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EN 14105:2011

Superseded

Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

View Superseded by
superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

Fat and oil derivatives - Fatty Acid Methyl Esters (FAME) - Determination of free and total glycerol and mono-, di-, triglyceride contents

Superseded date

15-12-2020

Published date

27-04-2011

Foreword
1 Scope
2 Principle
3 Reagents
4 Apparatus
5 Preparation of solutions
6 Sampling
7 Procedure
8 Determination of results
9 Expression of results
10 Precision
11 Test report
Annex A (informative) - Sample chromatogram
Annex B (normative) - Calibration function calculation
Annex C (informative) - Worked example
Annex D (informative) - Results of the interlaboratory
        trial
Bibliography

The purpose of this European Standard is to determine the free glycerol and residual mono-, di- and triglyceride contents in fatty acid methyl esters (FAME) intended for addition to mineral oils. The total glycerol content is then calculated from the obtained results. This method is the reference method for the determination of the free glycerol content. Under the conditions described, the quantification limits are 0,001 % (m/m) for free glycerol, 0,10 % (m/m) for all glycerides (mono-, di- and tri-). This method is suitable for FAME prepared from rapeseed, sunflower, soybean, palm, animal oils and fats and mixture of them. It is not suitable for FAME produced from or containing coconut and palm kernel oils derivatives because of overlapping of different glyceride peaks.NOTE For the purposes of this European Standard, the term "% (m/m)" is used to represent respectively the mass fraction.WARNING - The use of this method may involve hazardous equipment, materials and operations. This method does not purport to address to all of the safety problems associated with its use, but it is the responsibility of the user to search and establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Committee
CEN/TC 307
DevelopmentNote
Supersedes PREN 14105. (08/2011)
DocumentType
Standard
PublisherName
Comite Europeen de Normalisation
Status
Superseded
SupersededBy

Standards Relationship
ONORM EN 14105 : 2011 Identical
DIN EN 14105:2011-07 Identical
NF EN 14105 : 2011 Identical
BS EN 14105:2011 Identical
SANS 54105 : 1ED 2007 Identical
UNI EN 14105 : 2011 Identical
NBN EN 14105 : 2011 Identical
UNE-EN 14105:2003 Identical
I.S. EN 14105:2011 Identical
NEN EN 14105 : 2011 Identical
NS EN 14105 : 2011 Identical
UNE-EN 14105:2011 Identical
PN EN 14105 : 2012 Identical
SN EN 14105 : 2011 Identical
SS-EN 14105 : 2011 Identical
GOST R EN 14105 : 2008 Identical
SANS 54105:2020 Identical

09/30205523 DC : 0 BS EN 14214 - AUTOMOTIVE FUELS - FATTY ACID METHYL ESTERS (FAME) FOR DIESEL ENGINES - REQUIREMENTS AND TEST METHODS
I.S. EN 14213:2003 HEATING FUELS - FATTY ACID METHYL ESTERS (FAME) - REQUIREMENTS AND TEST METHODS
BS EN 14214:2012 LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS
DIN EN 14214:2014-06 LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS
DIN EN 14214 E : 2003 LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS
I.S. EN 14214:2012 LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS
UNI EN 14214 : 2014 LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS
EN 14214:2012+A1:2014/AC:2014 LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS
PREN 14214 : DRAFT 2009 AUTOMOTIVE FUELS - FATTY ACID METHYL ESTERS (FAME) FOR DIESEL ENGINES - REQUIREMENTS AND TEST METHODS
PD ISO/TS 17306:2016 Petroleum products. Biodiesel. Determination of free and total glycerin and mono-, di- and tracylglycerols by gas chromatography
BS EN 14213:2003 Heating fuels. Fatty acid methyl esters (FAME). Requirements and test methods
EN 14213:2003/AC:2003 HEATING FUELS - FATTY ACID METHYL ESTERS (FAME) - REQUIREMENTS AND TEST METHODS
13/30280877 DC : 0 BS ISO 17306 - PETROLEUM PRODUCTS - BIODIESEL - DETERMINATION OF FREE AND TOTALGLYCERIN AND MONO-, DI- AND TRACYLGLYCEROLS BY GAS CHROMATOGRAPHY
UNE-EN 14214:2013 Liquid petroleum products - Fatty acid methyl esters (FAME) for use in diesel engines and heating applications - Requirements and test methods
ISO/TS 17306:2016 Petroleum products — Biodiesel — Determination of free and total glycerin and mono-, di- and tracylglycerols by gas chromatography
DIN EN 14213 E : 2003 HEATING FUELS - FATTY ACID METHYL ESTERS (FAME) - REQUIREMENTS AND TEST METHODS
DIN EN 14214:2003-11 LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS
DIN EN 14213:2003-11 HEATING FUELS - FATTY ACID METHYL ESTERS (FAME) - REQUIREMENTS AND TEST METHODS

ISO 5555:2001 Animal and vegetable fats and oils — Sampling
ISO 3170:2004 Petroleum liquids — Manual sampling
ISO 4259:2006 Petroleum products Determination and application of precision data in relation to methods of test
EN ISO 3170:2004 Petroleum liquids - Manual sampling (ISO 3170:2004)
EN ISO 4259:2006 Petroleum products - Determination and application of precision data in relation to methods of test (ISO 4259:2006)

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