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ASTM D 128 : 1998 : R2003 : EDT 1

Superseded

Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

View Superseded by
superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

Standard Test Methods for Analysis of Lubricating Grease

Available format(s)

Hardcopy , PDF

Superseded date

11-11-2014

Language(s)

English

Published date

10-05-2003

CONTAINED IN VOL. 05.01, 2015 Defines greases of the conventional type, which consist essentially of petroleum oil and soap.

1.1 These test methods for analysis cover greases of the conventional type, which consist essentially of petroleum oil and soap. The constituents that can be determined are soap, unsaponifiable matter (petroleum oil, and so forth), water, free alkalinity, free fatty acid, fat, glycerin, and insolubles.

Note 1—Any of the test methods described herein are best used by an experienced grease analyst who may also be able to make appropriate adaptations of the techniques as occasion requires.

1.2 A supplementary test method is provided in Appencix X1. This test method is intended primarily for application to greases containing thickeners that are essentially insoluble in n-hexane, and to greases that cannot be analyzed by conventional methods because of the presence of such constituents as nonpetroleum fluids or nonsoap-type thickeners, or both. In some cases, these constituents can react with strong acid or alkaline solutions.

1.3 These test methods appear in the following order:

Sections
Ash Determination7-11
Insolubles, Soap, Fat, Petroleum Oil,and Unsaponifiable Matter12-20
Free Alkali and Free Acid21-23
Water24
Glycerin (Quantitative)25-29

1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices, and determine the applicability of regulatory limitations prior to use.

1.5 The values stated in SI units are to be regarded as the standard.

Committee
D 02
DocumentType
Test Method
Pages
11
ProductNote
Reconfirmed EDT 1
PublisherName
American Society for Testing and Materials
Status
Superseded
SupersededBy
Supersedes

ASTM D 1353 : 2013 : REDLINE Standard Test Method for Nonvolatile Matter in Volatile Solvents for Use in Paint, Varnish, Lacquer, and Related Products
ASTM D 156 : 2015 : REDLINE Standard Test Method for Saybolt Color of Petroleum Products (Saybolt Chromometer Method)
ASTM D 217 : 2017 : REDLINE TEST METHODS FOR CONE PENETRATION OF LUBRICATING GREASE

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