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  • ASTM D 7039 : 2015 : REV A

    Superseded A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.
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    Standard Test Method for Sulfur in Gasoline, Diesel Fuel, Jet Fuel, Kerosine, Biodiesel, Biodiesel Blends, and Gasoline-Ethanol Blends by Monochromatic Wavelength Dispersive X-ray Fluorescence Spectrometry

    Available format(s):  Hardcopy, PDF

    Superseded date:  10-08-2020

    Language(s):  English

    Published date:  01-07-2015

    Publisher:  American Society for Testing and Materials

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    1.1This test method covers the determination of total sulfur by monochromatic wavelength-dispersive X-ray fluorescence (MWDXRF) spectrometry in single-phase gasoline, diesel fuel, refinery process streams used to blend gasoline and diesel, jet fuel, kerosine, biodiesel, biodiesel blends, and gasoline-ethanol blends.

    Note 1:Volatile samples such as high-vapor-pressure gasolines or light hydrocarbons might not meet the stated precision because of the evaporation of light components during the analysis.

    1.2The range of this test method is between the pooled limit of quantitation (PLOQ) value (calculated by procedures consistent with Practice D6259) of 3.2 mg/kg total sulfur and the highest level sample in the round robin, 2822 mg/kg total sulfur.

    1.3Samples containing oxygenates can be analyzed with this test method provided the matrix of the calibration standards is either matched to the sample matrices or the matrix correction described in Section 5 or Annex A1 is applied to the results. The conditions for matrix matching and matrix correction are provided in the Interferences section (Section 5).

    1.4Samples with sulfur content above 2822 mg/kg can be analyzed after dilution with appropriate solvent (see 5.4). The precision and bias of sulfur determinations on diluted samples has not been determined and may not be the same as shown for neat samples (Section 15).

    1.5When the elemental composition of the samples differ significantly from the calibration standards used to prepare the calibration curve, the cautions and recommendation in Section 5 should be carefully observed.

    1.6The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.

    1.7This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific hazard information, see 3.1.

    General Product Information - (Show below) - (Hide below)

    Committee D 02
    Document Type Test Method
    Publisher American Society for Testing and Materials
    Status Superseded
    Superseded By
    Supersedes

    Standards Referenced By This Book - (Show below) - (Hide below)

    ASTM D 4806 : 2019 Standard Specification for Denatured Fuel Ethanol for Blending with Gasolines for Use as Automotive Spark-Ignition Engine Fuel
    ASTM D 4814 : 2019 Standard Specification for Automotive Spark-Ignition Engine Fuel
    ASTM D 7455 : 2019 Standard Practice for Sample Preparation of Petroleum and Lubricant Products for Elemental Analysis
    ASTM D 4868 : 2017 Standard Test Method for Estimation of Net and Gross Heat of Combustion of Hydrocarbon Burner and Diesel Fuels
    ASTM D 7578 : 2018 Standard Guide for Calibration Requirements for Elemental Analysis of Petroleum Products and Lubricants
    ASTM D 4529 : 2017 Standard Test Method for Estimation of Net Heat of Combustion of Aviation Fuels
    ASTM D 396 : 2019 Standard Specification for Fuel Oils
    ASTM D 8076 : 2018 Standard Specification for 100 Research Octane Number Test Fuel for Automotive Spark-Ignition Engines
    ASTM D 8048 : 2019 Standard Test Method for Evaluation of Diesel Engine Oils in T-13 Diesel Engine
    ASTM D 7343 : 2018 Standard Practice for Optimization, Sample Handling, Calibration, and Validation of X-ray Fluorescence Spectrometry Methods for Elemental Analysis of Petroleum Products and Lubricants
    ASTM D 8048 : 2019 : REV A Standard Test Method for Evaluation of Diesel Engine Oils in T-13 Diesel Engine
    ASTM D 396 : 2019 : REV A Standard Specification for Fuel Oils
    ASTM D 8076 : 2019 : REV A Standard Specification for 100 Research Octane Number Test Fuel for Automotive Spark-Ignition Engines

    Standards Referencing This Book - (Show below) - (Hide below)

    ASTM D 4057 : 2019 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
    ASTM D 6300 : 2013 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
    ASTM D 4057 : 1995 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
    ASTM D 7343 : 2007 Standard Practice for Optimization, Sample Handling, Calibration, and Validation of X-ray Fluorescence Spectrometry Methods for Elemental Analysis of Petroleum Products and Lubricants
    ASTM D 6299 : 2010 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 6300 : 2014 : REV A : EDT 1 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
    ASTM D 6299 : 2013 : EDT 1 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 6259 : 1998 : R2004 Standard Practice for Determination of a Pooled Limit of Quantitation
    ASTM D 4177 : 2016 : EDT 1 Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
    ASTM D 6299 : 2017 : REV A Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 6299 : 2017 : REV B Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 6300 : 2017 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
    ASTM D 6299 : 2009 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 4177 : 1995 Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
    ASTM D 6300 : 2017 : REV A Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
    ASTM D 4057 : 2012 : R2018 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
    ASTM D 6299 : 2013 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 6299 : 2010 : EDT 1 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 6300 : 2016 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
    ASTM D 4057 : 1981 : EDT 2 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
    ASTM D 6300 : 2004 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
    ASTM D 6259 : 2015 Standard Practice for Determination of a Pooled Limit of Quantitation for a Test Method
    ASTM D 6300 : 2019 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
    ASTM D 6300 : 2019 : REV A Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
    ASTM D 6300 : 2020 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products, Liquid Fuels, and Lubricants
    ASTM D 6299 : 2000 Standard Practice for Applying Statistical Quality Assurance Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 6259 : 1998 Standard Practice for Determination of a Pooled Limit of Quantitation
    ASTM D 6299 : 2010 : EDT 2 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 6299 : 2016 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 4057 : 2006 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
    ASTM D 4177 : 2015 Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
    ASTM D 6299 : 2019 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 6259 : 1998 : R2010 Standard Practice for Determination of a Pooled Limit of Quantitation
    ASTM D 4057 : 2012 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
    ASTM D 6299 : 2000 : REV A Standard Practice for Applying Statistical Quality Assurance Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 6300 : 2006 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
    ASTM D 6300 : 2014 : REV A Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
    ASTM D 6300 : 2015 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
    ASTM D 6300 : 1999 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
    ASTM D 6299 : 2020 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 4177 : 1995 : R2010 Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
    ASTM D 6259 : 2015 : R2019 Standard Practice for Determination of a Pooled Limit of Quantitation for a Test Method
    ASTM D 6299 : 2008 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 4177 : 1995 : R2000 Standard Practice for Automatic Sampling of Peroleum and Petroleum Products
    ASTM D 7343 : 2018 Standard Practice for Optimization, Sample Handling, Calibration, and Validation of X-ray Fluorescence Spectrometry Methods for Elemental Analysis of Petroleum Products and Lubricants
    ASTM D 6300 : 2013 : REV A Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
    ASTM D 7343 : 2012 Standard Practice for Optimization, Sample Handling, Calibration, and Validation of X-ray Fluorescence Spectrometry Methods for Elemental Analysis of Petroleum Products and Lubricants
    ASTM D 6299 : 2002 : EDT 1 Standard Practice for Applying Statistical Quality Assurance Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 7343 : 2012 : R2017 Standard Practice for Optimization, Sample Handling, Calibration, and Validation of X-ray Fluorescence Spectrometry Methods for Elemental Analysis of Petroleum Products and Lubricants
    ASTM D 6300 : 2008 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
    ASTM D 6300 : 2003 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
    ASTM D 6300 : 2007 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
    ASTM D 6300 : 2002 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
    ASTM D 4177 : 2016 Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
    ASTM D 4177 : 1995 : R2005 Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
    ASTM D 6300 : 2016 : REV A Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
    ASTM D 6299 : 2007 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 6299 : 2007 : EDT 1 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 4057 : 1995 : R2000 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
    ASTM D 6299 : 2017 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 4177 : 2015 : REV A Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
    ASTM D 6300 : 2014 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
    ASTM D 4057 : 2006 : R2011 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
    ASTM D 6299 : 2002 Standard Practice for Applying Statistical Quality Assurance Techniques to Evaluate Analytical Measurement System Performance
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