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ASTM D 7756 : 2019

Current
Current

The latest, up-to-date edition.

Standard Test Method for Residues in Liquefied Petroleum (LP) Gases by Gas Chromatography with Liquid, On-Column Injection
Available format(s)

Hardcopy , PDF

Language(s)

English

Published date

18-06-2019

This test method covers the determination, by gas chromatography, of soluble hydrocarbon materials, sometimes called “oily residue,” which can be present in liquefied petroleum (LP) gases and which are substantially less volatile than the LPG product.

1.1This test method covers the determination, by gas chromatography, of soluble hydrocarbon materials, sometimes called “oily residue,” which can be present in liquefied petroleum (LP) gases and which are substantially less volatile than the LPG product.

1.2This test method quantifies, in the range of 10 mg/kg to 600 mg/kg (ppm mass), the residue with a boiling point between 174 °C and 522 °C (C10 to C40) in LPG. Higher boiling materials, or materials that adhere permanently to the chromatographic column, will not be detected.

1.3Appendix X3, Appendix X4, and Appendix X6 describe additional applications which could be performed based on the hardware and procedures described in this test method. Appendix X3 describes a test procedure for expanding the analysis range to benzene, Appendix X4 describes a test procedure for the analysis of diisopropanolamine, and Appendix X6 describes a test procedure for the analysis of heavy residues or contaminants from C40 to about C60 in LPG.

1.4The values stated in SI units are to be regarded as standard. The values given in parentheses after SI units are provided for information only and are not considered standard.

1.5This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.

1.6This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

Committee
D 02
DocumentType
Test Method
Pages
13
PublisherName
American Society for Testing and Materials
Status
Current
Supersedes

ASTM D 1835 : 2018 : REV A Standard Specification for Liquefied Petroleum (LP) Gases
ASTM D 7901 : 2014 : REV B Standard Specification for Dimethyl Ether for Fuel Purposes

ASTM D 2598 : 2021 Standard Practice for Calculation of Certain Physical Properties of Liquefied Petroleum (LP) Gases from Compositional Analysis
ASTM D 6300 : 2020 : REV A Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products, Liquid Fuels, and Lubricants
ASTM D 6300 : 2013 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
ASTM D 6667 : 2021 Standard Test Method for Determination of Total Volatile Sulfur in Gaseous Hydrocarbons and Liquefied Petroleum Gases by Ultraviolet Fluorescence
ASTM D 6299 : 2010 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 6300 : 2014 : REV A : EDT 1 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
ASTM D 2158 : 2005 Standard Test Method for Residues in Liquefied Petroleum (LP) Gases
ASTM D 1265 : 1997 Standard Practice for Sampling Liquefied Petroleum (LP) Gases (Manual Method)
ASTM D 6299 : 2013 : EDT 1 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 2421 : 2002 : R2007 Standard Practice for Interconversion of Analysis of C<i><inf>5</inf></i> and Lighter Hydrocarbons to Gas-Volume, Liquid-Volume, or Mass Basis
ASTM D 2158 : 2016 Standard Test Method for Residues in Liquefied Petroleum (LP) Gases
ASTM D 2421 : 2021 Standard Practice for Interconversion of Analysis of C<emph type="ital"><inf>5</inf ></emph> and Lighter Hydrocarbons to Gas-Volume, Liquid-Volume, or Mass Basis
ASTM D 6667 : 2001 Standard Test Method for Determination of Total Volatile Sulfur in Gaseous Hydrocarbons and Liquefied Petroleum Gases by Ultraviolet Fluorescence
ASTM D 6299 : 2017 : REV A Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 3700 : 2001 Standard Practice for Obtaining LPG Samples Using a Floating Piston Cylinder
ASTM D 6299 : 2017 : REV B Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 6300 : 2017 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
ASTM D 6299 : 2009 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 1835 : 1997 Standard Specification for Liquefied Petroleum (LP) Gases
ASTM D 2421 : 1995 Standard Practice for Interconversion of Analysis of C<sub>5</sub> and Lighter Hydrocarbons to Gas-Volume, Liquid-Volume, or Weight Basis
ASTM D 2163 : 2023 : EDT 1 Standard Test Method for Determination of Hydrocarbons in Liquefied Petroleum (LP) Gases and Propane/Propene Mixtures by Gas Chromatography
ASTM D 2158 : 2004 Standard Test Method for Residues in Liquefied Petroleum (LP) Gases
ASTM D 6300 : 2017 : REV A Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
ASTM D 2163 : 2014 : EDT 1 Standard Test Method for Determination of Hydrocarbons in Liquefied Petroleum (LP) Gases and Propane/Propene Mixtures by Gas Chromatography
ASTM D 2163 : 2007 Standard Test Method for Determination of Hydrocarbons in Liquefied Petroleum (LP) Gases and Propane/Propene Mixtures by Gas Chromatography
ASTM D 6299 : 2013 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 3700 : 2014 Standard Practice for Obtaining LPG Samples Using a Floating Piston Cylinder
ASTM D 6299 : 2021 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 6299 : 2010 : EDT 1 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 6667 : 2004 Standard Test Method for Determination of Total Volatile Sulfur in Gaseous Hydrocarbons and Liquefied Petroleum Gases by Ultraviolet Fluorescence
ASTM D 2158 : 2011 Standard Test Method for Residues in Liquefied Petroleum (LP) Gases
ASTM D 2421 : 2018 Standard Practice for Interconversion of Analysis of C<emph type="ital"><inf>5</inf ></emph> and Lighter Hydrocarbons to Gas-Volume, Liquid-Volume, or Mass Basis
ASTM D 6299 : 2022 : EDT 1 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 1265 : 2023 : REV A Standard Practice for Sampling Liquefied Petroleum (LP) Gases, Manual Method
ASTM D 6300 : 2016 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
ASTM D 2158 : 1989 Standard Test Method for Residues in Liquefied Petroleum (LP) Gases
ASTM D 3700 : 1994 Standard Practice for Obtaining LPG Samples Using a Floating Piston Cylinder
ASTM D 6300 : 2004 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
ASTM D 1835 : 2018 : REV A Standard Specification for Liquefied Petroleum (LP) Gases
ASTM D 1835 : 2012 Standard Specification for Liquefied Petroleum (LP) Gases
ASTM D 6300 : 2019 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
ASTM D 6299 : 2023 : REV A Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 2421 : 2001 Standard Practice for Interconversion of Analysis of C<sub>5</sub> and Lighter Hydrocarbons to Gas-Volume, Liquid-Volume, or Weight Basis
ASTM D 2598 : 2012 Standard Practice for Calculation of Certain Physical Properties of Liquefied Petroleum (LP) Gases from Compositional Analysis
ASTM D 6300 : 2021 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products, Liquid Fuels, and Lubricants
ASTM D 6300 : 2019 : REV A Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
ASTM D 6667 : 2004 : R2010 Standard Test Method for Determination of Total Volatile Sulfur in Gaseous Hydrocarbons and Liquefied Petroleum Gases by Ultraviolet Fluorescence
ASTM D 6300 : 2023 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products, Liquid Fuels, and Lubricants
ASTM D 6300 : 2020 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products, Liquid Fuels, and Lubricants
ASTM D 2421 : 2002 Standard Practice for Interconversion of Analysis of C<sub>5</sub> and Lighter Hydrocarbons to Gas-Volume, Liquid-Volume, or Weight Basis
ASTM D 6299 : 2000 Standard Practice for Applying Statistical Quality Assurance Techniques to Evaluate Analytical Measurement System Performance
ASTM D 3700 : 2021 Standard Practice for Obtaining LPG Samples Using a Floating Piston Cylinder
ASTM D 6299 : 2010 : EDT 2 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 6299 : 2016 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 2598 : 2002 Standard Practice for Calculation of Certain Physical Properties of Liquefied Petroleum (LP) Gases from Compositional Analysis
ASTM D 6300 : 2023 : REV A Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products, Liquid Fuels, and Lubricants
ASTM D 6299 : 2019 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 1835 : 2003 : REV A Standard Specification for Liquefied Petroleum (LP) Gases
ASTM D 6667 : 2010 Standard Test Method for Determination of Total Volatile Sulfur in Gaseous Hydrocarbons and Liquefied Petroleum Gases by Ultraviolet Fluorescence
ASTM D 6300 : 2020 : REV B Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products, Liquid Fuels, and Lubricants
ASTM D 6299 : 2023 : EDT 1 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 6299 : 2000 : REV A Standard Practice for Applying Statistical Quality Assurance Techniques to Evaluate Analytical Measurement System Performance
ASTM D 6300 : 2006 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
ASTM D 6300 : 2014 : REV A Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
ASTM E 355 : 1996 : R2021 : EDT 1 Standard Practice for Gas Chromatography Terms and Relationships
ASTM D 1835 : 2003 Standard Specification for Liquefied Petroleum (LP) Gases
ASTM D 6300 : 2015 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
ASTM D 6667 : 2014 : R2019 Standard Test Method for Determination of Total Volatile Sulfur in Gaseous Hydrocarbons and Liquefied Petroleum Gases by Ultraviolet Fluorescence
ASTM D 6300 : 1999 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
ASTM D 1835 : 2013 Standard Specification for Liquefied Petroleum (LP) Gases
ASTM D 2421 : 2013 Standard Practice for Interconversion of Analysis of C<emph type="ital"><inf>5</inf ></emph> and Lighter Hydrocarbons to Gas-Volume, Liquid-Volume, or Mass Basis
ASTM D 6299 : 2023 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 1835 : 2020 Standard Specification for Liquefied Petroleum (LP) Gases
ASTM D 6299 : 2020 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 6299 : 2008 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 6667 : 2014 : R2019 Standard Test Method for Determination of Total Volatile Sulfur in Gaseous Hydrocarbons and Liquefied Petroleum Gases by Ultraviolet Fluorescence
ASTM D 1835 : 2018 Standard Specification for Liquefied Petroleum (LP) Gases
ASTM D 2158 : 2002 Standard Test Method for Residues in Liquefied Petroleum (LP) Gases
ASTM D 2598 : 1996 : R2001 Standard Practice for Calculation of Certain Physical Properties of Liquefied Petroleum (LP) Gases from Compositional Analysis
ASTM D 2421 : 2021 : EDT 1 Standard Practice for Interconversion of Analysis of C<emph type="ital"><inf>5</inf ></emph> and Lighter Hydrocarbons to Gas-Volume, Liquid-Volume, or Mass Basis
ASTM D 1265 : 2004 Standard Practice for Sampling Liquefied Petroleum (LP) Gases (Manual Method)
ASTM D 6300 : 2013 : REV A Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
ASTM D 3700 : 2012 Standard Practice for Obtaining LPG Samples Using a Floating Piston Cylinder
ASTM D 6299 : 2002 : EDT 1 Standard Practice for Applying Statistical Quality Assurance Techniques to Evaluate Analytical Measurement System Performance
ASTM D 2158 : 2016 : REV A Standard Test Method for Residues in Liquefied Petroleum (LP) Gases
ASTM D 2163 : 1991 : R1996 Standard Test Method for Analysis of Liquefied Petroleum (LP) Gases and Propene Concentrates by Gas Chromatography (Withdrawn 2005)
ASTM D 1835 : 2022 Standard Specification for Liquefied Petroleum (LP) Gases
ASTM D 3700 : 2007 Standard Practice for Obtaining LPG Samples Using a Floating Piston Cylinder
ASTM D 6667 : 2014 Standard Test Method for Determination of Total Volatile Sulfur in Gaseous Hydrocarbons and Liquefied Petroleum Gases by Ultraviolet Fluorescence
ASTM D 1835 : 2016 Standard Specification for Liquefied Petroleum (LP) Gases
ASTM D 6300 : 2008 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
ASTM D 6300 : 2003 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
ASTM D 1265 : 2011 : R2017 : EDT 1 Standard Practice for Sampling Liquefied Petroleum (LP) Gases, Manual Method
ASTM D 6300 : 2007 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
ASTM D 6299 : 2022 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 2158 : 1997 : EDT 1 Standard Test Method for Residues in Liquefied Petroleum (LP) Gases
ASTM D 1835 : 2011 Standard Specification for Liquefied Petroleum (LP) Gases
ASTM D 2598 : 2016 Standard Practice for Calculation of Certain Physical Properties of Liquefied Petroleum (LP) Gases from Compositional Analysis
ASTM D 1265 : 2005 Standard Practice for Sampling Liquefied Petroleum (LP) Gases (Manual Method)
ASTM D 6300 : 2002 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
ASTM D 2598 : 2002 : R2007 Standard Practice for Calculation of Certain Physical Properties of Liquefied Petroleum (LP) Gases from Compositional Analysis
ASTM D 1265 : 2004 : REV A Standard Practice for Sampling Liquefied Petroleum (LP) Gases (Manual Method)
ASTM D 1265 : 2011 Standard Practice for Sampling Liquefied Petroleum (LP) Gases, Manual Method
ASTM D 2158 : 2016 : REV A : EDT 1 Standard Test Method for Residues in Liquefied Petroleum (LP) Gases
ASTM D 6300 : 2016 : REV A Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
ASTM D 2163 : 2014 Standard Test Method for Determination of Hydrocarbons in Liquefied Petroleum (LP) Gases and Propane/Propene Mixtures by Gas Chromatography
ASTM D 2163 : 2014 : R2019 Standard Test Method for Determination of Hydrocarbons in Liquefied Petroleum (LP) Gases and Propane/Propene Mixtures by Gas Chromatography
ASTM D 3700 : 2016 Standard Practice for Obtaining LPG Samples Using a Floating Piston Cylinder
ASTM E 355 : 1996 : R2014 Standard Practice for Gas Chromatography Terms and Relationships
ASTM D 6299 : 2007 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 1265 : 2023 Standard Practice for Sampling Liquefied Petroleum (LP) Gases, Manual Method
ASTM D 6299 : 2007 : EDT 1 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 6299 : 2020 : REV A Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 2163 : 2023 Standard Test Method for Determination of Hydrocarbons in Liquefied Petroleum (LP) Gases and Propane/Propene Mixtures by Gas Chromatography
ASTM D 1265 : 2022 Standard Practice for Sampling Liquefied Petroleum (LP) Gases, Manual Method
ASTM D 6299 : 2017 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 6300 : 2014 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
ASTM D 1835 : 2005 Standard Specification for Liquefied Petroleum (LP) Gases
ASTM D 2158 : 2021 Standard Test Method for Residues in Liquefied Petroleum (LP) Gases
ASTM D 2421 : 2019 Standard Practice for Interconversion of Analysis of C<emph type="ital"><inf>5</inf ></emph> and Lighter Hydrocarbons to Gas-Volume, Liquid-Volume, or Mass Basis
ASTM D 6299 : 2002 Standard Practice for Applying Statistical Quality Assurance Techniques to Evaluate Analytical Measurement System Performance
ASTM D 6300 : 2024 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products, Liquid Fuels, and Lubricants

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