Name: EN 16694 : 2015
Brand: CEN

WATER QUALITY - DETERMINATION OF SELECTED POLYBROMINATED DIPHENLY ETHER (PBDE) IN WHOLE WATER SAMPLES - METHOD USING SOLID PHASE EXTRACTION (SPE) WITH SPE-DISKS COMBINED WITH GAS CHROMATOGRAPHY - MASS SPECTROMETRY (GC-MS)

Published date

23-09-2015

Publisher

Comite Europeen de Normalisation

European foreword
Introduction
1 Scope
2 Normative references
3 Principle
4 Interferences
5 Reagents
6 Apparatus
7 Sampling
8 Procedure
9 Calibration
10 Quantification
11 Expression of results
12 Test report
Annex A (informative) - Suitable gas chromatographic
conditions and example chromatograms
Annex B (informative) - Repeatability and reproducibility data
Annex C (informative) - Examples of suitable solid phase
extraction disks
Annex D (informative) - Clean up procedure
Bibliography

This European Standard specifies a method for the determination of six selected polybrominated diphenyl ethers (PBDEs) listed in Table 1, representative for technical BDEs in water samples in mass concentrations ≥ 0,025 ng/l (for each individual congener).

Committee	CEN/TC 230
DevelopmentNote	Supersedes PREN 16694. (09/2015)
DocumentType	Standard
PublisherName	Comite Europeen de Normalisation
Status	Current

Standards	Relationship
SN EN 16694 : 2015	Identical
BS EN 16694:2015	Identical
NEN EN 16694 : 2015	Identical
NBN EN 16694 : 2015	Identical
I.S. EN 16694:2015	Identical
NF EN 16694 : 2015	Identical
DIN EN 16694:2015-12	Identical
UNI EN 16694 : 2015	Identical
PN EN 16694 : 2016	Identical
NS EN 16694 : 2015	Identical
UNE-EN 16694:2016	Identical
DIN EN 16694 E : 2015	Identical

EN 16377:2013	Characterization of waste - Determination of brominated flame retardants (BFR) in solid waste
ISO/TS 13530:2009	Water quality — Guidance on analytical quality control for chemical and physicochemical water analysis
ISO 22892:2006	Soil quality Guidelines for the identification of target compounds by gas chromatography and mass spectrometry
ISO 5667-3:2012	Water quality Sampling Part 3: Preservation and handling of water samples
ISO 5667-1:2006	Water quality Sampling Part 1: Guidance on the design of sampling programmes and sampling techniques
EN ISO 22032:2009	Water quality - Determination of selected polybrominated diphenyl ethers in sediment and sewage sludge - Method using extraction and gas chromatography/mass spectrometry (ISO 22032:2006)
ISO 5725-2:1994	Accuracy (trueness and precision) of measurement methods and results Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method
ISO 22032:2006	Water quality — Determination of selected polybrominated diphenyl ethers in sediment and sewage sludge — Method using extraction and gas chromatography/mass spectrometry
EN ISO 5667-3:2012	Water quality - Sampling - Part 3: Preservation and handling of water samples (ISO 5667-3:2012)
ISO 3696:1987	Water for analytical laboratory use — Specification and test methods
ISO 8466-1:1990	Water quality Calibration and evaluation of analytical methods and estimation of performance characteristics Part 1: Statistical evaluation of the linear calibration function
EN ISO 3696:1995	Water for analytical laboratory use - Specification and test methods (ISO 3696:1987)
EN ISO 22892:2011	Soil quality - Guidelines for the identification of target compounds by gas chromatography and mass spectrometry (ISO 22892:2006)
EN ISO 5667-1 : 2006 COR 2007	WATER QUALITY - SAMPLING - PART 1: GUIDANCE ON THE DESIGN OF SAMPLING PROGRAMMES AND SAMPLING TECHNIQUES