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  • ASTM D 5827 : 2009 : EDT 1

    Superseded A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.
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    Standard Test Method for Analysis of Engine Coolant for Chloride and Other Anions by Ion Chromatography

    Available format(s):  Hardcopy, PDF

    Superseded date:  11-11-2014

    Language(s):  English

    Published date:  01-03-2009

    Publisher:  American Society for Testing and Materials

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    Abstract - (Show below) - (Hide below)

    CONTAINED IN VOL. 15.05, 2015 Describes the chemical analysis of engine coolant for chloride ion by high-performance ion chromatography (HPIC).

    Scope - (Show below) - (Hide below)

    1.1 This test method covers the chemical analysis of engine coolant for chloride ion by high-performance ion chromatography (HPIC). Several other common anions found in engine coolant can be determined in one chromatographic analysis by this test method.

    1.2 This test method is applicable to both new and used engine coolant.

    1.3 Coelution of other ions may cause interferences for any of the listed anions. In the case of unfamiliar formulations, identification verification should be performed by either or both fortification and dilution of the sample matrix with the anions of interest.

    1.4 Analysis can be performed directly by this test method without pretreatment, other than dilution, as required by the linear ranges of the equipment. Table 1 indicates several applicable anions and approximate detection limits.

    1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

    1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to its use.

    TABLE 1 Analytes and Minimum Detection Limits

    AnalyteDetection Limit, mg/LA
    Chloride (Cl) 2.0
    Nitrite (NO2) 5.0
    Bromide (Br) 4.0
    Nitrate (NO3) 7.1
    o-Phosphate (HPO4)220.0
    Sulfate (SO4)2 8.0
    Oxalate (C2O4)212.0

    A Determined using 100-μL sample volume. Sample diluted 99 + 1 (v/v) with chromatographic eluant 30-μS/cm full scale, suppressed conductivity detection. Dionex AS4ASC column with AG4ASC guard columns. Other systems will require MDL determinations using chosen dilution factors, eluants, columns, and detector.

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    Committee D 15
    Document Type Test Method
    Product Note Reconfirmed EDT 1
    Publisher American Society for Testing and Materials
    Status Superseded
    Superseded By
    Supersedes

    Standards Referenced By This Book - (Show below) - (Hide below)

    ASTM D 7388 : 2018 Standard Specification for Engine Coolant Grade 1,3-Propanediol (PDO)
    ASTM E 1177 : 2014 Standard Specification for Engine Coolant Grade Glycol
    ASTM D 7517 : 2019 Standard Specification for Fully-Formulated 1,3 Propanediol (PDO) Base Engine Coolant for Heavy-Duty Engines
    ASTM D 7640 : 2016 Standard Specification for Engine Coolant Grade Glycerin
    ASTM D 8149 : 2017 Standard Practice for Optimization, Calibration, and Validation of Ion Chromatographic Determination of Heteroatoms and Anions in Petroleum Products and Lubricants
    ASTM D 3585 : 2008 : R2013 Standard Specification for ASTM Reference Fluid for Coolant Tests
    ASTM D 7328 : 2017 Standard Test Method for Determination of Existent and Potential Inorganic Sulfate and Total Inorganic Chloride in Fuel Ethanol by Ion Chromatography Using Aqueous Sample Injection
    ASTM D 7319 : 2017 Standard Test Method for Determination of Existent and Potential Sulfate and Inorganic Chloride in Fuel Ethanol and Butanol by Direct Injection Suppressed Ion Chromatography
    ASTM D 8116 : 2018 Standard Specification for Fully-Formulated Non-Aqueous Engine Coolant for Heavy-Duty Engines (Withdrawn 2019)
    ASTM D 8039 : 2016 Standard Specification for Heat Transfer Fluids (HTF) for Heating and Air Conditioning (HVAC) Systems
    ASTM D 4985 : 2010 : R2015 Standard Specification for Low Silicate Ethylene Glycol Base Engine Coolant for Heavy Duty Engines Requiring a Pre-Charge of Supplemental Coolant Additive (SCA)
    ASTM D 7518 : 2010 : R2015 : EDT 1 Standard Specification for 1,3 Propanediol (PDO) Base Engine Coolant for Automobile and Light-Duty Service
    ASTM D 7713 : 2018 Standard Specification for Aqueous Engine Coolant Grade Glycol (53 % by Volume Nominal)
    ASTM D 2847 : 2015 Standard Practice for Testing Engine Coolants in Car and Light Truck Service
    ASTM D 3306 : 2019 Standard Specification for Glycol Base Engine Coolant for Automobile and Light-Duty Service
    ASTM D 7714 : 2011 : R2016 : EDT 1 Standard Specification for Glycerin Base Engine Coolant for Automobile and Light-Duty Service
    ASTM D 5752 : 2010 : R2017 Standard Specification for Supplemental Coolant Additives (SCAs) for Use in Precharging Coolants for Heavy-Duty Engines
    ASTM D 8085 : 2017 Standard Specification for Non-Aqueous Engine Coolant for Automobile and Light-Duty Service

    Standards Referencing This Book - (Show below) - (Hide below)

    ASTM E 177 : 2014 : REDLINE Standard Practice for Use of the Terms Precision and Bias in ASTM Test Methods
    ASTM D 1176 : 2014 : REDLINE Standard Practice for Sampling and Preparing Aqueous Solutions of Engine Coolants or Antirusts for Testing Purposes
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