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01/121388 DC : DRAFT MARCH 2001

Superseded
Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

View Superseded by
superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

ISO 307 PLASTICS - POLYAMIDES - DETERMINATION OF VISCOSITY NUMBER
Superseded date

01-09-2003

Published date

23-11-2012

Foreword
1 Scope
2 Normative references
3 Definitions
4 Principle
5 Reagents and materials
6 Apparatus
7 Preparation of test samples
   7.1 General
   7.2 Samples with extractable ingredients
   7.3 Samples with auxiliaries (non-hydrolyzable
       and without ash) that are insoluble in hydrochloric
       acid, e.g. polymer modifiers, carbon fibres and certain
       flame-retardants
   7.4 Samples with auxiliaries that are soluble in dilute
       hydrochloric acid and/or cannot be determined from the
       ash owing to oxide formation, e.g. carbonates, metal
       powders and certain pigments
8 Calculation of mass of test portion
9 Selection of solvent
10 Procedure
   10.1 Cleaning of viscometer
   10.2 Preparation of test solution
   10.3 Measurements of flow times
11 Expression of results
12 Repeatability and reproducibility
13 Interconversion of the viscosity numbers determined in
   different solvents and Interconversion of the viscosity
   numbers determined in 96 % sulfuric acid and relative
   viscosities determined in accordance with ASTM D 789
   13.1 Viscosity numbers in 96 % (m/m) sulfuric acid and 90
        % (m/m) formic acid, respectively
   13.2 Viscosity numbers in 96 % (m/m) sulfuric acid and
        m-cresol, respectively
14 Test report
Annex A (normative) Determination of the concentration of
        commercial sulfuric acid (95 % to 97 %) and adjustment
        to 96 %
        A.1 General
        A.2 Apparatus and reagents
        A.3 Procedure
        A.4 Expression of results
        A.5 Adjustment of sulfuric acid and concentration

Committee
PRI/82
DocumentType
Draft
PublisherName
British Standards Institution
Status
Superseded
SupersededBy

ISO 1628-1:2009 Plastics Determination of the viscosity of polymers in dilute solution using capillary viscometers Part 1: General principles
ISO 1874-1:2010 Plastics Polyamide (PA) moulding and extrusion materials Part 1: Designation system and basis for specification
ISO 6427:2013 Plastics — Determination of matter extractable by organic solvents (conventional methods)
ISO 1042:1998 Laboratory glassware One-mark volumetric flasks
ISO 472:2013 Plastics Vocabulary
ISO 15512:2016 Plastics Determination of water content
ISO 3105:1994 Glass capillary kinematic viscometers — Specifications and operating instructions
ISO 3451-4:1998 Plastics — Determination of ash — Part 4: Polyamides

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