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ASTM C 781 : 2008

Superseded
Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

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superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

Standard Practice for Testing Graphite and Boronated Graphite Materials for High-Temperature Gas-Cooled Nuclear Reactor Components
Available format(s)

Hardcopy , PDF

Superseded date

24-10-2018

Language(s)

English

Published date

01-09-2008

CONTAINED IN VOL. 05.05, 2017 Defines the test methods for measuring the properties of graphite and boronated graphite materials.

1.1 This practice covers the test methods for measuring the properties of graphite and boronated graphite materials. These properties may be used for the design and evaluation of high-temperature gas-cooled reactor components.

1.2 The test methods referenced herein are applicable to materials used for replaceable and permanent components as defined in Section 7 and Section 9, and includes fuel elements; removable reflector elements and blocks; permanent side reflector elements and blocks; core support pedestals and elements; control rod, reserve shutdown, and burnable poison compacts; and neutron shield material.

1.3 This practice includes test methods that have been selected from existing ASTM standards, ASTM standards that have been modified, and new ASTM standards that are specific to the testing of materials listed in 1.2. Comments on individual test methods for graphite and boronated graphite components are given in Sections 8 and 10, respectively. The test methods are summarized in Tables 1 and 2.

1.4 The values stated in SI units are to be regarded as standard. The values given in parentheses are for information only.

1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

TABLE 1 Summary of Test Methods for Graphite Components

Note—Designations under preparation will be added when approved.

Fuel, Removable Reflector,
and Core Support Elements;
Pebble Bed Reflector,
Key and Sleeves;
and Dowel Pins
Permanent Side
Reflector Elements
and Dowel Pins
Core Support Pedestals
and Dowels
Fabrication
As Manufactured Bulk DensityC838C838C838
Mechanical Properties
Compressive StrengthC695C695C695
Tensile PropertiesC749AC749AC749A
Poissons RatioE132BE132BE132B
Flexural StrengthC651AC651AC651A
Fracture ToughnessBBB
Modulus of ElasticityC747C747C747
Physical Properties
Bulk DensityMachined SpecimensC559C559C559
Surface Area (BET)C1274C1274C1274
PermeabilityC577A,BC577A,BC577A,B
Apparent PorosityC1039C1039C1039
Spectroscopic AnalysisBBB
Electrical ResistivityC611C611C611
Thermal Properties
Linear Thermal ExpansionE228A
Thermal ConductivityE1461AE1461AE1461A
Chemical Properties
Oxidative Mass LossC1179BC1179BC1179B
Sulfur ConcentrationC816C816C816
Ash ContentC561AC561AC561A
Equivalent Boron ContentC1233AC1233AC

A Modification of this test method is required. See Section 8 for details.

B New test methods are required. See Section 8 for details.

C There is no identified need for determining this property.

TABLE 2 Summary of Test Methods for Boronated Graphite Components

Note—Designations under preparation will be added when approved.

CompactsNeutron
Shield
Material
Control
Rod
Burnable
Poison
Reserve
Shutdown
Bulk DensityC838C838C838D4292
Linear Thermal ExpansionAE228AE228AB
Particle SizeCCCD2862
Mechanical Strength:
Compressive StrengthC695AC695AC695AB
Impact PerformanceBBBC
Chemical Properties:
Sulfur ConcentrationCCCC
Hafnium ConcentrationCCCC
Relative Oxidation RateCCCC
Boron Analysis:
Total BoronCCCC
Boron as OxideCCCC
B4C Particle SizeD2862DD2862DD2862DD2862D

A Modification of this test method is required. See Section 10 for details.

B There is no identified need for determining this property.

C New test methods are required. See Section 10 for details.

D Additional test methods are required. See Section 10 for details.

Committee
D 02
DocumentType
Standard Practice
Pages
10
ProductNote
Reconfirmed 2008
PublisherName
American Society for Testing and Materials
Status
Superseded
SupersededBy
Supersedes

ASTM C 1233 : 2015 : REDLINE Standard Practice for Determining Equivalent Boron Contents of Nuclear Materials
ASTM E 228 : 2017 : REDLINE Standard Test Method for Linear Thermal Expansion of Solid Materials With a Push-Rod Dilatometer
ASTM D 5600 : 2017 : REDLINE Standard Test Method for Trace Metals in Petroleum Coke by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES)
ASTM C 625 : 2015 : REDLINE Standard Practice for Reporting Irradiation Results on Graphite
ASTM D 2862 : 2016 : REDLINE Standard Test Method for Particle Size Distribution of Granular Activated Carbon
ASTM C 1179 : 2015 : REDLINE Standard Test Method for Oxidation Mass Loss of Manufactured Carbon and Graphite Materials in Air
ASTM E 1461 : 2013 : REDLINE Standard Test Method for Thermal Diffusivity by the Flash Method
ASTM C 695 : 2015 : REDLINE Standard Test Method for Compressive Strength of Carbon and Graphite
ASTM C 749 : 2015 : REDLINE Standard Test Method for Tensile Stress-Strain of Carbon and Graphite
ASTM E 132 : 2017 : REDLINE Standard Test Method for Poisson’s Ratio at Room Temperature
ASTM C 561 : 2016 : REDLINE Standard Test Method for Ash in a Graphite Sample
ASTM C 577 : 2007 Standard Test Method for Permeability of Refractories
ASTM C 747 : 2016 : REDLINE Standard Test Method for Moduli of Elasticity and Fundamental Frequencies of Carbon and Graphite Materials by Sonic Resonance
ASTM E 11 : 2017 : REDLINE Standard Specification for Woven Wire Test Sieve Cloth and Test Sieves
ASTM E 261 : 2016 : REDLINE Standard Practice for Determining Neutron Fluence, Fluence Rate, and Spectra by Radioactivation Techniques
ASTM C 559 : 2016 : REDLINE Standard Test Method for Bulk Density by Physical Measurements of Manufactured Carbon and Graphite Articles
ASTM C 1274 : 2012 : REDLINE Standard Test Method for Advanced Ceramic Specific Surface Area by Physical Adsorption
ASTM C 816 : 2015 : REDLINE Standard Test Method for Sulfur Content in Graphite by Combustion-Iodometric Titration Method
ASTM C 838 : 2016 : REDLINE Standard Test Method for Bulk Density of As-Manufactured Carbon and Graphite Shapes
ASTM C 651 : 2015 : REDLINE Standard Test Method for Flexural Strength of Manufactured Carbon and Graphite Articles Using Four-Point Loading at Room Temperature
ASTM C 769 : 2015 : REDLINE Standard Test Method for Sonic Velocity in Manufactured Carbon and Graphite Materials for Use in Obtaining an Approximate Value of Young's Modulus

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