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ASTM D 7039 : 2015 : REV A : R2020

Current
Current

The latest, up-to-date edition.

Standard Test Method for Sulfur in Gasoline, Diesel Fuel, Jet Fuel, Kerosine, Biodiesel, Biodiesel Blends, and Gasoline-Ethanol Blends by Monochromatic Wavelength Dispersive X-ray Fluorescence Spectrometry
Available format(s)

Hardcopy , PDF

Language(s)

English

Published date

01-05-2020

1.1This test method covers the determination of total sulfur by monochromatic wavelength-dispersive X-ray fluorescence (MWDXRF) spectrometry in single-phase gasoline, diesel fuel, refinery process streams used to blend gasoline and diesel, jet fuel, kerosine, biodiesel, biodiesel blends, and gasoline-ethanol blends.

Note 1:Volatile samples such as high-vapor-pressure gasolines or light hydrocarbons might not meet the stated precision because of the evaporation of light components during the analysis.

1.2The range of this test method is between the pooled limit of quantitation (PLOQ) value (calculated by procedures consistent with Practice D6259) of 3.2 mg/kg total sulfur and the highest level sample in the round robin, 2822 mg/kg total sulfur.

1.3Samples containing oxygenates can be analyzed with this test method provided the matrix of the calibration standards is either matched to the sample matrices or the matrix correction described in Section 5 or Annex A1 is applied to the results. The conditions for matrix matching and matrix correction are provided in the Interferences section (Section 5).

1.4Samples with sulfur content above 2822 mg/kg can be analyzed after dilution with appropriate solvent (see 5.4). The precision and bias of sulfur determinations on diluted samples has not been determined and may not be the same as shown for neat samples (Section 15).

1.5When the elemental composition of the samples differ significantly from the calibration standards used to prepare the calibration curve, the cautions and recommendation in Section 5 should be carefully observed.

1.6The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.

1.7This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific hazard information, see 3.1.

1.8This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

Committee
D 02
DocumentType
Test Method
Pages
12
PublisherName
American Society for Testing and Materials
Status
Current
Supersedes

ASTM D 7455 : 2019 Standard Practice for Sample Preparation of Petroleum and Lubricant Products for Elemental Analysis
ASTM D 8076 : 2019 : REV A Standard Specification for 100 Research Octane Number Test Fuel for Automotive Spark-Ignition Engines
ASTM D 4868 : 2017 Standard Test Method for Estimation of Net and Gross Heat of Combustion of Hydrocarbon Burner and Diesel Fuels
ASTM D 4529 : 2017 Standard Test Method for Estimation of Net Heat of Combustion of Aviation Fuels
ASTM D 8048 : 2019 : REV A Standard Test Method for Evaluation of Diesel Engine Oils in T-13 Diesel Engine
ASTM D 7343 : 2018 Standard Practice for Optimization, Sample Handling, Calibration, and Validation of X-ray Fluorescence Spectrometry Methods for Elemental Analysis of Petroleum Products and Lubricants
ASTM D 396 : 2019 : REV A Standard Specification for Fuel Oils

ASTM D 4057 : 2019 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
ASTM D 7343 : 2020 Standard Practice for Optimization, Sample Handling, Calibration, and Validation of X-ray Fluorescence Spectrometry Methods for Elemental Analysis of Petroleum Products and Lubricants
ASTM D 6299 : 2021 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 6299 : 2022 : EDT 1 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 6299 : 2023 : REV A Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 6300 : 2021 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products, Liquid Fuels, and Lubricants
ASTM D 6300 : 2023 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products, Liquid Fuels, and Lubricants
ASTM D 6300 : 2023 : REV A Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products, Liquid Fuels, and Lubricants
ASTM D 6300 : 2020 : REV B Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products, Liquid Fuels, and Lubricants
ASTM D 6299 : 2023 : EDT 1 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 6300 : 1999 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
ASTM D 4177 : 2022 Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
ASTM D 6299 : 2023 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 6259 : 2015 : R2019 Standard Practice for Determination of a Pooled Limit of Quantitation for a Test Method
ASTM D 6259 : 2023 Standard Practice for Determination of a Pooled Limit of Quantitation for a Test Method
ASTM D 6299 : 2022 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 4057 : 2022 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
ASTM D 4177 : 2020 Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
ASTM D 6299 : 2020 : REV A Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 4177 : 2022 : EDT 1 Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
ASTM D 6300 : 2024 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products, Liquid Fuels, and Lubricants

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