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ASTM D 6299 : 2002 : EDT 1

Superseded
Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

View Superseded by
superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

Standard Practice for Applying Statistical Quality Assurance Techniques to Evaluate Analytical Measurement System Performance
Available format(s)

Hardcopy , PDF

Superseded date

11-11-2014

Language(s)

English

Published date

10-06-2002

1.1 This practice provides information for the design and operation of a program to monitor and control ongoing stability and precision and bias performance of selected analytical measurement systems using a collection of generally accepted statistical quality control (SQC) procedures and tools.

Note 1—A complete list of criteria for selecting measurement systems to which this practice should be applied and for determining the frequency at which it should be applied is beyond the scope of this practice. However, some factors to be considered include (1) frequency of use of the analytical measurement system, (2) criticality of the parameter being measured, (3) system stability and precision performance based on historical data, (4) business economics, and (5) regulatory, contractual, or test method requirements.

1.2 This practice is applicable to stable analytical measurement systems that produce results on a continuous numerical scale.

1.3 This practice is applicable to laboratory test methods.

1.4 This practice is applicable to validated process stream analyzers.

Note 2—For validation of univariate process stream analyzers, see also Practice D 3764.

1.5 This practice assumes that the normal (Gaussian) model is adequate for the description and prediction of measurement system behavior when it is in a state of statistical control.

Note 3—For non-Gaussian processes, transformations of test results may permit proper application of these tools. Consult a statistician for further guidance and information.

1.6 This practice does not address statistical techniques for comparing two or more analytical measurement systems applying different analytical techniques or equipment components that purport to measure the same property(s).

Committee
D 02
DocumentType
Standard Practice
Pages
22
PublisherName
American Society for Testing and Materials
Status
Superseded
SupersededBy
Supersedes

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ASTM D 8071 : 2017 Standard Test Method for Determination of Hydrocarbon Group Types and Select Hydrocarbon and Oxygenate Compounds in Automotive Spark-Ignition Engine Fuel Using Gas Chromatography with Vacuum Ultraviolet Absorption Spectroscopy Detection (GC-VUV)
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ASTM D 5191 : 2019 Standard Test Method for Vapor Pressure of Petroleum Products and Liquid Fuels (Mini Method)
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ASTM D 8150 : 2017 Standard Test Method for Determination of Organic Chloride Content in Crude Oil by Distillation Followed by Detection Using Combustion Ion Chromatography
ASTM D 2700 : 2019 Standard Test Method for Motor Octane Number of Spark-Ignition Engine Fuel
ASTM D 7423 : 2017 Standard Test Method for Determination of Oxygenates in C2, C3, C4, and C5 Hydrocarbon Matrices by Gas Chromatography and Flame Ionization Detection
ASTM D 7623 : 2010 : R2015 Standard Test Method for Total Mercury in Crude Oil Using Combustion-Gold Amalgamation and Cold Vapor Atomic Absorption Method
ASTM D 7591 : 2012 : R2017 Standard Test Method for Determination of Free and Total Glycerin in Biodiesel Blends by Anion Exchange Chromatography
ASTM D 7920 : 2015 : EDT 1 Standard Test Method for Determination of Fuel Methanol (M99) and Methanol Fuel Blends (M10 to M99) by Gas Chromatography
ASTM D 7372 : 2017 Standard Guide for Analysis and Interpretation of Proficiency Test Program Results
ASTM F 2980 : 2013 : R2017 Standard Test Method for Analysis of Heavy Metals in Glass by Field Portable X-Ray Fluorescence (XRF)
ASTM D 3246 : 2015 Standard Test Method for Sulfur in Petroleum Gas by Oxidative Microcoulometry (Withdrawn 2024)
ASTM D 3828 : 2016 : REV A Standard Test Methods for Flash Point by Small Scale Closed Cup Tester
ASTM F 3078 : 2015 Standard Test Method for Identification and Quantification of Lead in Paint and Similar Coating Materials using Energy Dispersive X-ray Fluorescence Spectrometry (EDXRF)
ASTM D 7622 : 2010 : R2015 Standard Test Method for Total Mercury in Crude Oil Using Combustion and Direct Cold Vapor Atomic Absorption Method with Zeeman Background Correction
ASTM D 5863 : 2000 : REV A : R2016 Standard Test Methods for Determination of Nickel, Vanadium, Iron, and Sodium in Crude Oils and Residual Fuels by Flame Atomic Absorption Spectrometry
ASTM D 7111 : 2016 Standard Test Method for Determination of Trace Elements in Middle Distillate Fuels by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES)
ASTM D 7170 : 2016 Standard Test Method for Determination of Derived Cetane Number (DCN) of Diesel Fuel Oils—Fixed Range Injection Period, Constant Volume Combustion Chamber Method (Withdrawn 2019)
ASTM D 4294 : 2016 : EDT 1 Standard Test Method for Sulfur in Petroleum and Petroleum Products by Energy Dispersive X-ray Fluorescence Spectrometry
ASTM D 4057 : 2012 : R2018 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
ASTM E 2469 : 2016 Standard Test Method for Chloride in Mono-, Di- and Tri-ethylene Glycol by Ion Chromatography
ASTM D 7371 : 2014 Standard Test Method for Determination of Biodiesel (Fatty Acid Methyl Esters) Content in Diesel Fuel Oil Using Mid Infrared Spectroscopy (FTIR-ATR-PLS Method)
ASTM D 7040 : 2004 : R2015 Standard Test Method for Determination of Low Levels of Phosphorus in ILSAC GF 4 and Similar Grade Engine Oils by Inductively Coupled Plasma Atomic Emission Spectrometry
ASTM D 7862 : 2019 Standard Specification for Butanol for Blending with Gasoline for Use as Automotive Spark-Ignition Engine Fuel
ASTM D 8267 : 2019 Standard Test Method for Determination of Saturated Hydrocarbon, Aromatic, and Diaromatic Content of Aviation Turbine Fuels Using Gas Chromatography with Vacuum Ultraviolet Absorption Spectroscopy Detection (GC-VUV)
ASTM D 8185 : 2018 Standard Guide for In-Service Lubricant Viscosity Measurement
ASTM D 7861 : 2014 : R2019 Standard Test Method for Determination of Fatty Acid Methyl Esters (FAME) in Diesel Fuel by Linear Variable Filter (LVF) Array Based Mid-Infrared Spectroscopy
ASTM D 8088 : 2016 Standard Practice for Determination of the Six Major Rare Earth Elements in Fluid Catalytic Cracking Catalysts, Zeolites, Additives, and Related Materials by Inductively Coupled Plasma Optical Emission Spectroscopy
ASTM D 1018 : 2011 : R2016 Standard Test Method for Hydrogen In Petroleum Fractions (Withdrawn 2021)
ASTM D 7828 : 2012 Standard Test Method for Determination of Residue Composition in Liquefied Petroleum Gas (LPG) Using Automated Thermal Desorption/Gas Chromatography (ATD/GC) (Withdrawn 2021)
ASTM D 5708 : 2015 Standard Test Methods for Determination of Nickel, Vanadium, and Iron in Crude Oils and Residual Fuels by Inductively Coupled Plasma (ICP) Atomic Emission Spectrometry
ASTM D 7807 : 2012 Standard Test Method for Determination of Boiling Range Distribution of Hydrocarbon and Sulfur Components of Petroleum Distillates by Gas Chromatography and Chemiluminescence Detection
ASTM D 5501 : 2012 : R2016 Standard Test Method for Determination of Ethanol and Methanol Content in Fuels Containing Greater than 20% Ethanol by Gas Chromatography
ASTM D 6550 : 2015 Standard Test Method for Determination of Olefin Content of Gasolines by Supercritical-Fluid Chromatography
ASTM D 2622 : 2016 Standard Test Method for Sulfur in Petroleum Products by Wavelength Dispersive X-ray Fluorescence Spectrometry
ASTM D 6278 : 2017 : EDT 1 Standard Test Method for Shear Stability of Polymer Containing Fluids Using a European Diesel Injector Apparatus
ASTM D 7319 : 2017 Standard Test Method for Determination of Existent and Potential Sulfate and Inorganic Chloride in Fuel Ethanol and Butanol by Direct Injection Suppressed Ion Chromatography
ASTM D 1218 : 2012 : R2016 Standard Test Method for Refractive Index and Refractive Dispersion of Hydrocarbon Liquids
ASTM D 8001 : 2016 : EDT 1 Standard Test Method for Determination of Total Nitrogen, Total Kjeldahl Nitrogen by Calculation, and Total Phosphorus in Water, Wastewater by Ion Chromatography
ASTM D 3231 : 2018 Standard Test Method for Phosphorus in Gasoline

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