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PREN 14582 : DRAFT 2015

Superseded
Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

View Superseded by
superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

CHARACTERIZATION OF WASTE - HALOGEN AND SULFUR CONTENT - OXYGEN COMBUSTION IN CLOSED SYSTEMS AND DETERMINATION METHODS
Superseded date

01-08-2016

Published date

06-07-2015

Foreword
Introduction
1 Scope
2 Normative references
3 Terms and definitions
4 Principle
5 Interferences
6 Hazards
7 Reagents and control mixtures
8 Sample conservation and pre-treatment
   of test portion
9 Equipment
10 Procedure
11 Recommended methods of determination
12 Control measurements
13 Evaluation
14 Test report
Annex A (informative) - Performance characteristics
Annex B (informative) - Oxygen flask combustion
        by Schoeniger
Annex C (informative) - Recovery yields obtained
        for control mixtures with different absorption
        solutions and analytical techniques
Annex D (informative) - Examples of possible
        control substances
Annex E (informative) - Additional results of
        inter-laboratory tests
Annex F (informative) - Summary of
         general requirements and recommendations
Annex G (informative) - Additional validation data
Bibliography

Defines a combustion method for the determination of halogen and sulfur contents in materials by combustion in a closed system containing oxygen (calorimetric bomb), and the subsequent analysis of the combustion product using different analytical techniques.

Committee
TC 292
DocumentType
Draft
PublisherName
Comite Europeen de Normalisation
Status
Superseded
SupersededBy

I.S. CEN TS 15289:2006 SOLID BIOFUELS - DETERMINATION OF TOTAL CONTENT OF SULPHUR AND CHLORINE
CEN/TS 15289:2006 Solid Biofuels - Determination of total content of sulphur and chlorine
DD CEN/TS 15289:2006 Solid biofuels. Determination of total content of sulphur and chlorine

EN ISO 11885:2009 Water quality - Determination of selected elements by inductively coupled plasma optical emission spectrometry (ICP-OES) (ISO 11885:2007)
EN ISO 10304-3 : 1997 Water quality - Determination of dissolved anions by liquid chromatography of ions - Part 3: Determination of chromate, iodide, sulfite, thiocyanate and thiosulfate (ISO 10304-3:1997)
ASTM D 808 : 2016 : REDLINE Standard Test Method for Chlorine in New and Used Petroleum Products (High Pressure Decomposition Device Method)
ISO 10304-3:1997 Water quality — Determination of dissolved anions by liquid chromatography of ions — Part 3: Determination of chromate, iodide, sulfite, thiocyanate and thiosulfate
EN 14346:2006 CHARACTERIZATION OF WASTE - CALCULATION OF DRY MATTER BY DETERMINATION OF DRY RESIDUE OR WATER CONTENT
ISO 9297:1989 Water quality Determination of chloride Silver nitrate titration with chromate indicator (Mohr's method)
ISO 11885:2007 Water quality Determination of selected elements by inductively coupled plasma optical emission spectrometry (ICP-OES)
ISO 10304-1:2007 Water quality Determination of dissolved anions by liquid chromatography of ions Part 1: Determination of bromide, chloride, fluoride, nitrate, nitrite, phosphate and sulfate
ISO 10359-1:1992 Water quality — Determination of fluoride — Part 1: Electrochemical probe method for potable and lightly polluted water
ISO 3696:1987 Water for analytical laboratory use — Specification and test methods
EN ISO 3696:1995 Water for analytical laboratory use - Specification and test methods (ISO 3696:1987)
EN 15002:2015 Characterization of waste - Preparation of test portions from the laboratory sample
ASTM E 442 : 1991 Test Method for Chlorine, Bromine, or Iodine in Organic Compounds by Oxygen Flask Combustion (Withdrawn 1997)
EN ISO 10304-1:2009 Water quality - Determination of dissolved anions by liquid chromatography of ions - Part 1: Determination of bromide, chloride, fluoride, nitrate, nitrite, phosphate and sulfate (ISO 10304-1:2007)

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