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ASTM D 4603 : 2018

Current

Current

The latest, up-to-date edition.

Standard Test Method for Determining Inherent Viscosity of Poly(Ethylene Terephthalate) (PET) by Glass Capillary Viscometer

Available format(s)

Hardcopy , PDF

Language(s)

English

Published date

01-05-2018

This test method is for the determination of the inherent viscosity of poly(ethylene terephthalate) (PET) soluble at 0.50 % concentration in a 60/40 phenol/1,1,2,2-tetrachloroethane solution by means of a glass capillary viscometer.

1.1This test method is for the determination of the inherent viscosity of poly(ethylene terephthalate) (PET) soluble at 0.50 % concentration in a 60/40 phenol/1,1,2,2-tetrachloroethane solution by means of a glass capillary viscometer. Highly crystalline forms of PET that are not soluble in this solvent mixture will require a different procedure.

1.2The inherent viscosity values obtained by this test method are comparable with those obtained using differential viscometry described in Test Method D5225.

1.3The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.

1.4This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific hazards statements are given in Section 8.

1.4.1Warning—Mercury has been designated by many regulatory agencies as a hazardous material that can cause serious medical issues. Mercury, or its vapor, has been demonstrated to be hazardous to health and corrosive to materials. Caution should be taken when handling mercury and mercury containing products. See the applicable product Safety Data Sheet (SDS) for additional information. Users should be aware that selling mercury and/or mercury containing products into your state or country may be prohibited by law

Note 1:This standard and ISO 1628-5 address the same subject matter, but differ in technical content. This ISO standard gives an option of solvents for PET. Solvent specified in this ASTM test method is one of the options in the ISO method. ISO also uses Type 1C Ubbelohde viscometer, rather than the 1B, and reports viscosity number, rather than inherent viscosity.

1.5This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

Committee
D 20
DocumentType
Test Method
Pages
4
PublisherName
American Society for Testing and Materials
Status
Current
Supersedes

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ASTM F 2313 : 2018 Standard Specification for Poly(glycolide) and Poly(glycolide-co-lactide) Resins for Surgical Implants with Mole Fractions Greater Than or Equal to 70 % Glycolide
ASTM D 8105 : 2018 Standard Guide for Use and Application of Geosynthetic Reinforcement Reduction Factor Test Results
ASTM D 2857 : 2016 Standard Practice for Dilute Solution Viscosity of Polymers
ASTM F 1925 : 2017 Standard Specification for Semi-Crystalline Poly(lactide) Polymer and Copolymer Resins for Surgical Implants
ASTM D 6389 : 2017 Standard Practice for Tests to Evaluate the Chemical Resistance of Geotextiles to Liquids
ASTM D 6213 : 2017 Standard Practice for Tests to Evaluate the Chemical Resistance of Geogrids to Liquids

ASTM D 5225 : 2009 Standard Test Method for Measuring Solution Viscosity of Polymers with a Differential Viscometer
ASTM D 5225 : 1998 Standard Test Method for Measuring Solution Viscosity of Polymers with a Differential Viscometer
ASTM D 5225 : 2014 Standard Test Method for Measuring Solution Viscosity of Polymers with a Differential Viscometer
ASTM D 1972 : 1997 : R2005 Standard Practice for Generic Marking of Plastic Products (Withdrawn 2014)
ASTM E 2251 : 2007 Standard Specification for Liquid-in-Glass ASTM Thermometers with Low-Hazard Precision Liquids
ASTM E 2251 : 2003 : REV A Standard Specification for Liquid-in-Glass ASTM Thermometers with Low-Hazard Precision Liquids
ASTM E 2935 : 2017 Standard Practice for Conducting Equivalence Testing in Laboratory Applications
ASTM E 2935 : 2014 Standard Practice for Conducting Equivalence Testing in Laboratory Applications
ASTM D 445 : 2021 : EDT 2 Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity)
ASTM E 691 : 2020 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
ASTM E 2935 : 2013 Standard Practice for Conducting Equivalence Testing in Laboratory Applications
ASTM D 445 : 2017 : REV A Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity)
ASTM E 2251 : 2003 Standard Specification for Liquid-in-Glass ASTM Thermometers with Low-Hazard Precision Liquids
ASTM D 5225 : 2017 Standard Test Method for Measuring Solution Viscosity of Polymers with a Differential Viscometer
ASTM E 2251 : 2014 : R2021 Standard Specification for Liquid-in-Glass ASTM Thermometers with Low-Hazard Precision Liquids
ASTM D 445 : 1988 Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and the Calculation of Dynamic Viscosity)
ASTM E 691 : 2019 : EDT 1 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
ASTM E 691 : 2023 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
ASTM D 5225 : 2022 Standard Test Method for Measuring Solution Viscosity of Polymers with a Differential Viscometer
ASTM E 2251 : 2010 Standard Specification for Liquid-in-Glass ASTM Thermometers with Low-Hazard Precision Liquids
ASTM E 2935 : 2020 Standard Practice for Conducting Equivalence Tests for Comparing Testing Processes
ASTM E 2251 : 2011 Standard Specification for Liquid-in-Glass ASTM Thermometers with Low-Hazard Precision Liquids
ASTM E 2251 : 2014 Standard Specification for Liquid-in-Glass ASTM Thermometers with Low-Hazard Precision Liquids
ASTM E 691 : 2022 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
ASTM E 691 : 2009 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
ASTM E 2935 : 2020 : EDT 1 Standard Practice for Conducting Equivalence Tests for Comparing Testing Processes
ASTM D 445 : 2019 : REV A Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity)
ASTM D 445 : 2019 Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity)
ASTM E 691 : 2021 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
ASTM D 445 : 2001 Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (the Calculation of Dynamic Viscosity)
ASTM D 1972 : 1997 Standard Practice for Generic Marking of Plastic Products
ASTM E 2935 : 2016 Standard Practice for Conducting Equivalence Testing in Laboratory Applications
ASTM D 445 : 2024 Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity)
ASTM D 445 : 2021 Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity)
ASTM E 2935 : 2021 Standard Practice for Evaluating Equivalence of Two Testing Processes
ASTM D 445 : 2018 Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity)
ASTM E 2935 : 2015 Standard Practice for Conducting Equivalence Testing in Laboratory Applications
ASTM D 1972 : 1997 : R2001 Standard Practice for Generic Marking of Plastic Products
ASTM D 445 : 2021 : EDT 1 Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity)
ASTM D 445 : 2023 Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity)

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