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ASTM D 4821 : 2016

Superseded
Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

View Superseded by
superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

Standard Guide for Carbon Black—Validation of Test Method Precision and Bias
Available format(s)

Hardcopy , PDF

Superseded date

16-09-2019

Language(s)

English

Published date

15-08-2016

1.1This guide covers procedures for using the ASTM Standard Reference Blacks2 (SRBs) and the HT and INR Iodine Number Standards to continuously monitor the precision of those carbon black test methods for which reference values have been established. It also offers guidelines for troubleshooting various test methods.

1.2This guide defines the environmental conditions that are required for laboratories that perform carbon black testing activities for those test methods under D24’s jurisdiction.

1.3This guide establishes procedures for the use of x-charts to continuously monitor those tests listed in Section 2 for within-lab precision (repeatability) and between-lab accuracy (reproducibility).

1.4This guide provides a statistical procedure for improving test reproducibility when a laboratory cannot physically calibrate its apparatus to obtain the reference values of the ASTM reference blacks, within the ranges given in this guide.

Committee
D 24
DocumentType
Guide
Pages
13
PublisherName
American Society for Testing and Materials
Status
Superseded
SupersededBy
Supersedes

ASTM D 2414 : 2018 : REV A Standard Test Method for Carbon Black—Oil Absorption Number (OAN)
ASTM D 8043 : 2016 Standard Guide for Carbon Black—Shelf Life
ASTM D 1510 : 2019 Standard Test Method for Carbon Black—Iodine Adsorption Number
ASTM D 3493 : 2018 : REV A Standard Test Method for Carbon Black—Oil Absorption Number of Compressed Sample (COAN)
ASTM D 3265 : 2019 Standard Test Method for Carbon Black—Tint Strength
ASTM D 6915 : 2017 : EDT 1 Standard Practice for Carbon Black—Evaluation of Standard Reference Blacks

ASTM D 3493 : 2001 Standard Test Method for Carbon Black—Oil Absorption Number of Compressed Sample
ASTM E 2586 : 2012 Standard Practice for Calculating and Using Basic Statistics
ASTM D 2414 : 2008 Standard Test Method for Carbon Black<span class='unicode'>—</span>Oil Absorption Number (OAN)
ASTM D 3493 : 2009 Standard Test Method for Carbon Black-Oil Absorption Number of Compressed Sample (COAN)
ASTM D 3493 : 2006 : EDT 1 Standard Test Method for Carbon Black-Oil Absorption Number of Compressed Sample (COAN)
ASTM D 2414 : 2008 : REV A Standard Test Method for Carbon Black<span class='unicode'>—</span>Oil Absorption Number (OAN)
ASTM D 1765 : 2005 : REV A : EDT 1 Standard Classification System for Carbon Blacks Used in Rubber Products
ASTM D 3493 : 2006 Standard Test Method for Carbon Black-Oil Absorption Number of Compressed Sample (COAN)
ASTM D 1513 : 2004 Standard Test Method for Carbon Black, Pelleted—Pour Density
ASTM D 3265 : 2011 Standard Test Method for Carbon Black-Tint Strength
ASTM D 3493 : 2004 Standard Test Method for Carbon Black—Oil Absorption Number of Compressed Sample (COAN)
ASTM D 1765 : 2003 Standard Classification System for Carbon Blacks Used in Rubber Products
ASTM D 2414 : 2000 : REV A Standard Test Method for Carbon Black—Oil Absorption Number
ASTM D 1510 : 2007 Standard Test Method for Carbon Black-Iodine Adsorption Number
ASTM D 1510 : 2019 Standard Test Method for Carbon Black—Iodine Adsorption Number
ASTM D 2414 : 2003 Standard Test Method for Carbon Black—Oil Absorption Number (OAN)
ASTM D 1765 : 2004 : EDT 1 Standard Classification System for Carbon Blacks Used in Rubber Products
ASTM D 2414 : 2016 Standard Test Method for Carbon Black—Oil Absorption Number (OAN)
ASTM D 1510 : 2008 : REV B Standard Test Method for Carbon Black<span class='unicode'>—</span>Iodine Adsorption Number
ASTM D 6556 : 2009 Standard Test Method for Carbon Black-Total and External Surface Area by Nitrogen Adsorption
ASTM D 1765 : 2017 Standard Classification System for Carbon Blacks Used in Rubber Products
ASTM D 3265 : 2017 : EDT 1 Standard Test Method for Carbon Black—Tint Strength
ASTM D 2414 : 2006 : REV A Standard Test Method for Carbon Black-Oil Absorption Number (OAN)
ASTM D 6556 : 2007 Standard Test Method for Carbon Black-Total and External Surface Area by Nitrogen Adsorption
ASTM D 3493 : 2003 Standard Test Method for Carbon Black—Oil Absorption Number of Compressed Sample
ASTM D 2414 : 2013 Standard Test Method for Carbon Black—Oil Absorption Number (OAN)
ASTM D 1510 : 2011 Standard Test Method for Carbon Black<span class='unicode'>—</span>Iodine Adsorption Number
ASTM D 6556 : 2002 : REV A Standard Test Method for Carbon Black—Total and External Surface Area by Nitrogen Adsorption
ASTM D 3265 : 2015 : REV A Standard Test Method for Carbon Black—Tint Strength
ASTM D 1510 : 2008 Standard Test Method for Carbon Black<span class='unicode'>—</span>Iodine Adsorption Number
ASTM D 1510 : 2016 : REV A Standard Test Method for Carbon Black—Iodine Adsorption Number
ASTM D 1765 : 2014 Standard Classification System for Carbon Blacks Used in Rubber Products
ASTM D 6556 : 2003 Standard Test Method for Carbon Black—Total and External Surface Area by Nitrogen Adsorption
ASTM D 1765 : 2000 : REV A Standard Classification System for Carbon Blacks Used in Rubber Products
ASTM D 2414 : 2011 Standard Test Method for Carbon Black<span class='unicode'>—</span>Oil Absorption Number (OAN)
ASTM E 2586 : 2014 Standard Practice for Calculating and Using Basic Statistics
ASTM D 1510 : 2003 Standard Test Method for Carbon Black—Iodine Adsorption Number
ASTM D 2414 : 2005 : REV A Standard Test Method for Carbon Black—Oil Absorption Number (OAN)
ASTM D 3493 : 2007 Standard Test Method for Carbon Black-Oil Absorption Number of Compressed Sample (COAN)
ASTM D 3493 : 2014 Standard Test Method for Carbon Black—Oil Absorption Number of Compressed Sample (COAN)
ASTM D 1513 : 2005 : EDT 1 Standard Test Method for Carbon Black, Pelleted—Pour Density
ASTM D 3265 : 2015 Standard Test Method for Carbon Black—Tint Strength
ASTM D 2414 : 2005 Standard Test Method for Carbon Black—Oil Absorption Number (OAN)
ASTM D 3265 : 2003 Standard Test Method for Carbon Black—Tint Strength
ASTM D 1510 : 2017 Standard Test Method for Carbon Black—Iodine Adsorption Number
ASTM D 6556 : 2019 Standard Test Method for Carbon Black—Total and External Surface Area by Nitrogen Adsorption
ASTM D 1765 : 2018 Standard Classification System for Carbon Blacks Used in Rubber Products
ASTM D 3493 : 2000 : REV A Standard Test Method for Carbon Black—Oil Absorption Number of Compressed Sample
ASTM D 1765 : 2001 : EDT 1 Standard Classification System for Carbon Blacks Used in Rubber Products
ASTM D 2414 : 2012 Standard Test Method for Carbon Black—Oil Absorption Number (OAN)
ASTM D 3265 : 2006 Standard Test Method for Carbon Black-Tint Strength
ASTM D 1765 : 2004 : REV A Standard Classification System for Carbon Blacks Used in Rubber Products
ASTM E 2586 : 2010 : REV A Standard Practice for Calculating and Using Basic Statistics
ASTM D 3265 : 2013 : REV A Standard Test Method for Carbon Black—Tint Strength
ASTM D 3265 : 2005 Standard Test Method for Carbon Black—Tint Strength
ASTM D 1513 : 2005 : R2012 Standard Test Method for Carbon Black, Pelleted—Pour Density
ASTM E 2282 : 2013 Standard Guide for Defining the Test Result of a Test Method
ASTM D 1510 : 2005 : REV A Standard Test Method for Carbon Black—Iodine Adsorption Number
ASTM E 2586 : 2019 Standard Practice for Calculating and Using Basic Statistics
ASTM D 1765 : 2001 Standard Classification System for Carbon Blacks Used in Rubber Products
ASTM D 3265 : 2007 Standard Test Method for Carbon Black-Tint Strength
ASTM D 1510 : 2013 Standard Test Method for Carbon Black—Iodine Adsorption Number
ASTM D 1765 : 2016 Standard Classification System for Carbon Blacks Used in Rubber Products
ASTM D 3493 : 2016 Standard Test Method for Carbon Black—Oil Absorption Number of Compressed Sample (COAN)
ASTM D 2414 : 2002 Standard Test Method for Carbon Black—Oil Absorption Number
ASTM D 2414 : 2016 : EDT 1 Standard Test Method for Carbon Black—Oil Absorption Number (OAN)
ASTM D 3493 : 2018 Standard Test Method for Carbon Black—Oil Absorption Number of Compressed Sample (COAN)
ASTM D 6556 : 2002 Standard Test Method for Carbon Black—Total and External Surface Area by Nitrogen Adsorption
ASTM E 2586 : 2012 : REV A Standard Practice for Calculating and Using Basic Statistics
ASTM D 6556 : 2017 Standard Test Method for Carbon Black—Total and External Surface Area by Nitrogen Adsorption
ASTM D 1510 : 1999 Standard Test Method for Carbon Black—Iodine Adsorption Number
ASTM D 1765 : 2005 : REV A Standard Classification System for Carbon Blacks Used in Rubber Products
ASTM D 1765 : 2013 Standard Classification System for Carbon Blacks Used in Rubber Products
ASTM D 1513 : 2005 : EDT 2 Standard Test Method for Carbon Black, Pelleted—Pour Density
ASTM D 2414 : 2009 : REV A Standard Test Method for Carbon Black<span class='unicode'>—</span>Oil Absorption Number (OAN)
ASTM D 1510 : 2009 Standard Test Method for Carbon Black<span class='unicode'>—</span>Iodine Adsorption Number
ASTM D 1510 : 2012 Standard Test Method for Carbon Black—Iodine Adsorption Number
ASTM E 2282 : 2003 Standard Guide for Defining the Test Result of a Test Method
ASTM D 1513 : 1999 : REV A : EDT 1 Standard Test Method for Carbon Black, Pelleted-Pour Density
ASTM E 2586 : 2007 Standard Practice for Calculating and Using Basic Statistics
ASTM D 3493 : 2004 : REV A Standard Test Method for Carbon Black—Oil Absorption Number of Compressed Sample (COAN)
ASTM D 2414 : 2006 Standard Test Method for Carbon Black-Oil Absorption Number (OAN)
ASTM D 3265 : 2017 Standard Test Method for Carbon Black—Tint Strength
ASTM E 2586 : 2016 Standard Practice for Calculating and Using Basic Statistics
ASTM D 1765 : 2006 Standard Classification System for Carbon Blacks Used in Rubber Products
ASTM D 1510 : 2008 : REV C Standard Test Method for Carbon Black<span class='unicode'>—</span>Iodine Adsorption Number
ASTM D 1510 : 2007 : REV A Standard Test Method for Carbon Black-Iodine Adsorption Number
ASTM D 2414 : 2018 : REV A Standard Test Method for Carbon Black—Oil Absorption Number (OAN)
ASTM D 2414 : 2017 Standard Test Method for Carbon Black—Oil Absorption Number (OAN)
ASTM E 2586 : 2018 Standard Practice for Calculating and Using Basic Statistics
ASTM D 3265 : 2013 Standard Test Method for Carbon Black—Tint Strength
ASTM D 2414 : 2014 Standard Test Method for Carbon Black—Oil Absorption Number (OAN)
ASTM D 2414 : 2006 : REV A : EDT 1 Standard Test Method for Carbon Black-Oil Absorption Number (OAN)
ASTM D 6556 : 2001 Standard Test Method for Carbon Black—Total and External Surface Area by Nitrogen Adsorption
ASTM D 6556 : 2000 : REV A Standard Test Method for Carbon Black—Total and External Surface Area by Nitrogen Adsorption
ASTM D 2414 : 2002 : REV A Standard Test Method for Carbon Black—Oil Absorption Number
ASTM D 6556 : 2014 Standard Test Method for Carbon Black—Total and External Surface Area by Nitrogen Adsorption
ASTM E 2586 : 2012 : REV B Standard Practice for Calculating and Using Basic Statistics
ASTM D 6556 : 2001 : REV A Standard Test Method for Carbon Black—Total and External Surface Area by Nitrogen Adsorption
ASTM D 1510 : 2006 : REV A Standard Test Method for Carbon Black-Iodine Adsorption Number
ASTM D 2414 : 2001 Standard Test Method for Carbon Black—Oil Absorption Number
ASTM E 2282 : 2014 Standard Guide for Defining the Test Result of a Test Method
ASTM D 1510 : 2002 : REV A Standard Test Method for Carbon Black—Iodine Adsorption Number
ASTM D 3324 : 2001 Standard Practice for Carbon Black—Improving Test Reproducibility Using ASTM Standard Reference Blacks
ASTM D 3493 : 2018 : REV A Standard Test Method for Carbon Black—Oil Absorption Number of Compressed Sample (COAN)
ASTM D 1510 : 2006 Standard Test Method for Carbon Black—Iodine Adsorption Number
ASTM D 3493 : 2013 Standard Test Method for Carbon Black—Oil Absorption Number of Compressed Sample (COAN)
ASTM D 2414 : 2004 Standard Test Method for Carbon Black—Oil Absorption Number (OAN)
ASTM D 3265 : 2002 Standard Test Method for Carbon Black—Tint Strength
ASTM D 1510 : 2016 Standard Test Method for Carbon Black—Iodine Adsorption Number
ASTM D 1765 : 2010 Standard Classification System for Carbon Blacks Used in Rubber Products
ASTM D 1510 : 2005 Standard Test Method for Carbon Black—Iodine Adsorption Number
ASTM E 2586 : 2010 Standard Practice for Calculating and Using Basic Statistics
ASTM D 1510 : 2010 Standard Test Method for Carbon Black<span class='unicode'>—</span>Iodine Adsorption Number
ASTM D 1765 : 2004 Standard Classification System for Carbon Blacks Used in Rubber Products
ASTM D 1513 : 2005 : R2017 Standard Test Method for Carbon Black, Pelleted—Pour Density
ASTM D 6556 : 2004 Standard Test Method for Carbon Black-Total and External Surface Area by Nitrogen Adsorption
ASTM D 1510 : 2001 : REV A Standard Test Method for Carbon Black—Iodine Adsorption Number
ASTM D 1510 : 2002 Standard Test Method for Carbon Black—Iodine Adsorption Number
ASTM E 2282 : 2009 Standard Guide for Defining the Test Result of a Test Method
ASTM D 3324 : 1999 Standard Practice for Carbon Black—Improving Test Reproducibility Using ASTM Standard Reference Blacks
ASTM D 2414 : 2018 Standard Test Method for Carbon Black—Oil Absorption Number (OAN)
ASTM D 1513 : 1999 : REV A : R2004 Standard Test Method for Carbon Black, Pelleted—Pour Density
ASTM D 6556 : 2016 Standard Test Method for Carbon Black—Total and External Surface Area by Nitrogen Adsorption
ASTM D 1510 : 2009 : REV B Standard Test Method for Carbon Black<span class='unicode'>—</span>Iodine Adsorption Number
ASTM D 3265 : 2019 Standard Test Method for Carbon Black—Tint Strength
ASTM D 3265 : 2001 Standard Test Method for Carbon Black—Tint Strength
ASTM E 2586 : 2013 Standard Practice for Calculating and Using Basic Statistics
ASTM D 1510 : 2011 : REV A Standard Test Method for Carbon Black<span class='unicode'>—</span>Iodine Adsorption Number
ASTM D 1510 : 2008 : REV A Standard Test Method for Carbon Black<span class='unicode'>—</span>Iodine Adsorption Number
ASTM D 1510 : 2009 : REV A Standard Test Method for Carbon Black<span class='unicode'>—</span>Iodine Adsorption Number
ASTM D 2414 : 2009 Standard Test Method for Carbon Black<span class='unicode'>—</span>Oil Absorption Number (OAN)
ASTM D 3265 : 2014 Standard Test Method for Carbon Black—Tint Strength
ASTM D 3265 : 2000 Standard Test Method for Carbon Black—Tint Strength
ASTM D 2414 : 2013 : REV A Standard Test Method for Carbon Black—Oil Absorption Number (OAN)
ASTM D 1510 : 2001 Standard Test Method for Carbon Black—Iodine Adsorption Number
ASTM D 3265 : 2017 : REV A Standard Test Method for Carbon Black—Tint Strength
ASTM D 1765 : 2005 Standard Classification System for Carbon Blacks Used in Rubber Products
ASTM D 1513 : 2005 Standard Test Method for Carbon Black, Pelleted—Pour Density
ASTM D 6556 : 2010 Standard Test Method for Carbon Black-Total and External Surface Area by Nitrogen Adsorption

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