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ASTM D 5630 : 2013

Superseded
Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

View Superseded by
superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

Standard Test Method for Ash Content in Plastics (Withdrawn 2022)
Available format(s)

Hardcopy , PDF

Superseded date

12-11-2022

Language(s)

English

Published date

11-04-2013

This test method was developed to determine the inorganic content of plastics by destructive ashing procedures.

1.1This test method was developed to determine the inorganic content of plastics by destructive ashing procedures. Ash levels of 0.01 % or above are covered by this test method.

1.2These ashing procedures are used only to quantify the residual solids in the polymer and can not be used to identify the individual chemical components of the ash, qualitatively.

1.3This test method is limited to those materials (including glass) that are stable to 900°C. Test Method D2584 is recommended for unknown samples, and in instances where fusion of the inorganic portions may be of concern.

1.4Fluorinated polymers and polymers containing halogenated components have not been included in these procedures.

1.5Two procedures for determining the inorganic residue in plastics are listed as follows:

1.5.1Procedure A, Muffle-Furnace Technique— For 5 – 50 gram samples. Samples are flamed over a burner prior to being ashed in a muffle furnace.

1.5.2Procedure B, Rapid-Ash Muffle-Furnace Technique— For 2–10 gram samples. Samples are ignited and ashed in a muffle furnace.

Note 1For more efficient ashing, the plastic sample should be in the form of powder or pellet.
Note 2This test method provides consistent results of filler content for a specific filler in a specific resin. However, this method may not provide the absolute filler content in all cases. This includes polymers filled with CaCO3, nano clays, and Carbon Black.
Note 3Procedure B is equivalent to ISO 3451/1-(E), Method A.

1.6The values stated in SI units are to be regarded as the standard.

1.7This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. See Section 9 for specific precautionary statements.

Committee
D 20
DocumentType
Test Method
Pages
5
PublisherName
American Society for Testing and Materials
Status
Superseded
SupersededBy
Supersedes

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ASTM F 628 : 2012 : EDT 3 Standard Specification for Acrylonitrile-Butadiene-Styrene (ABS) Schedule 40 Plastic Drain, Waste, and Vent Pipe With a Cellular Core (Withdrawn 2021)
ASTM D 4067 : 2016 Standard Classification System and Basis for Specification for Reinforced and Filled Poly(Phenylene Sulfide) (PPS) Injection Molding and Extrusion Materials Using ASTM Methods
ASTM D 5138 : 2016 Standard Classification System and Basis for Specification for Liquid Crystal Polymers Molding and Extrusion Materials (LCP)
ASTM D 4066 : 2013 : R2019 Standard Classification System for Nylon Injection and Extrusion Materials (PA)
ASTM D 6778 : 2020 Standard Classification System and Basis for Specification for Polyoxymethylene Molding and Extrusion Materials (POM)
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ASTM D 4101 : 2017 : EDT 1 Standard Classification System and Basis for Specification for Polypropylene Injection and Extrusion Materials
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ASTM D 1600 : 1999 Standard Terminology for Abbreviated Terms Relating to Plastics
ASTM D 2584 : 2002 Standard Test Method for Ignition Loss of Cured Reinforced Resins
ASTM D 2584 : 2008 Standard Test Method for Ignition Loss of Cured Reinforced Resins
ASTM D 2584 : 1994 Standard Test Method for Ignition Loss of Cured Reinforced Resins
ASTM E 691 : 2020 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
ASTM D 1600 : 2007 Standard Terminology for Abbreviated Terms Relating to Plastics
ASTM D 1600 : 2013 Standard Terminology for Abbreviated Terms Relating to Plastics
ASTM D 1600 : 2014 Standard Terminology for Abbreviated Terms Relating to Plastics
ASTM D 2584 : 2011 Standard Test Method for Ignition Loss of Cured Reinforced Resins
ASTM D 1600 : 2008 Standard Terminology for Abbreviated Terms Relating to Plastics
ASTM E 691 : 2019 : EDT 1 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
ASTM E 691 : 2009 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
ASTM D 2584 : 1968 Standard Method Of Test For Ignition Loss Of Cured Reinforced Resins
ASTM D 1600 : 2018 Standard Terminology for Abbreviated Terms Relating to Plastics (Withdrawn 2024)
ASTM E 691 : 2021 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
ASTM D 2584 : 2018 Standard Test Method for Ignition Loss of Cured Reinforced Resins

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