Name: UNI EN 16167 : 2012
Brand: UNI

UNI EN 16167 : 2012

Superseded

SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF POLYCHLORINATED BIPHENYLS (PCB) BY GAS CHROMATOGRAPHY WITH MASS SELECTIVE DETECTION (GC-MS) AND GAS CHROMATOGRAPHY WITH ELECTRON-CAPTURE DETECTION (GC-ECD)

Superseded date

20-09-2018

Published date

01-01-2012

Publisher

Ente Nazionale Italiano di Unificazione (UNI)

Foreword
Introduction
1 Scope
2 Normative references
3 Terms and definitions
4 Principle
5 Interferences
6 Safety remarks
7 Reagents
8 Apparatus
9 Sample storage and preservation
10 Procedure
11 Performance characteristics
12 Precision
13 Test report
Annex A (informative) - Repeatability and
reproducibility data
Annex B (informative) - Examples for retention
times of PCBs
Bibliography

Defines a method for quantitative determination of seven selected polychlorinated biphenyls (PCB28, PCB52, PCB101, PCB118, PCB138, PCB153 and PCB180) in sludge and treated biowaste using GC-MS and GC-ECD.

DocumentType	Standard
PublisherName	Ente Nazionale Italiano di Unificazione (UNI)
Status	Superseded
SupersededBy	UNI EN 16167:2018

Standards	Relationship
EN 16167:2012	Identical

EN ISO 6468 : 1996	WATER QUALITY - DETERMINATION OF CERTAIN ORGANOCHLORINE INSECTICIDES, POLYCHLORINATED BIPHENYLS AND CHLOROBENZENES - GAS CHROMATOGRAPHIC METHOD AFTER LIQUID-LIQUID EXTRACTION
EN 12766-1:2000	Petroleum products and used oils - Determination of PCBs and related products - Part 1: Separation and determination of selected PCB congeners by gas chromatography (GC) using an electron capture detector (ECD)
ISO 22892:2006	Soil quality Guidelines for the identification of target compounds by gas chromatography and mass spectrometry
EN 61619:1997	Insulating liquids - Contamination by polychlorinated biphenyls (PCBs) - Method of determination by capillary column gas chromatography
EN 15308:2016	Characterization of waste - Determination of selected polychlorinated biphenyls (PCB) in solid waste by gas chromatography with electron capture or mass spectrometric detection
ISO 5667-15:2009	Water quality — Sampling — Part 15: Guidance on the preservation and handling of sludge and sediment samples
ISO 16720:2005	Soil quality Pretreatment of samples by freeze-drying for subsequent analysis
EN ISO 16720:2007	Soil quality - Pretreatment of samples by freeze-drying for subsequent analysis (ISO 16720:2005)
ISO 5725-2:1994	Accuracy (trueness and precision) of measurement methods and results Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method
ISO 8466-1:1990	Water quality Calibration and evaluation of analytical methods and estimation of performance characteristics Part 1: Statistical evaluation of the linear calibration function
EN ISO 22892:2011	Soil quality - Guidelines for the identification of target compounds by gas chromatography and mass spectrometry (ISO 22892:2006)
EN ISO 5667-15:2009	Water quality - Sampling - Part 15: Guidance on the preservation and handling of sludge and sediment samples (ISO 5667-15:2009)
EN 15934:2012	Sludge, treated biowaste, soil and waste - Calculation of dry matter fraction after determination of dry residue or water content
IEC 61619:1997	Insulating liquids - Contamination by polychlorinated biphenyls (PCBs) - Method of determination by capillary column gas chromatography
EN 16179:2012	Sludge, treated biowaste and soil - Guidance for sample pretreatment
ISO 6468:1996	Water quality Determination of certain organochlorine insecticides, polychlorinated biphenyls and chlorobenzenes Gas chromatographic method after liquid-liquid extraction
ISO 18512:2007	Soil quality Guidance on long and short term storage of soil samples