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ASTM D 5315 : 2004

Superseded
Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

View Superseded by
superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

Standard Test Method for Determination of N-Methyl-Carbamoyloximes and N-Methylcarbamates in Water by Direct Aqueous Injection HPLC with Post-Column Derivatization
Available format(s)

Hardcopy , PDF

Superseded date

11-11-2014

Language(s)

English

Published date

01-06-2004

Publisher

American Society for Testing and Materials

CONTAINED IN VOL. 11.02, 2018 Defines a high-performance liquid chromatographic (HPLC) test method applicable to the determination of certain n-methylcarbamoyloximes and n-methylcarbamates in ground water and finished drinking water.

1.1 This is a high-performance liquid chromatographic (HPLC) test method applicable to the determination of certain n-methylcarbamoyloximes and n-methylcarbamates in ground water and finished drinking water (). This test method is applicable to any carbamate analyte that can be hydrolyzed to a primary amine. The following compounds have been validated using this test method:

Numbering system of Chemical Abstracts, Inc.

AnalyteChemical Abstract Services Registry Number
Aldicarb 116-06-3
Aldicarb sulfone 1646-88-4
Aldicarb sulfoxide 1646-87-3
Baygon 114-26-1
Carbaryl 63-25-2
Carbofuran 1563-66-2
3-Hydroxycarbofuran 16655-82-6
Methiocarb 2032-65-7
Methomyl 16752-77-5
Oxamyl 23135-22-0

1.2 This test method has been validated in a collaborative round-robin study () and estimated detection limits (EDLs) have been determined for the analytes listed in (). Observed detection limits may vary between ground waters, depending on the nature of interferences in the sample matrix and the specific instrumentation used.

1.3 This test method is restricted to use by, or under the supervision of, analysts experienced in both the use of liquid chromatography and the interpretation of liquid chromatograms. Each analyst should demonstrate an ability to generate acceptable results with this test method using the procedure described in .

1.4 When this test method is used to analyze unfamiliar samples for any or all of the analytes listed in , analyte identifications should be confirmed by at least one additional qualitative technique.

Committee
D 19
DocumentType
Test Method
Pages
16
ProductNote
Reconfirmed 2004
PublisherName
American Society for Testing and Materials
Status
Superseded
SupersededBy
Supersedes

ASTM D 3694 : 1996 : R2017 Standard Practices for Preparation of Sample Containers and for Preservation of Organic Constituents

ASTM D 1129 : 2013 : REDLINE Standard Terminology Relating to Water
ASTM D 2777 : 2013 : REDLINE Standard Practice for Determination of Precision and Bias of Applicable Test Methods of Committee D19 on Water
ASTM E 682 : 1992 Standard Practice for Liquid Chromatography Terms and Relationships
ASTM D 1192 : 1998 Standard Guide for Equipment for Sampling Water and Steam in Closed Conduits (Withdrawn 2003)

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Hardcopy - English
PDF - English
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