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  • ASTM D 7528 : 2017 : REV A

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    Standard Test Method for Bench Oxidation of Engine Oils by ROBO Apparatus

    Available format(s):  Hardcopy, PDF

    Superseded date:  11-01-2021

    Language(s):  English

    Published date:  17-10-2017

    Publisher:  American Society for Testing and Materials

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    1.1This test method describes a bench procedure to simulate the oil aging encountered in Test Method D7320, the Sequence IIIG engine test method. These aged oils are then tested for kinematic viscosity and for low-temperature pumpability properties as described in the Sequence IIIGA engine test, Appendix X1 of Test Method D7320.

    1.2Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

    1.2.1Exceptions—There are no SI equivalents for some apparatus in Section 6, and there are some figures where inch units are to be regarded as standard.

    1.3This test method is arranged as follows:

    Section

    Scope

    1

    Reference Documents

    2

    Terminology

    3

    Summary of Test Method

    4

    Significance and Use

    5

    Apparatus

    6

    Reagents and Materials

    7

    Hazards

    8

    New and Existing Test Stand Calibration

    9

    Procedure

    10

    Cleaning

    11

    Calculations and Determination of Test Results

    12

    Report

    13

    Precision and Bias

    14

    Keywords

    15

    Annexes

    ASTM Test Monitoring Center: Organization

    Annex A1

    ASTM Test Monitoring Center: Calibration Procedures

    Annex A2

    ASTM Test Monitoring Center: Maintenance Activities

    Annex A3

    ASTM Test Monitoring Center: Related Information

    Annex A4

    Reaction Vessel

    Annex A5

    Reaction Vessel Head

    Annex A6

    Reaction Vessel-to-Head Seal

    Annex A7

    Agitator Turbine Blade

    Annex A8

    Agitator Packing Gland

    Annex A9

    Nitrogen Dioxide Graduated Tube

    Annex A10

    Vacuum System Plumbing

    Annex A11

    Vacuum Trap Condensers

    Annex A12

    Setting the Vacuum Control Valve

    Annex A13

    Appendixes

    Sample Preparation and Addition

    Appendix X1

    Charging the Liquid Nitrogen Dioxide

    Appendix X2

    Nitrogen Dioxide Precision Needle Valve

    Appendix X3

    Example of an Assembled ROBO Apparatus

    Appendix X4

    Information Package to Aid Setting Up a New Robo Apparatus

    Appendix X5

    1.4This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific warning statements are given in Sections 7 and 8.

    1.5This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

    General Product Information - (Show below) - (Hide below)

    Committee D 02
    Document Type Test Method
    Publisher American Society for Testing and Materials
    Status Superseded
    Superseded By
    Supersedes

    Standards Referencing This Book - (Show below) - (Hide below)

    ASTM D 4175 : 2020 Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
    ASTM D 7320 : 2011 Standard Test Method for Evaluation of Automotive Engine Oils in the Sequence IIIG, Spark-Ignition Engine
    ASTM D 4175 : 2014 Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
    ASTM D 4485 : 2003 : REV A Standard Specification for Performance of Engine Oils
    ASTM D 4175 : 2009 : REV A : EDT 1 Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
    ASTM D 4684 : 2002 Standard Test Method for Determination of Yield Stress and Apparent Viscosity of Engine Oils at Low Temperature
    ASTM D 4175 : 2008 : REV B : EDT 1 Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
    ASTM D 4485 : 2006 Standard Specification for Performance of Engine Oils
    ASTM D 4175 : 2005 Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
    ASTM D 4485 : 2011 : REV C Standard Specification for Performance of Active API Service Category Engine Oils
    ASTM D 4175 : 2005 : EDT 2 Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
    ASTM D 4485 : 2001 Standard Specification for Performance of Engine Oils
    ASTM D 4175 : 2015 : REV C Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
    ASTM D 4175 : 2017 : REV A : EDT 1 Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
    ASTM D 4485 : 2003 Standard Specification for Performance of Engine Oils
    ASTM D 4485 : 2008 Standard Specification for Performance of Engine Oils
    ASTM D 4485 : 2015 Standard Specification for Performance of Active API Service Category Engine Oils
    ASTM D 4485 : 2005 : REV A Standard Specification for Performance of Engine Oils
    ASTM D 4684 : 2008 Standard Test Method for Determination of Yield Stress and Apparent Viscosity of Engine Oils at Low Temperature
    ASTM D 4175 : 2008 : REV A Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
    ASTM D 4175 : 2020 : REV A Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
    ASTM D 4684 : 2020 Standard Test Method for Determination of Yield Stress and Apparent Viscosity of Engine Oils at Low Temperature
    ASTM D 4175 : 2017 : REV B Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
    ASTM D 4175 : 2009 Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
    ASTM D 4485 : 2011 : REV A Standard Specification for Performance of Active API Service Category Engine Oils
    ASTM D 5293 : 2010 : EDT 1 Standard Test Method for Apparent Viscosity of Engine Oils and Base Stocks Between –5 and –35°C Using Cold-Cranking Simulator
    ASTM D 7320 : 2014 Standard Test Method for Evaluation of Automotive Engine Oils in the Sequence IIIG, Spark-Ignition Engine
    ASTM D 4485 : 2018 Standard Specification for Performance of Active API Service Category Engine Oils
    ASTM D 5293 : 2020 Standard Test Method for Apparent Viscosity of Engine Oils and Base Stocks Between –10 °C and –35 °C Using Cold-Cranking Simulator
    ASTM D 4175 : 2009 : REV A : EDT 4 Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
    ASTM D 4175 : 2009 : REV A : EDT 3 Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
    ASTM D 4485 : 2011 : REV B Standard Specification for Performance of Active API Service Category Engine Oils
    ASTM D 4684 : 2007 Standard Test Method for Determination of Yield Stress and Apparent Viscosity of Engine Oils at Low Temperature
    ASTM D 4485 : 2016 Standard Specification for Performance of Active API Service Category Engine Oils
    ASTM D 4175 : 2018 Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
    ASTM D 4485 : 2007 Standard Specification for Performance of Engine Oils
    ASTM D 4485 : 2010 Standard Specification for Performance of Engine Oils
    ASTM D 4485 : 2001 : REV A Standard Specification for Performance of Engine Oils
    ASTM D 4175 : 2001 : EDT 1 Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
    ASTM D 4684 : 2017 Standard Test Method for Determination of Yield Stress and Apparent Viscosity of Engine Oils at Low Temperature
    ASTM D 4175 : 2001 Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
    ASTM D 4175 : 2005 : EDT 1 Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
    ASTM D 4175 : 2002 Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
    ASTM D 7320 : 2015 : REV A Standard Test Method for Evaluation of Automotive Engine Oils in the Sequence IIIG, Spark-Ignition Engine
    ASTM D 4485 : 2004 Standard Specification for Performance of Engine Oils
    ASTM D 5293 : 2014 Standard Test Method for Apparent Viscosity of Engine Oils and Base Stocks Between –5°C and –35°C Using Cold-Cranking Simulator
    ASTM D 7320 : 2016 Standard Test Method for Evaluation of Automotive Engine Oils in the Sequence IIIG, Spark-Ignition Engine
    ASTM D 4684 : 2012 Standard Test Method for Determination of Yield Stress and Apparent Viscosity of Engine Oils at Low Temperature
    ASTM D 7320 : 2015 Standard Test Method for Evaluation of Automotive Engine Oils in the Sequence IIIG, Spark-Ignition Engine
    ASTM D 4175 : 2015 Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
    ASTM D 4485 : 2000 Standard Specification for Performance of Engine Oils
    ASTM D 4175 : 2002 : REV A : EDT 2 Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
    ASTM D 5293 : 2008 : EDT 1 Standard Test Method for Apparent Viscosity of Engine Oils Between -5 and -35°C Using the Cold-Cranking Simulator
    ASTM D 4485 : 2015 : REV A Standard Specification for Performance of Active API Service Category Engine Oils
    ASTM D 7320 : 2007 : REV A Standard Test Method for Evaluation of Automotive Engine Oils in the Sequence IIIG, Spark-Ignition Engine
    ASTM D 5293 : 2017 : REV A Standard Test Method for Apparent Viscosity of Engine Oils and Base Stocks Between –10 °C and –35 °C Using Cold-Cranking Simulator
    ASTM D 4684 : 2014 Standard Test Method for Determination of Yield Stress and Apparent Viscosity of Engine Oils at Low Temperature
    ASTM D 4175 : 2009 : REV A : EDT 5 Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
    ASTM D 4175 : 2016 : REV C Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
    ASTM D 4175 : 2015 : REV B Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
    ASTM D 7320 : 2011 : REV A Standard Test Method for Evaluation of Automotive Engine Oils in the Sequence IIIG, Spark-Ignition Engine
    ASTM D 7320 : 2006 Standard Test Method for Evaluation of Automotive Engine Oils in the Sequence IIIG, Spark-Ignition Engine
    ASTM D 7320 : 2017 Standard Test Method for Evaluation of Automotive Engine Oils in the Sequence IIIG, Spark-Ignition Engine
    ASTM D 4175 : 2015 : REV A Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
    ASTM D 4485 : 2006 : REV A Standard Specification for Performance of Engine Oils
    ASTM D 4684 : 2002 : REV A Standard Test Method for Determination of Yield Stress and Apparent Viscosity of Engine Oils at Low Temperature
    ASTM D 4175 : 2009 : REV A Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
    ASTM D 4175 : 2016 : REV B Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
    ASTM D 4175 : 2002 : REV A : EDT 1 Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
    ASTM D 4175 : 2008 Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
    ASTM D 5293 : 2009 Standard Test Method for Apparent Viscosity of Engine Oils Between -5 and -35°C Using the Cold-Cranking Simulator
    ASTM D 4175 : 2002 : REV A Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
    ASTM D 4175 : 2000 : EDT 1 Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
    ASTM D 4175 : 2016 : REV A Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
    ASTM D 4684 : 2007 : EDT 1 Standard Test Method for Determination of Yield Stress and Apparent Viscosity of Engine Oils at Low Temperature
    ASTM D 4684 : 1999 : EDT 1 Standard Test Method for Determination of Yield Stress and Apparent Viscosity of Engine Oils at Low Temperature
    ASTM D 4175 : 2019 : EDT 1 Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
    ASTM D 7320 : 2009 : REV A Standard Test Method for Evaluation of Automotive Engine Oils in the Sequence IIIG, Spark-Ignition Engine
    ASTM D 4485 : 2018 : REV A Standard Specification for Performance of Active API Service Category Engine Oils
    ASTM D 7320 : 2013 Standard Test Method for Evaluation of Automotive Engine Oils in the Sequence IIIG, Spark-Ignition Engine
    ASTM D 5293 : 1999 : REV A : EDT 1 Standard Test Method for Apparent Viscosity of Engine Oils Between -5 and -35oC Using the Cold-Cranking Simulator
    ASTM D 4485 : 2005 Standard Specification for Performance of Engine Oils
    ASTM D 4684 : 2017 : REV A Standard Test Method for Determination of Yield Stress and Apparent Viscosity of Engine Oils at Low Temperature
    ASTM D 7320 : 2008 : REV A Standard Test Method for Evaluation of Automotive Engine Oils in the Sequence IIIG, Spark-Ignition Engine
    ASTM D 5293 : 2017 : EDT 1 Standard Test Method for Apparent Viscosity of Engine Oils and Base Stocks Between –10 °C and –35 °C Using Cold-Cranking Simulator
    ASTM D 4485 : 2014 Standard Specification for Performance of Active API Service Category Engine Oils
    ASTM D 4485 : 2002 Standard Specification for Performance of Engine Oils
    ASTM D 4175 : 2017 : REV A Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
    ASTM D 7320 : 2018 Standard Test Method for Evaluation of Automotive Engine Oils in the Sequence IIIG, Spark-Ignition Engine
    ASTM D 4485 : 2005 : EDT 1 Standard Specification for Performance of Engine Oils
    ASTM D 4175 : 2009 : REV A : EDT 2 Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
    ASTM D 7320 : 2017 : REV A Standard Test Method for Evaluation of Automotive Engine Oils in the Sequence IIIG, Spark-Ignition Engine
    ASTM D 4175 : 2018 : EDT 1 Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
    ASTM D 4175 : 2016 Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
    ASTM D 5293 : 2004 Standard Test Method for Apparent Viscosity of Engine Oils Between -5 and -35°C Using the Cold-Cranking Simulator
    ASTM D 5293 : 2015 Standard Test Method for Apparent Viscosity of Engine Oils and Base Stocks Between –10 °C and –35 °C Using Cold-Cranking Simulator
    ASTM D 4684 : 2018 Standard Test Method for Determination of Yield Stress and Apparent Viscosity of Engine Oils at Low Temperature
    ASTM D 5293 : 2008 Standard Test Method for Apparent Viscosity of Engine Oils Between -5 and -35°C Using the Cold-Cranking Simulator
    ASTM D 7320 : 2012 : REV A Standard Test Method for Evaluation of Automotive Engine Oils in the Sequence IIIG, Spark-Ignition Engine
    ASTM D 4175 : 2017 Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
    ASTM D 7320 : 2010 : REV B Standard Test Method for Evaluation of Automotive Engine Oils in the Sequence IIIG, Spark-Ignition Engine
    ASTM D 5293 : 2010 Standard Test Method for Apparent Viscosity of Engine Oils Between -5 and -35°C Using the Cold-Cranking Simulator
    ASTM D 7320 : 2016 : REV A Standard Test Method for Evaluation of Automotive Engine Oils in the Sequence IIIG, Spark-Ignition Engine
    ASTM D 7320 : 2010 : REV A Standard Test Method for Evaluation of Automotive Engine Oils in the Sequence IIIG, Spark-Ignition Engine
    ASTM D 4175 : 2019 Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
    ASTM D 4485 : 2009 Standard Specification for Performance of Engine Oils
    ASTM D 4485 : 2019 Standard Specification for Performance of Active API Service Category Engine Oils
    ASTM D 4175 : 2015 : REV B : EDT 1 Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
    ASTM D 4485 : 2010 : REV A Standard Specification for Performance of Engine Oils
    ASTM D 5293 : 2017 Standard Test Method for Apparent Viscosity of Engine Oils and Base Stocks Between –10 °C and –35 °C Using Cold-Cranking Simulator
    ASTM D 5293 : 2002 Standard Test Method for Apparent Viscosity of Engine Oils Between -5 and -35°C Using the Cold-Cranking Simulator
    ASTM D 4485 : 2011 Standard Specification for Performance of Engine Oils
    ASTM D 4175 : 2008 : REV B Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
    ASTM D 4485 : 2007 : REV A Standard Specification for Performance of Engine Oils
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