EN 15934:2012
Current
Current
The latest, up-to-date edition.
Sludge, treated biowaste, soil and waste - Calculation of dry matter fraction after determination of dry residue or water content
Published date
22-08-2012
Publisher
Foreword
Introduction
1 Scope
2 Normative references
3 Terms and definitions
4 Principle
5 Sample preparation
6 Method A - Drying at 105 degrees C
7 Method B - Direct Karl-Fischer-titration
(volumetric/coulometric detection)
8 Calculation of dry matter fraction
9 Precision
10 Test report
Annex A (informative) - Repeatability and reproducibility
Annex B (informative) - Azeotropic distillation with toluene
Annex C (informative) - Summary of general requirements
and recommendations
This European Standard specifies methods for the calculation of the dry matter of sludge, treated biowaste, soil and waste for which the results of performed analysis are to be calculated to the dry matter basis. Depending on the nature and origin of the sample, the calculation is based on a determination of the dry residue (Method A) or a determination of the water content (Method B). It applies to samples containing more than 1 % (mass fraction) of dry residue or more than 1 % (mass fraction) of water.Method A applies to sludge, treated biowaste, soil and solid waste, Method B applies to liquid waste and to samples which are suspected or known to contain volatiles except for water.
| Committee |
CEN/TC 444
|
| DevelopmentNote |
Supersedes PREN 15934. (09/2012)
|
| DocumentType |
Standard
|
| PublisherName |
Comite Europeen de Normalisation
|
| Status |
Current
|
| Standards | Relationship |
| DIN EN 15934:2012-11 | Identical |
| DIN EN 15934 E : 2012 | Identical |
| NEN EN 15934 : 2012 | Identical |
| I.S. EN 15934:2012 | Identical |
| UNE-EN 15934:2012 | Identical |
| PN EN 15934 : 2013 | Identical |
| SN EN 15934:2012 | Identical |
| NF EN 15934 : 2012 | Identical |
| NBN EN 15934 : 2012 | Identical |
| NS EN 15934 : 2012 | Identical |
| BS EN 15934:2012 | Identical |
| UNI EN 15934 : 2012 | Identical |
| S.R. CEN/TS 16171:2012 | SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF ELEMENTS USING INDUCTIVELY COUPLED PLASMA MASS SPECTROMETRY (ICP-MS) |
| ISO 18187:2016 | Soil quality Contact test for solid samples using the dehydrogenase activity of Arthrobacter globiformis |
| BS ISO 16729:2013 | Soil quality. Digestion of nitric acid soluble fractions of elements |
| S.R. CEN/TS 16170:2012 | SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF ELEMENTS USING INDUCTIVELY COUPLED PLASMA OPTICAL EMISSION SPECTROMETRY (ICP-OES) |
| PD CEN/TR 16193:2013 | Sludge, treated biowaste and soil. Detection and enumeration of Escherichia coli |
| DIN EN 15936 E : 2012 | SLUDGE, TREATED BIOWASTE, SOIL AND WASTE - DETERMINATION OF TOTAL ORGANIC CARBON (TOC) BY DRY COMBUSTION |
| S.R. CEN/TR 16193:2013 | SLUDGE, TREATED BIOWASTE AND SOIL - DETECTION AND ENUMERATION OF ESCHERICHIA COLI |
| I.S. EN 15936:2012 | SLUDGE, TREATED BIOWASTE, SOIL AND WASTE - DETERMINATION OF TOTAL ORGANIC CARBON (TOC) BY DRY COMBUSTION |
| EN ISO 18187:2018 | Soil quality - Contact test for solid samples using the dehydrogenase activity of Arthrobacter globiformis (ISO 18187:2016) |
| DIN EN 16167:2012-11 | SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF POLYCHLORINATED BIPHENYLS (PCB) BY GAS CHROMATOGRAPHY WITH MASS SELECTIVE DETECTION (GC-MS) AND GAS CHROMATOGRAPHY WITH ELECTRON-CAPTURE DETECTION (GC-ECD) |
| 17/30363999 DC : 0 | BS EN 16190 - SOIL, TREATED BIOWASTE AND SLUDGE - DETERMINATION OF DIOXINS AND FURANS AND DIOXIN-LIKE POLYCHLORINATED BIPHENYLS BY GAS CHROMATOGRAPHY WITH HIGH RESOLUTION MASS SELECTIVE DETECTION (HR GC-MS) |
| 17/30364005 DC : 0 | BS EN 16181 - SOIL, TREATED BIOWASTE AND SLUDGE - DETERMINATION OF POLYCYCLIC AROMATIC HYDROCARBONS (PAH) BY GAS CHROMATOGRAPHY (GC) AND HIGH PERFORMANCE LIQUID CHROMATOGRAPHY (HPLC) |
| CEN/TS 16171:2012 | Sludge, treated biowaste and soil - Determination of elements using inductively coupled plasma mass spectrometry (ICP-MS) |
| CEN/TS 16172:2013 | Sludge, treated biowaste and soil - Determination of elements using graphite furnace atomic absorption spectrometry (GF-AAS) |
| EN 16175-2:2016 | Sludge, treated biowaste and soil - Determination of mercury - Part 2: Cold-vapour atomic fluorescence spectrometry (CV-AFS) |
| DIN EN 15935:2012-11 | Sludge, treated biowaste, soil and waste - Determination of loss on ignition; German version EN 15935:2012 |
| CEN/TS 16175-1:2013 | Sludge, treated biowaste and soil - Determination of mercury - Part 1: Cold-vapour atomic absorption spectrometry (CV-AAS) |
| DIN EN 15936:2012-11 | Sludge, treated biowaste, soil and waste - Determination of total organic carbon (TOC) by dry combustion |
| BS EN 16179:2012 | Sludge, treated biowaste and soil. Guidance for sample pretreatment |
| UNI CEN/TS 16170 : 2013 | SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF ELEMENTS USING INDUCTIVELY COUPLED PLASMA OPTICAL EMISSION SPECTROMETRY (ICP-OES) |
| UNI EN 16169 : 2012 | SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF KJELDAHL NITROGEN |
| I.S. EN 16173:2012 | SLUDGE, TREATED BIOWASTE AND SOIL - DIGESTION OF NITRIC ACID SOLUBLE FRACTIONS OF ELEMENTS |
| I.S. EN ISO 18187:2018 | SOIL QUALITY - CONTACT TEST FOR SOLID SAMPLES USING THE DEHYDROGENASE ACTIVITY OF ARTHROBACTER GLOBIFORMIS (ISO 18187:2016) |
| PREN 16190 : DRAFT 2017 | SOIL, TREATED BIOWASTE AND SLUDGE - DETERMINATION OF DIOXINS AND FURANS AND DIOXIN-LIKE POLYCHLORINATED BIPHENYLS BY GAS CHROMATOGRAPHY WITH HIGH RESOLUTION MASS SELECTIVE DETECTION (HR GC-MS) |
| S.R. CEN/TS 16181:2013 | SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF POLYCYCLIC AROMATIC HYDROCARBONS (PAH) BY GAS CHROMATOGRAPHY (GC) AND HIGH PERFORMANCE LIQUID CHROMATOGRAPHY (HPLC) |
| VDI 3957 Blatt 2:2016-03 | Biological measuring techniques for the determination and assessment of effects of air pollutants on plants (biomonitoring) - Method of the standardised grass exposure |
| ISO 13913:2014 | Soil quality Determination of selected phthalates using capillary gas chromatography with mass spectrometric detection (GC/MS) |
| BS EN 16175-2:2016 | Sludge, treated biowaste and soil. Determination of mercury Cold-vapour atomic fluorescence spectrometry (CV-AFS) |
| BS EN 16166:2012 | Sludge, treated biowaste and soil. Determination of adsorbable organically bound halogens (AOX) |
| BS EN 15935:2012 | Sludge, treated biowaste, soil and waste. Determination of loss on ignition |
| UNI EN 15936 : 2012 | SLUDGE, TREATED BIOWASTE, SOIL AND WASTE - DETERMINATION OF TOTAL ORGANIC CARBON (TOC) BY DRY COMBUSTION |
| UNI CEN/TS 16172 : 2013 | SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF ELEMENTS USING GRAPHITE FURNACE ATOMIC ABSORPTION SPECTROMETRY (GF-AAS) |
| BS ISO 18187 : 2016 | SOIL QUALITY - CONTACT TEST FOR SOLID SAMPLES USING THE DEHYDROGENASE ACTIVITY OF ARTHROBACTER GLOBIFORMIS |
| UNI EN 16167 : 2012 | SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF POLYCHLORINATED BIPHENYLS (PCB) BY GAS CHROMATOGRAPHY WITH MASS SELECTIVE DETECTION (GC-MS) AND GAS CHROMATOGRAPHY WITH ELECTRON-CAPTURE DETECTION (GC-ECD) |
| UNI CEN/TS 16189 : 2012 | SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF LINEAR ALKYLBENZENE SULFONATES (LAS) BY HIGH-PERFORMANCE LIQUID CHROMATOGRAPHY (HPLC) WITH FLUORESCENCE DETECTION (FLD) OR MASS SELECTIVE DETECTION (MS) |
| DIN EN 16173:2012-11 | SLUDGE, TREATED BIOWASTE AND SOIL - DIGESTION OF NITRIC ACID SOLUBLE FRACTIONS OF ELEMENTS |
| I.S. EN 16167:2012 | SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF POLYCHLORINATED BIPHENYLS (PCB) BY GAS CHROMATOGRAPHY WITH MASS SELECTIVE DETECTION (GC-MS) AND GAS CHROMATOGRAPHY WITH ELECTRONCAPTURE DETECTION (GC-ECD) |
| I.S. EN 16166:2012 | SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF ADSORBABLE ORGANICALLY BOUND HALOGENS (AOX) |
| I.S. EN 15935:2012 | SLUDGE, TREATED BIOWASTE, SOIL AND WASTE - DETERMINATION OF LOSS ON IGNITION |
| EN 15935:2012 | Sludge, treated biowaste, soil and waste - Determination of loss on ignition |
| I.S. EN 16168:2012 | SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF TOTAL NITROGEN USING DRY COMBUSTION METHOD |
| 17/30364002 DC : 0 | BS EN 16167 - SOIL, TREATED BIOWASTE AND SLUDGE - DETERMINATION OF POLYCHLORINATED BIPHENYLS (PCB) BY GAS CHROMATOGRAPHY WITH MASS SELECTIVE DETECTION (GC-MS) AND GAS CHROMATOGRAPHY WITH ELECTRON-CAPTURE DETECTION (GC-ECD) |
| I.S. EN 16175-1:2016 | SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF MERCURY - PART 1: COLD-VAPOUR ATOMIC ABSORPTION SPECTROMETRY (CV-AAS) |
| UNE-EN 16179:2013 | Sludge, treated biowaste and soil - Guidance for sample pretreatment |
| UNI EN 16179 : 2012 | SLUDGE, TREATED BIOWASTE AND SOIL - GUIDANCE FOR SAMPLE PRETREATMENT |
| UNI CEN/TS 16171 : 2013 | SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF ELEMENTS USING INDUCTIVELY COUPLED PLASMA MASS SPECTROMETRY (ICP-MS) |
| UNI EN 16168 : 2012 | SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF TOTAL NITROGEN USING DRY COMBUSTION METHOD |
| UNI CEN/TS 16181 : 2013 | SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF POLYCYCLIC AROMATIC HYDROCARBONS (PAH) BY GAS CHROMATOGRAPHY (GC) AND HIGH PERFORMANCE LIQUID CHROMATOGRAPHY (HPLC) |
| BS EN ISO 18187:2018 | Soil quality. Contact test for solid samples using the dehydrogenase activity of Arthrobacter globiformis |
| 17/30362321 DC : 0 | BS EN ISO 23161 - SOIL QUALITY - DETERMINATION OF SELECTED ORGANOTIN COMPOUNDS - GAS-CHROMATOGRAPHIC METHOD |
| BS EN 15936:2012 | Sludge, treated biowaste, soil and waste. Determination of total organic carbon (TOC) by dry combustion |
| DIN EN 16169:2012-11 | SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF KJELDAHL NITROGEN |
| S.R. CEN/TS 16172:2013 | SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF ELEMENTS USING GRAPHITE FURNACE ATOMIC ABSORPTION SPECTROMETRY (GF-AAS) |
| S.R. CEN/TS 16175-2:2013 | SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF MERCURY - PART 2: COLD-VAPOUR ATOMIC FLUORESCENCE SPECTROMETRY (CV-AFS) |
| DIN EN 16168:2012-11 | Sludge, treated biowaste and soil - Determination of total nitrogen using dry combustion method; German version EN 16168:2012 |
| UNI CEN/TS 16182 : 2012 | SLUDGE TREATED BIOWASTE AND SOIL - DETERMINATION OF NONYLPHENOLS (NP) AND NONYLPHENOL-MONO- AND DIETHOXYLATES USING GAS CHROMATOGRAPHY WITH MASS SELECTIVE DETECTION (GCMS) |
| I.S. EN 16169:2012 | SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF KJELDAHL NITROGEN |
| I.S. EN 16171:2016 | SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF ELEMENTS USING INDUCTIVELY COUPLED PLASMA MASS SPECTROMETRY (ICP-MS) |
| PREN 16167 : DRAFT 2017 | SOIL, TREATED BIOWASTE AND SLUDGE - DETERMINATION OF POLYCHLORINATED BIPHENYLS (PCB) BY GAS CHROMATOGRAPHY WITH MASS SELECTIVE DETECTION (GC-MS) AND GAS CHROMATOGRAPHY WITH ELECTRON-CAPTURE DETECTION (GC-ECD) |
| EN 16169:2012 | Sludge, treated biowaste and soil - Determination of Kjeldahl nitrogen |
| EN 16179:2012 | Sludge, treated biowaste and soil - Guidance for sample pretreatment |
| EN 16168:2012 | Sludge, treated biowaste and soil - Determination of total nitrogen using dry combustion method |
| EN 16173:2012 | Sludge, treated biowaste and soil - Digestion of nitric acid soluble fractions of elements |
| EN 15936:2012 | Sludge, treated biowaste, soil and waste - Determination of total organic carbon (TOC) by dry combustion |
| BS EN 16168:2012 | Sludge, treated biowaste and soil. Determination of total nitrogen using dry combustion method |
| DIN EN 15935 E : 2012 | SLUDGE, TREATED BIOWASTE, SOIL AND WASTE - DETERMINATION OF LOSS ON IGNITION |
| UNI CEN/TS 16183 : 2012 | SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF SELECTED PHTHALATES USING CAPILLARY GAS CHROMATOGRAPHY WITH MASS SPECTROMETRIC DETECTION (GC-MS) |
| BS EN 16169:2012 | Sludge, treated biowaste and soil. Determination of Kjeldahl nitrogen |
| UNI EN 16173 : 2012 | SLUDGE, TREATED BIOWASTE AND SOIL - DIGESTION OF NITRIC ACID SOLUBLE FRACTIONS OF ELEMENTS |
| DIN EN 16179:2012-11 | Sludge, treated biowaste and soil - Guidance for sample pretreatment |
| BS EN 16173:2012 | Sludge, treated biowaste and soil. Digestion of nitric acid soluble fractions of elements |
| DIN EN 16166:2012-11 | Sludge, treated biowaste and soil - Determination of adsorbable organically bound halogens (AOX) |
| BS ISO 13913:2014 | Soil quality. Determination of selected phthalates using capillary gas chromatography with mass spectrometric detection (GC/MS) |
| UNI EN 15935 : 2012 | SLUDGE, TREATED BIOWASTE, SOIL AND WASTE - DETERMINATION OF LOSS ON IGNITION |
| I.S. EN 16179:2012 | SLUDGE, TREATED BIOWASTE AND SOIL - GUIDANCE FOR SAMPLE PRETREATMENT |
| I.S. EN 16170:2016 | SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF ELEMENTS USING INDUCTIVELY COUPLED PLASMA OPTICAL EMISSION SPECTROMETRY (ICP-OES) |
| I.S. EN 16175-2:2016 | SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF MERCURY - PART 2: COLD-VAPOUR ATOMIC FLUORESCENCE SPECTROMETRY (CV-AFS) |
| S.R. CEN/TS 16175-1:2013 | SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF MERCURY - PART 1: COLD-VAPOUR ATOMIC ABSORPTION SPECTROMETRY (CV-AAS) |
| EN 16167:2012 | Sludge, treated biowaste and soil - Determination of polychlorinated biphenyls (PCB) by gas chromatography with mass selective detection (GC-MS) and gas chromatography with electron-capture detection (GC-ECD) |
| CEN/TR 16193:2013 | Sludge, treated biowaste and soil - Detection and enumeration of Escherichia coli |
| ISO 16729:2013 | Soil quality Digestion of nitric acid soluble fractions of elements |
| CEN/TS 16181:2013 | Sludge, treated biowaste and soil - Determination of polycyclic aromatic hydrocarbons (PAH) by gas chromatography (GC) and high performance liquid chromatography (HPLC) |
| CEN/TS 16175-2:2013 | Sludge, treated biowaste and soil - Determination of mercury - Part 2: Cold-vapour atomic fluorescence spectrometry (CV-AFS) |
| UNI EN 16166 : 2012 | SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF ADSORBABLE ORGANICALLY BOUND HALOGENS (AOX) |
| CEN/TS 16170:2012 | Sludge, treated biowaste and soil - Determination of elements using inductively coupled plasma optical emission spectrometry (ICP-OES) |
| EN 16166:2012 | Sludge, treated biowaste and soil - Determination of adsorbable organically bound halogens (AOX) |
| EN 15002:2015 | Characterization of waste - Preparation of test portions from the laboratory sample |
| EN 16179:2012 | Sludge, treated biowaste and soil - Guidance for sample pretreatment |
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