

12-01-2013

Foreword
Introduction
1 Scope
2 Normative references
3 Terms and definitions
4 Principle
5 Equipment and reagents
   5.1 General
6 Sample pre-treatment
   6.1 General
   6.2 Sample preparation
   6.3 Test portion
   6.4 Determination of dry residue
7 Procedure
   7.1 Temperature
   7.2 Preparation
   7.3 Packing of the column
   7.4 Start-up of the test
   7.5 Collection of additional eluate fractions
   7.6 Further preparation of the eluates for analysis
   7.7 Blank test
8 Calculations
9 Test report
10 Test performance
Annex A (informative) Illustration of the column and
                      accompanying equipment
Annex B (informative) Suggestions for packing the column,
                      water saturation and establishment
                      and checking of equilibrium
                      conditions
   B.1 General
   B.2 Guidelines on column filling and packing
   B.3 Water saturation
   B.4 Equilibration and checking of equilibrium conditions
Annex C (informative) Background for the choices made in
                      developing this percolation test
   C.1 Introduction
   C.2 Particle size/particle size distribution
   C.3 Column dimensions
   C.4 Flow mode (up-flow/down-flow)
   C.5 Flow rate of the leachant
   C.6 L/S ratio and eluate fractions collected/duration of
       the test
   C.7 Nature of the leachant
   C.8 Temperature
   C.9 Beneficial use of the test results
Bibliography

Applies to determine the leaching behaviour of inorganic constituents from granular waste (without or with size reduction).

Committee
TC 292
DocumentType
Standard
PublisherName
Comite Europeen de Normalisation
Status
Superseded
SupersededBy

PD CEN/TR 16376:2012 Characterization of waste. Overall guidance document for characterization of waste from the extractive industries
S.R. CEN/TR 16098:2010 CONSTRUCTION PRODUCTS: ASSESSMENT OF RELEASE OF DANGEROUS SUBSTANCES - CONCEPT OF HORIZONTAL TESTING PROCEDURES IN SUPPORT OF REQUIREMENTS UNDER THE CPD
DIN EN 15863:2015-06 CHARACTERIZATION OF WASTE - LEACHING BEHAVIOUR TEST FOR BASIC CHARACTERIZATION - DYNAMIC MONOLITHIC LEACHING TEST WITH PERIODIC LEACHANT RENEWAL, UNDER FIXED CONDITIONS
CEN/TS 15862:2012 Characterisation of waste - Compliance leaching test - One stage batch leaching test for monoliths at fixed liquid to surface area ratio (L/A) for test portions with fixed minimum dimensions
CEN/TR 16376:2012 Characterization of waste - Overall guidance document for characterization of waste from the extractive industries
CEN/TS 16637-3:2016 Construction products - Assessment of release of dangerous substances - Part 3: Horizontal up-flow percolation test
EN 15863:2015 Characterization of waste - Leaching behaviour test for basic characterization - Dynamic monolithic leaching test with periodic leachant renewal, under fixed conditions
DIN EN ISO 18772 E : 2014 SOIL QUALITY - GUIDANCE ON LEACHING PROCEDURES FOR SUBSEQUENT CHEMICAL AND ECOTOXICOLOGICAL TESTING OF SOILS AND SOIL MATERIALS (ISO 18772:2008)
UNI EN 16457 : 2014 CHARACTERIZATION OF WASTE - FRAMEWORK FOR THE PREPARATION AND APPLICATION OF A TESTING PROGRAMME - OBJECTIVES, PLANNING AND REPORT
10/30233988 DC : 0 BS EN 16192 - CHARACTERIZATION OF WASTE - ANALYSIS OF ELUATES
UNI EN ISO 18772 : 2014 SOIL QUALITY - GUIDANCE ON LEACHING PROCEDURES FOR SUBSEQUENT CHEMICAL AND ECOTOXICOLOGICAL TESTING OF SOILS AND SOIL MATERIALS
DIN EN ISO 18772:2014-07 Soil quality - Guidance on leaching procedures for subsequent chemical and ecotoxicological testing of soils and soil materials (ISO 18772:2008)
I.S. EN 16457:2014 CHARACTERIZATION OF WASTE - FRAMEWORK FOR THE PREPARATION AND APPLICATION OF A TESTING PROGRAMME - OBJECTIVES, PLANNING AND REPORT
S.R. CEN/TR 16376:2012 CHARACTERIZATION OF WASTE - OVERALL GUIDANCE DOCUMENT FOR CHARACTERIZATION OF WASTE FROM THE EXTRACTIVE INDUSTRIES
UNI CEN ISO/TS 21268-3 : 2010 SOIL QUALITY - LEACHING PROCEDURES FOR SUBSEQUENT CHEMICAL AND ECOTOXICOLOGICAL TESTING OF SOIL AND SOIL MATERIALS - PART 3: UP-FLOW PERCOLATION TEST
DIN EN 15863 E : 2015 CHARACTERIZATION OF WASTE - LEACHING BEHAVIOUR TEST FOR BASIC CHARACTERIZATION - DYNAMIC MONOLITHIC LEACHING TEST WITH PERIODIC LEACHANT RENEWAL, UNDER FIXED CONDITIONS
UNE-EN 15863:2015 Characterization of waste - Leaching behaviour test for basic characterization - Dynamic monolithic leaching test with periodic leachant renewal, under fixed conditions
UNE-EN 15002:2015 Characterization of waste - Preparation of test portions from the laboratory sample
S.R. CEN/TS 15863:2012 CHARACTERISATION OF WASTE - LEACHING BEHAVIOUR TEST FOR BASIC CHARACTERISATION - DYNAMIC MONOLITHIC LEACHING TEST WITH PERIODIC LEACHANT RENEWAL, UNDER FIXED TEST CONDITIONS
I.S. EN 15002:2015 CHARACTERIZATION OF WASTE - PREPARATION OF TEST PORTIONS FROM THE LABORATORY SAMPLE
S.R. CEN/TS 15862:2012 CHARACTERISATION OF WASTE - COMPLIANCE LEACHING TEST - ONE STAGE BATCH LEACHING TEST FOR MONOLITHS AT FIXED LIQUID TO SURFACE AREA RATIO (L/A) FOR TEST PORTIONS WITH FIXED MINIMUM DIMENSIONS
PD CEN/TS 16660:2015 Characterization of waste. Leaching behaviour test. Determination of the reducing character and the reducing capacity
BS EN 16192:2011 Characterization of waste. Analysis of eluates
DIN EN 16192:2012-02 Characterization of waste - Analysis of eluates
BS EN ISO 18772:2014 Soil quality. Guidance on leaching procedures for subsequent chemical and ecotoxicological testing of soils and soil materials
PD CEN/TR 16098:2010 Construction products. Assessment of release of dangerous substances. Concept of horizontal testing procedures in support of requirements under the CPD
UNE-EN 16457:2014 Characterization of waste - Framework for the preparation and application of a testing programme - Objectives, planning and report
S.R. CEN/TR 16110:2010 CHARACTERIZATION OF WASTE - GUIDANCE ON THE USE OF ECOTOXICITY TESTS APPLIED TO WASTE
I.S. EN 16192:2011 CHARACTERIZATION OF WASTE - ANALYSIS OF ELUATES
S.R. CEN ISO TS 21268-3:2009 SOIL QUALITY - LEACHING PROCEDURES FOR SUBSEQUENT CHEMICAL AND ECOTOXICOLOGICAL TESTING OF SOIL AND SOIL MATERIALS - PART 3: UP-FLOW PERCOLATION TEST
UNI CEN/TS 15862 : 2012 CHARACTERISATION OF WASTE - COMPLIANCE LEACHING TEST - ONE STAGE BATCH LEACHING TEST FOR MONOLITHS AT FIXED LIQUID TO SURFACE AREA RATIO (L/A) FOR TEST PORTIONS WITH FIXED MINIMUM DIMENSIONS
PD CEN/TS 15864:2012 Characterisation of waste. Leaching behaviour test for basic characterisation. Dynamic monolithic leaching test with continuous leachant renewal under conditions relevant for specified scenario(s)
PD CEN/TS 16637-3:2016 Construction products. Assessment of release of dangerous substances Horizontal up-flow percolation test
I.S. EN 15863:2015 CHARACTERIZATION OF WASTE - LEACHING BEHAVIOUR TEST FOR BASIC CHARACTERIZATION - DYNAMIC MONOLITHIC LEACHING TEST WITH PERIODIC LEACHANT RENEWAL, UNDER FIXED CONDITIONS
12/30263896 DC : 0 BS EN 16457 - CHARACTERIZATION OF WASTE - FRAMEWORK FOR THE PREPARATION AND APPLICATION OF A TESTING PROGRAMME - OBJECTIVES, PLANNING AND REPORT
FD CEN/TR 16110 : 2011 FD CHARACTERIZATION OF WASTE - GUIDANCE ON THE USE OF ECOTOXICITY TESTS APPLIED TO WASTE
DIN EN 16457:2014-07 CHARACTERIZATION OF WASTE - FRAMEWORK FOR THE PREPARATION AND APPLICATION OF A TESTING PROGRAMME - OBJECTIVES, PLANNING AND REPORT
S.R. CEN/TS 16637-3:2016 CONSTRUCTION PRODUCTS - ASSESSMENT OF RELEASE OF DANGEROUS SUBSTANCES - PART 3: HORIZONTAL UP-FLOW PERCOLATION TEST
S.R. CEN/TS 15864:2015 CHARACTERISATION OF WASTE - LEACHING BEHAVIOUR TEST FOR BASIC CHARACTERIZATION - DYNAMIC MONOLITHIC LEACHING TEST WITH CONTINUOUS LEACHANT RENEWAL UNDER CONDITIONS RELEVANT FOR SPECIFIED SCENARIO(S)
PD CEN/TS 15862:2012 Characterisation of waste. Compliance leaching test. One stage batch leaching test for monoliths at fixed liquid to surface area ratio (L/A) for test portions with fixed minimum dimensions
PD CEN/TS 15863:2012 Characterisation of waste. Leaching behaviour test for basic characterisation. Dynamic monolithic leaching test with periodic leachant renewal, under fixed test conditions
ISO/TS 21268-3:2007 Soil quality Leaching procedures for subsequent chemical and ecotoxicological testing of soil and soil materials Part 3: Up-flow percolation test
ISO 18772:2008 Soil quality — Guidance on leaching procedures for subsequent chemical and ecotoxicological testing of soils and soil materials
13/30291099 DC : 0 BS EN 15002 - CHARACTERIZATION OF WASTE - PREPARATION OF TEST PORTIONS FROM THE LABORATORY SAMPLE
BS EN 15863:2015 Characterization of waste. Leaching behaviour test for basic characterization. Dynamic monolithic leaching test with periodic leachant renewal, under fixed conditions
DIN EN 15002:2015-07 CHARACTERIZATION OF WASTE - PREPARATION OF TEST PORTIONS FROM THE LABORATORY SAMPLE
EN 15002:2015 Characterization of waste - Preparation of test portions from the laboratory sample
EN ISO 18772:2014 Soil quality - Guidance on leaching procedures for subsequent chemical and ecotoxicological testing of soils and soil materials (ISO 18772:2008)
EN 16457:2014 Characterization of waste - Framework for the preparation and application of a testing programme - Objectives, planning and report
13/30286658 DC : 0 BS EN 16660 - CHARACTERIZATION OF WASTE - LEACHING BEHAVIOUR TEST - DETERMINATION OF THE REDUCING CHARACTER AND THE REDUCING CAPACITY
DIN EN 16457 E : 2014 CHARACTERIZATION OF WASTE - FRAMEWORK FOR THE PREPARATION AND APPLICATION OF A TESTING PROGRAMME - OBJECTIVES, PLANNING AND REPORT
BS EN 16457:2014 Characterization of waste. Framework for the preparation and application of a testing programme. Objectives, planning and report
UNE-EN 16192:2012 Characterization of waste - Analysis of eluates
S.R. CEN/TS 16660:2015 CHARACTERIZATION OF WASTE - LEACHING BEHAVIOUR TEST - DETERMINATION OF THE REDUCING CHARACTER AND THE REDUCING CAPACITY
UNE-CEN/TR 16110:2011 IN Characterization of waste - Guidance on the use of ecotoxicity tests applied to waste
BS ISO 18772 : 2008 COR 2014 SOIL QUALITY - GUIDANCE ON LEACHING PROCEDURES FOR SUBSEQUENT CHEMICAL AND ECOTOXICOLOGICAL TESTING OF SOILS AND SOIL MATERIALS
I.S. EN ISO 18772:2014 SOIL QUALITY - GUIDANCE ON LEACHING PROCEDURES FOR SUBSEQUENT CHEMICAL AND ECOTOXICOLOGICAL TESTING OF SOILS AND SOIL MATERIALS (ISO 18772:2008)
UNI EN 16192 : 2012 CHARACTERIZATION OF WASTE - ANALYSIS OF ELUATES
DIN EN 15002 E : 2015 CHARACTERIZATION OF WASTE - PREPARATION OF TEST PORTIONS FROM THE LABORATORY SAMPLE
13/30286655 DC : 0 BS EN 15863 - CHARACTERIZATION OF WASTE - LEACHING BEHAVIOUR TEST FOR BASIC CHARACTERIZATION - DYNAMIC MONOLITHIC LEACHING TEST WITH PERIODIC LEACHANT RENEWAL, UNDER FIXED TEST CONDITIONS
BS EN 15002:2015 Characterization of waste. Preparation of test portions from the laboratory sample
CEN/TR 16098:2010 Construction products: Assessment of release of dangerous substances - Concept of horizontal testing procedures in support of requirements under the CPD
CEN/TS 15864:2015 Characterization of waste - Leaching behaviour test for basic characterization - Dynamic monolithic leaching test with continuous leachant renewal under conditions relevant for specified scenario(s)
CEN/TR 16110:2010 Characterization of waste - Guidance on the use of ecotoxicity tests applied to waste
CEN/TS 16660:2015 Characterization of waste - Leaching behaviour test - Determination of the reducing character and the reducing capacity
CEN ISO/TS 21268-3:2009 Soil quality - Leaching procedures for subsequent chemical and ecotoxicological testing of soil and soil materials - Part 3: Up-flow percolation test (ISO/TS 21268-3:2007)
EN 16192:2011 Characterization of waste - Analysis of eluates
CEN/TS 15863:2012 Characterisation of waste - Leaching behaviour test for basic characterisation - Dynamic monolithic leaching test with periodic leachant renewal, under fixed test conditions

PREN 14346 : DRAFT 2004 CHARACTERIZATION OF WASTE - CALCULATION OF DRY MATTER BY DETERMINATION OF DRY RESIDUE AND WATER CONTENT
ENV 12920 : 1997 CHARACTERIZATION OF WASTE - METHODOLOGY FOR THE DETERMINATION OF THE LEACHING BEHAVIOUR OF WASTE UNDER SPECIFIED CONDITIONS
ISO 11464:2006 Soil quality Pretreatment of samples for physico-chemical analysis
ISO 5667-3:2012 Water quality Sampling Part 3: Preservation and handling of water samples
EN 13370:2003 Characterization of waste - Analysis of eluates - Determination of Ammonium, AOX, conductivity, Hg, phenol index, TOC, easily liberatable CN-, F-
EN ISO 5667-3:2012 Water quality - Sampling - Part 3: Preservation and handling of water samples (ISO 5667-3:2012)
EN 12506:2003 Characterization of waste - Analysis of eluates - Determination of pH, As, Ba, Cd, Cl-, Co, Cr, Cr Vl, Cu, Mo, Ni, NO2-, Pb, total S, SO42-, V and Zn
NEN 7343 : 1995 LEACHING CHARACTERISTICS OF SOLID EARTHY AND STONY BUILDING AND WASTE MATERIALS - LEACHING TESTS - DETERMINATION OF THE LEACHING OF INORGANIC COMPONENTS FROM GRANULAR MATERIALS WITH THE COLUMN TEST

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