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ASTM D 5501 : 2020

Current

Current

The latest, up-to-date edition.

Standard Test Method for Determination of Ethanol and Methanol Content in Fuels Containing Greater than 20 % Ethanol by Gas Chromatography

Available format(s)

Hardcopy , PDF

Language(s)

English

Published date

01-05-2020

1.1This test method covers the determination of the ethanol content of hydrocarbon blends containing greater than 20 % ethanol. This method is applicable to denatured fuel ethanol, ethanol fuel blends, and mid-level ethanol blends.

1.1.1Ethanol is determined from 20 % by mass to 100 % by mass and methanol is determined from 0.01 % by mass to 0.6 % by mass. Equations used to convert these individual alcohols from percent by mass to percent by volume are provided.

Note 1:Fuels containing less than 20 % ethanol may be quantified using Test Method D5599, and less than 12 % ethanol may be quantified using Test Method D4815.

1.2This test method does not purport to identify all individual components common to ethanol production or those components that make up the denaturant or hydrocarbon constituent of the fuel.

1.3Water cannot be determined by this test method and shall be measured by a procedure such as Test Method D7923, E203, or E1064 and the result used to correct the concentrations determined by this method.

1.4This test method is inappropriate for impurities that boil at temperatures higher than 225 °C or for impurities that cause poor or no response in a flame ionization detector, such as water.

1.5The values stated in SI units are to be regarded as the standard. The values given in parentheses are provided for information purposes only.

1.6This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.

1.7This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

Committee
D 02
DocumentType
Test Method
Pages
16
ProductNote
THIS STANDARD ALSO REFERS TO ASTM E 3237
PublisherName
American Society for Testing and Materials
Status
Current
Supersedes

ASTM D 7794 : 2018 : REV A Standard Practice for Blending Mid-Level Ethanol Fuel Blends for Flexible-Fuel Vehicles with Automotive Spark-Ignition Engines
ASTM E 3050 : 2016 Standard Specification for Denatured Ethanol for Use as Cooking and Appliance Fuel
ASTM D 7717 : 2011 : R2017 Standard Practice for Preparing Volumetric Blends of Denatured Fuel Ethanol and Gasoline Blendstocks for Laboratory Analysis

ASTM D 4057 : 2019 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
ASTM D 4806 : 2021 Standard Specification for Denatured Fuel Ethanol for Blending with Gasolines for Use as Automotive Spark-Ignition Engine Fuel
ASTM D 6792 : 2021 : REV A Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories
ASTM D 5798 : 2020 Standard Specification for Ethanol Fuel Blends for Flexible-Fuel Automotive Spark-Ignition Engines
ASTM D 4806 : 2021 : REV A Standard Specification for Denatured Fuel Ethanol for Blending with Gasolines for Use as Automotive Spark-Ignition Engine Fuel
ASTM D 4815 : 2015 : REV B Standard Test Method for Determination of MTBE, ETBE, TAME, DIPE, tertiary-Amyl Alcohol and C<inf>1</inf> to C<inf>4</inf> Alcohols in Gasoline by Gas Chromatography
ASTM D 4175 : 2020 : REV B Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
ASTM D 5599 : 2022 Standard Test Method for Determination of Oxygenates in Gasoline by Gas Chromatography and Oxygen Selective Flame Ionization Detection
ASTM E 1510 : 1995 : R2013 : EDT 1 Standard Practice for Installing Fused Silica Open Tubular Capillary Columns in Gas Chromatographs
ASTM D 4052 : 2018 : REV A Standard Test Method for Density, Relative Density, and API Gravity of Liquids by Digital Density Meter
ASTM D 1298 : 2012 : REV B : R2017 : EDT 1 Standard Test Method for Density, Relative Density, or API Gravity of Crude Petroleum and Liquid Petroleum Products by Hydrometer Method
ASTM D 1364 : 2022 Standard Test Method for Water in Volatile Solvents (Karl Fischer Reagent Titration Method)
ASTM D 6299 : 2021 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 4815 : 2015 : REV B : R2019 Standard Test Method for Determination of MTBE, ETBE, TAME, DIPE, tertiary-Amyl Alcohol and C<inf>1</inf> to C<inf>4</inf> Alcohols in Gasoline by Gas Chromatography
ASTM D 4175 : 2022 Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
ASTM D 6299 : 2022 : EDT 1 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 4815 : 2022 Standard Test Method for Determination of MTBE, ETBE, TAME, DIPE, tertiary-Amyl Alcohol and C<inf>1</inf> to C<inf>4</inf> Alcohols in Gasoline by Gas Chromatography
ASTM D 1298 : 2012 : REV B : R2017 Standard Test Method for Density, Relative Density, or API Gravity of Crude Petroleum and Liquid Petroleum Products by Hydrometer Method
ASTM D 5599 : 2018 Standard Test Method for Determination of Oxygenates in Gasoline by Gas Chromatography and Oxygen Selective Flame Ionization Detection
ASTM D 6792 : 2021 : REV B Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories
ASTM D 6792 : 2023 : REV C Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories
ASTM D 6299 : 2023 : REV A Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 4175 : 2001 : EDT 1 Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
ASTM D 4175 : 2020 : REV B : EDT 1 Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
ASTM D 4175 : 2022 : REV A Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
ASTM D 4175 : 2002 Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
ASTM E 203 : 2023 Standard Test Method for Water Using Volumetric Karl Fischer Titration
ASTM D 4175 : 2023 Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
ASTM D 6792 : 2023 : REV B Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories
ASTM D 6792 : 2020 Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories
ASTM D 6792 : 2021 Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories
ASTM D 6299 : 2023 : EDT 1 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 4175 : 2022 : REV A : EDT 1 Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
ASTM E 1064 : 2024 Standard Test Method for Water in Organic Liquids by Coulometric Karl Fischer Titration
ASTM E 1510 : 1995 : R2021 Standard Practice for Installing Fused Silica Open Tubular Capillary Columns in Gas Chromatographs
ASTM E 355 : 1996 : R2021 : EDT 1 Standard Practice for Gas Chromatography Terms and Relationships
ASTM D 6792 : 2021 : REV C Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories
ASTM D 6299 : 2023 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 4307 : 2017 Standard Practice for Preparation of Liquid Blends for Use as Analytical Standards
ASTM D 6792 : 2023 : REV A Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories
ASTM D 4626 : 1995 : R2019 Standard Practice for Calculation of Gas Chromatographic Response Factors
ASTM D 1364 : 2002 : R2012 Standard Test Method for Water in Volatile Solvents (Karl Fischer Reagent Titration Method) (Withdrawn 2021)
ASTM D 4175 : 2023 : EDT 1 Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
ASTM D 4052 : 1996 Standard Test Method for Density and Relative Density of Liquids by Digital Density Meter
ASTM D 4175 : 2023 : REV A Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
ASTM D 4307 : 2017 : R2021 Standard Practice for Preparation of Liquid Blends for Use as Analytical Standards
ASTM D 4175 : 2022 : EDT 1 Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
ASTM D 6299 : 2022 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 4626 : 2023 Standard Practice for Calculation of Gas Chromatographic Response Factors
ASTM D 6792 : 2022 Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories
ASTM D 4057 : 2022 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
ASTM E 1064 : 2023 Standard Test Method for Water in Organic Liquids by Coulometric Karl Fischer Titration
ASTM D 4052 : 2022 Standard Test Method for Density, Relative Density, and API Gravity of Liquids by Digital Density Meter
ASTM D 4806 : 2020 Standard Specification for Denatured Fuel Ethanol for Blending with Gasolines for Use as Automotive Spark-Ignition Engine Fuel
ASTM D 5798 : 2021 Standard Specification for Ethanol Fuel Blends for Flexible-Fuel Automotive Spark-Ignition Engines
ASTM E 355 : 1996 : R2014 Standard Practice for Gas Chromatography Terms and Relationships
ASTM D 6792 : 2023 Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories
ASTM D 6299 : 2020 : REV A Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 6792 : 2022 : REV A Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories
ASTM E 203 : 2024 Standard Test Method for Water Using Volumetric Karl Fischer Titration
ASTM E 1064 : 2016 Standard Test Method for Water in Organic Liquids by Coulometric Karl Fischer Titration
ASTM E 203 : 2016 Standard Test Method for Water Using Volumetric Karl Fischer Titration

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