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EN ISO 5509 : 2000

Superseded
Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

View Superseded by
superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

ANIMAL AND VEGETABLE FATS AND OILS - PREPARATION OF METHYL ESTER OF FATTY ACIDS
Superseded date

01-02-2011

Published date

12-01-2013

Foreword
Introduction
1 Scope
2 Normative references
3 General method using boron trifluoride
4 Trimethylsulfonium hydroxide (TMSH) method
5 Trans-esterification method
6 Precision
Annex A (normative) General analytical procedures
Annex B (informative) Results of interlaboratory test
Annex ZA (normative) Normative references to international
         publications with their relevant European publications
Bibliography

Specifies methods of preparing the methyl esters of fatty acids. It includes methods for preparing fatty acid methyl esters from animal and vegetable fats and oils, fatty acids and soaps. To cover different requirements, three methylation methods are specified, as follows: a) boron trifluoride(BF3) method; b) trimethylsulfonium hydroxide(TMSH) method; c) trans-esterification method.

Committee
TC 307
DocumentType
Standard
PublisherName
Comite Europeen de Normalisation
Status
Superseded
SupersededBy

UNE-EN 15779:2010 Petroleum products and fat and oil derivates - Fatty acid methyl esters (FAME) for diesel engines - Determination of polyunsaturated (>= 4 double bonds) fatty acid methyl esters (PUFA) by gas chromatography
I.S. EN ISO 15304:2002 ANIMAL AND VEGETABLE FATS AND OILS - DETERMINATION OF THE CONTENT OF TRANS FATTY ACID ISOMERS OF VEGETABLE FATS AND OIL - GAS CHROMATOGRAPHIC METHOD
UNI EN 15779 : 2013 PETROLEUM PRODUCTS AND FAT AND OIL DERIVATES - FATTY ACID METHYL ESTERS (FAME) FOR DIESEL ENGINES - DETERMINATION OF POLYUNSATURATED (>=4 DOUBLE BONDS) FATTY ACID METHYL ESTERS (PUFA) BY GAS CHROMATOGRAPHY
08/30176795 DC : DRAFT APR 2008 BS EN 15779 - FATS AND OIL DERIVATES - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES - DETERMINATION OF POLY-UNSATURATED FATTY ACID METHYL ESTERS BY GAS CHROMATOGRAPHY
DIN EN 15779:2013-12 Petroleum products and fat and oil derivates - Fatty acid methyl esters (FAME) for diesel engines - Determination of polyunsaturated (<groesser
DIN EN 15779 E : 2013 PETROLEUM PRODUCTS AND FAT AND OIL DERIVATES - FATTY ACID METHYL ESTERS (FAME) FOR DIESEL ENGINES - DETERMINATION OF POLYUNSATURATED (>/= 4 DOUBLE BONDS) FATTY ACID METHYL ESTERS (PUFA) BY GAS CHROMATOGRAPHY
EN ISO 15304:2002/AC:2004 ANIMAL AND VEGETABLE FATS AND OILS - DETERMINATION OF THE CONTENT OF TRANS FATTY ACID ISOMERS OF VEGETABLE FATS AND OIL - GAS CHROMATOGRAPHIC METHOD
I.S. EN 15779:2009 PETROLEUM PRODUCTS AND FAT AND OIL DERIVATES - FATTY ACID METHYL ESTERS (FAME) FOR DIESEL ENGINES - DETERMINATION OF POLYUNSATURATED (>=4 DOUBLE BONDS) FATTY ACID METHYL ESTERS (PUFA) BY GAS CHROMATOGRAPHY
BS EN 15779 : 2009 PETROLEUM PRODUCTS AND FAT AND OIL DERIVATES - FATTY ACID METHYL ESTERS (FAME) FOR DIESEL ENGINES - DETERMINATION OF POLYUNSATURATED (>= 4 DOUBLE BONDS) FATTY ACID METHYL ESTERS (PUFA) BY GAS CHROMATOGRAPHY
ISO 15304:2002 Animal and vegetable fats and oils Determination of the content of trans fatty acid isomers of vegetable fats and oils Gas chromatographic method
BS EN ISO 15304:2002 Animal and vegetable fats and oils. Determination of the content of trans fatty acid isomers of vegetable fats and oil. Gas chromatographic method
EN 15779:2009+A1:2013 Petroleum products and fat and oil derivates - Fatty acid methyl esters (FAME) for diesel engines - Determination of polyunsaturated (≥4 double bonds) fatty acid methyl esters (PUFA) by gas chromatography
BS 2000-578(2009) : 2009 PETROLEUM PRODUCTS AND FAT AND OIL DERIVATES - FATTY ACID METHYL ESTERS (FAME) FOR DIESEL ENGINES - DETERMINATION OF POLYUNSATURATED (>= 4 DOUBLE BONDS) FATTY ACID METHYL ESTERS (PUFA) BY GAS CHROMATOGRAPHY
IP 578 : 2015 PETROLEUM PRODUCTS AND FAT AND OIL DERIVATES - FATTY ACID METHYL ESTERS (FAME) FOR DIESEL ENGINES - DETERMINATION OF POLYUNSATURATED (>= 4 DOUBLE BONDS) FATTY ACID METHYL ESTERS (PUFA) BY GAS CHROMATOGRAPHY
DIN EN ISO 13884:2005-11 Animal and vegetable fats and oils - Determination of isolated trans isomers by infrared spectrometry (ISO 13884:2003)

EN ISO 661:2005/AC:2006 ANIMAL AND VEGETABLE FATS AND OILS - PREPARATION OF TEST SAMPLE
ISO 3696:1987 Water for analytical laboratory use — Specification and test methods
ISO 661:2003 Animal and vegetable fats and oils Preparation of test sample
EN ISO 3696:1995 Water for analytical laboratory use - Specification and test methods (ISO 3696:1987)

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