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EN ISO 22155:2016

Current
Current

The latest, up-to-date edition.

Soil quality - Gas chromatographic determination of volatile aromatic and halogenated hydrocarbons and selected ethers - Static headspace method (ISO 22155:2016)
Published date

16-03-2016

European foreword
Foreword
1 Scope
2 Normative references
3 Principle
4 Reagents
5 Apparatus
6 Sampling, preservation, and sample pretreatment
7 Procedure
8 Calculation
9 Expression of results
10 Precision
11 Test report
Annex A (informative) - Relative retention times with
        respect to ethylbenzene-D10 of volatile aromatic
        hydrocarbons and volatile halogenated
        hydrocarbons - Examples of suitable target
        and qualifier ions
Annex B (normative) - Check on internal standards
Annex C (informative) - Validation (general)
Annex D (informative) - Performance characteristics
Bibliography

ISO 22155:2016 specifies a static headspace method for quantitative gas chromatographic determination of volatile aromatic and halogenated hydrocarbons and selected aliphatic ethers in soil.ISO 22155:2016 is applicable to all types of soil.The limit of quantification is dependent on the detection system used and the quality of the methanol grade used for the extraction of the soil sample.Under the conditions specified in this International Standard, the following limits of quantifications apply (expressed on basis of dry matter).Typical limit of quantification when using GC-FID:- volatile aromatic hydrocarbons: 0,2 mg/kg;- aliphatic ethers as methyl tert.-butyl ether(MTBE) and tert.-amyl methyl ether (TAME): 0,5 mg/kg.Typical limit of quantification when using GC-ECD:- volatile halogenated hydrocarbons: 0,01 mg/kg to 0,2 mg/kg.Lower limits of quantification for some compounds can be achieved by using mass spectrometry (MS) with selected ion detection (see Annex D).

Committee
CEN/TC 444
DocumentType
Standard
PublisherName
Comite Europeen de Normalisation
Status
Current

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ISO 15009:2016 Soil quality Gas chromatographic determination of the content of volatile aromatic hydrocarbons, naphthalene and volatile halogenated hydrocarbons Purge-and-trap method with thermal desorption
ISO 10381-1:2002 Soil quality Sampling Part 1: Guidance on the design of sampling programmes
ISO 22892:2006 Soil quality Guidelines for the identification of target compounds by gas chromatography and mass spectrometry
ISO 10381-2:2002 Soil quality Sampling Part 2: Guidance on sampling techniques
ISO 10301:1997 Water quality — Determination of highly volatile halogenated hydrocarbons — Gas-chromatographic methods
ISO 14507:2003 Soil quality Pretreatment of samples for determination of organic contaminants
ISO 15680:2003 Water quality Gas-chromatographic determination of a number of monocyclic aromatic hydrocarbons, naphthalene and several chlorinated compounds using purge-and-trap and thermal desorption
ISO 5725-5:1998 Accuracy (trueness and precision) of measurement methods and results — Part 5: Alternative methods for the determination of the precision of a standard measurement method
ISO 18512:2007 Soil quality Guidance on long and short term storage of soil samples

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