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  • ASTM D 7756 : 2019

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    Standard Test Method for Residues in Liquefied Petroleum (LP) Gases by Gas Chromatography with Liquid, On-Column Injection

    Available format(s):  Hardcopy, PDF

    Language(s):  English

    Published date:  18-06-2019

    Publisher:  American Society for Testing and Materials

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    Abstract - (Show below) - (Hide below)

    This test method covers the determination, by gas chromatography, of soluble hydrocarbon materials, sometimes called “oily residue,” which can be present in liquefied petroleum (LP) gases and which are substantially less volatile than the LPG product.

    Scope - (Show below) - (Hide below)

    1.1This test method covers the determination, by gas chromatography, of soluble hydrocarbon materials, sometimes called “oily residue,” which can be present in liquefied petroleum (LP) gases and which are substantially less volatile than the LPG product.

    1.2This test method quantifies, in the range of 10 mg/kg to 600 mg/kg (ppm mass), the residue with a boiling point between 174 °C and 522 °C (C10 to C40) in LPG. Higher boiling materials, or materials that adhere permanently to the chromatographic column, will not be detected.

    1.3Appendix X3, Appendix X4, and Appendix X6 describe additional applications which could be performed based on the hardware and procedures described in this test method. Appendix X3 describes a test procedure for expanding the analysis range to benzene, Appendix X4 describes a test procedure for the analysis of diisopropanolamine, and Appendix X6 describes a test procedure for the analysis of heavy residues or contaminants from C40 to about C60 in LPG.

    1.4The values stated in SI units are to be regarded as standard. The values given in parentheses after SI units are provided for information only and are not considered standard.

    1.5This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.

    1.6This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

    General Product Information - (Show below) - (Hide below)

    Committee D 02
    Document Type Test Method
    Publisher American Society for Testing and Materials
    Status Current
    Supersedes

    Standards Referenced By This Book - (Show below) - (Hide below)

    ASTM D 7901 : 2014 : REV B Standard Specification for Dimethyl Ether for Fuel Purposes
    ASTM D 1835 : 2018 : REV A Standard Specification for Liquefied Petroleum (LP) Gases

    Standards Referencing This Book - (Show below) - (Hide below)

    ASTM D 2598 : 2021 Standard Practice for Calculation of Certain Physical Properties of Liquefied Petroleum (LP) Gases from Compositional Analysis
    ASTM D 6300 : 2020 : REV A Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products, Liquid Fuels, and Lubricants
    ASTM D 6300 : 2013 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
    ASTM D 6667 : 2021 Standard Test Method for Determination of Total Volatile Sulfur in Gaseous Hydrocarbons and Liquefied Petroleum Gases by Ultraviolet Fluorescence
    ASTM D 6299 : 2010 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 6300 : 2014 : REV A : EDT 1 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
    ASTM D 2158 : 2005 Standard Test Method for Residues in Liquefied Petroleum (LP) Gases
    ASTM D 1265 : 1997 Standard Practice for Sampling Liquefied Petroleum (LP) Gases (Manual Method)
    ASTM D 6299 : 2013 : EDT 1 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 2421 : 2002 : R2007 Standard Practice for Interconversion of Analysis of C5 and Lighter Hydrocarbons to Gas-Volume, Liquid-Volume, or Mass Basis
    ASTM D 2158 : 2016 Standard Test Method for Residues in Liquefied Petroleum (LP) Gases
    ASTM D 2421 : 2021 Standard Practice for Interconversion of Analysis of C5 and Lighter Hydrocarbons to Gas-Volume, Liquid-Volume, or Mass Basis
    ASTM D 6667 : 2001 Standard Test Method for Determination of Total Volatile Sulfur in Gaseous Hydrocarbons and Liquefied Petroleum Gases by Ultraviolet Fluorescence
    ASTM D 6299 : 2017 : REV A Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 3700 : 2001 Standard Practice for Obtaining LPG Samples Using a Floating Piston Cylinder
    ASTM D 6299 : 2017 : REV B Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 6300 : 2017 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
    ASTM D 6299 : 2009 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 1835 : 1997 Standard Specification for Liquefied Petroleum (LP) Gases
    ASTM D 2421 : 1995 Standard Practice for Interconversion of Analysis of C5 and Lighter Hydrocarbons to Gas-Volume, Liquid-Volume, or Weight Basis
    ASTM D 2158 : 2004 Standard Test Method for Residues in Liquefied Petroleum (LP) Gases
    ASTM D 6300 : 2017 : REV A Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
    ASTM D 2163 : 2014 : EDT 1 Standard Test Method for Determination of Hydrocarbons in Liquefied Petroleum (LP) Gases and Propane/Propene Mixtures by Gas Chromatography
    ASTM D 2163 : 2007 Standard Test Method for Determination of Hydrocarbons in Liquefied Petroleum (LP) Gases and Propane/Propene Mixtures by Gas Chromatography
    ASTM D 6299 : 2013 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 3700 : 2014 Standard Practice for Obtaining LPG Samples Using a Floating Piston Cylinder
    ASTM D 6299 : 2021 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 6299 : 2010 : EDT 1 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 6667 : 2004 Standard Test Method for Determination of Total Volatile Sulfur in Gaseous Hydrocarbons and Liquefied Petroleum Gases by Ultraviolet Fluorescence
    ASTM D 2158 : 2011 Standard Test Method for Residues in Liquefied Petroleum (LP) Gases
    ASTM D 2421 : 2018 Standard Practice for Interconversion of Analysis of C5 and Lighter Hydrocarbons to Gas-Volume, Liquid-Volume, or Mass Basis
    ASTM D 6300 : 2016 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
    ASTM D 2158 : 1989 Standard Test Method for Residues in Liquefied Petroleum (LP) Gases
    ASTM D 3700 : 1994 Standard Practice for Obtaining LPG Samples Using a Floating Piston Cylinder
    ASTM D 6300 : 2004 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
    ASTM D 1835 : 2018 : REV A Standard Specification for Liquefied Petroleum (LP) Gases
    ASTM D 1835 : 2012 Standard Specification for Liquefied Petroleum (LP) Gases
    ASTM D 6300 : 2019 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
    ASTM D 2421 : 2001 Standard Practice for Interconversion of Analysis of C5 and Lighter Hydrocarbons to Gas-Volume, Liquid-Volume, or Weight Basis
    ASTM D 2598 : 2012 Standard Practice for Calculation of Certain Physical Properties of Liquefied Petroleum (LP) Gases from Compositional Analysis
    ASTM D 6300 : 2021 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products, Liquid Fuels, and Lubricants
    ASTM D 6300 : 2019 : REV A Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
    ASTM D 6667 : 2004 : R2010 Standard Test Method for Determination of Total Volatile Sulfur in Gaseous Hydrocarbons and Liquefied Petroleum Gases by Ultraviolet Fluorescence
    ASTM D 6300 : 2020 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products, Liquid Fuels, and Lubricants
    ASTM D 2421 : 2002 Standard Practice for Interconversion of Analysis of C5 and Lighter Hydrocarbons to Gas-Volume, Liquid-Volume, or Weight Basis
    ASTM D 6299 : 2000 Standard Practice for Applying Statistical Quality Assurance Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 3700 : 2021 Standard Practice for Obtaining LPG Samples Using a Floating Piston Cylinder
    ASTM D 6299 : 2010 : EDT 2 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 6299 : 2016 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 2598 : 2002 Standard Practice for Calculation of Certain Physical Properties of Liquefied Petroleum (LP) Gases from Compositional Analysis
    ASTM D 6299 : 2019 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 1835 : 2003 : REV A Standard Specification for Liquefied Petroleum (LP) Gases
    ASTM D 6667 : 2010 Standard Test Method for Determination of Total Volatile Sulfur in Gaseous Hydrocarbons and Liquefied Petroleum Gases by Ultraviolet Fluorescence
    ASTM D 6300 : 2020 : REV B Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products, Liquid Fuels, and Lubricants
    ASTM D 6299 : 2000 : REV A Standard Practice for Applying Statistical Quality Assurance Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 6300 : 2006 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
    ASTM D 6300 : 2014 : REV A Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
    ASTM E 355 : 1996 : R2021 : EDT 1 Standard Practice for Gas Chromatography Terms and Relationships
    ASTM D 1835 : 2003 Standard Specification for Liquefied Petroleum (LP) Gases
    ASTM D 6300 : 2015 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
    ASTM D 6667 : 2014 : R2019 Standard Test Method for Determination of Total Volatile Sulfur in Gaseous Hydrocarbons and Liquefied Petroleum Gases by Ultraviolet Fluorescence
    ASTM D 6300 : 1999 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
    ASTM D 1835 : 2013 Standard Specification for Liquefied Petroleum (LP) Gases
    ASTM D 2421 : 2013 Standard Practice for Interconversion of Analysis of C5 and Lighter Hydrocarbons to Gas-Volume, Liquid-Volume, or Mass Basis
    ASTM D 1835 : 2020 Standard Specification for Liquefied Petroleum (LP) Gases
    ASTM D 6299 : 2020 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 6299 : 2008 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 6667 : 2014 : R2019 Standard Test Method for Determination of Total Volatile Sulfur in Gaseous Hydrocarbons and Liquefied Petroleum Gases by Ultraviolet Fluorescence
    ASTM D 1835 : 2018 Standard Specification for Liquefied Petroleum (LP) Gases
    ASTM D 2158 : 2002 Standard Test Method for Residues in Liquefied Petroleum (LP) Gases
    ASTM D 2598 : 1996 : R2001 Standard Practice for Calculation of Certain Physical Properties of Liquefied Petroleum (LP) Gases from Compositional Analysis
    ASTM D 2421 : 2021 : EDT 1 Standard Practice for Interconversion of Analysis of C5 and Lighter Hydrocarbons to Gas-Volume, Liquid-Volume, or Mass Basis
    ASTM D 1265 : 2004 Standard Practice for Sampling Liquefied Petroleum (LP) Gases (Manual Method)
    ASTM D 6300 : 2013 : REV A Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
    ASTM D 3700 : 2012 Standard Practice for Obtaining LPG Samples Using a Floating Piston Cylinder
    ASTM D 6299 : 2002 : EDT 1 Standard Practice for Applying Statistical Quality Assurance Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 2158 : 2016 : REV A Standard Test Method for Residues in Liquefied Petroleum (LP) Gases
    ASTM D 2163 : 1991 : R1996 Standard Test Method for Analysis of Liquefied Petroleum (LP) Gases and Propene Concentrates by Gas Chromatography (Withdrawn 2005)
    ASTM D 3700 : 2007 Standard Practice for Obtaining LPG Samples Using a Floating Piston Cylinder
    ASTM D 6667 : 2014 Standard Test Method for Determination of Total Volatile Sulfur in Gaseous Hydrocarbons and Liquefied Petroleum Gases by Ultraviolet Fluorescence
    ASTM D 1835 : 2016 Standard Specification for Liquefied Petroleum (LP) Gases
    ASTM D 6300 : 2008 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
    ASTM D 6300 : 2003 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
    ASTM D 1265 : 2011 : R2017 : EDT 1 Standard Practice for Sampling Liquefied Petroleum (LP) Gases, Manual Method
    ASTM D 6300 : 2007 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
    ASTM D 2158 : 1997 : EDT 1 Standard Test Method for Residues in Liquefied Petroleum (LP) Gases
    ASTM D 1835 : 2011 Standard Specification for Liquefied Petroleum (LP) Gases
    ASTM D 2598 : 2016 Standard Practice for Calculation of Certain Physical Properties of Liquefied Petroleum (LP) Gases from Compositional Analysis
    ASTM D 1265 : 2005 Standard Practice for Sampling Liquefied Petroleum (LP) Gases (Manual Method)
    ASTM D 6300 : 2002 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
    ASTM D 2598 : 2002 : R2007 Standard Practice for Calculation of Certain Physical Properties of Liquefied Petroleum (LP) Gases from Compositional Analysis
    ASTM D 1265 : 2004 : REV A Standard Practice for Sampling Liquefied Petroleum (LP) Gases (Manual Method)
    ASTM D 1265 : 2011 Standard Practice for Sampling Liquefied Petroleum (LP) Gases, Manual Method
    ASTM D 2158 : 2016 : REV A : EDT 1 Standard Test Method for Residues in Liquefied Petroleum (LP) Gases
    ASTM D 6300 : 2016 : REV A Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
    ASTM D 2163 : 2014 Standard Test Method for Determination of Hydrocarbons in Liquefied Petroleum (LP) Gases and Propane/Propene Mixtures by Gas Chromatography
    ASTM D 2163 : 2014 : R2019 Standard Test Method for Determination of Hydrocarbons in Liquefied Petroleum (LP) Gases and Propane/Propene Mixtures by Gas Chromatography
    ASTM D 3700 : 2016 Standard Practice for Obtaining LPG Samples Using a Floating Piston Cylinder
    ASTM E 355 : 1996 : R2014 Standard Practice for Gas Chromatography Terms and Relationships
    ASTM D 6299 : 2007 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 6299 : 2007 : EDT 1 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 6299 : 2020 : REV A Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 6299 : 2017 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 6300 : 2014 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
    ASTM D 1835 : 2005 Standard Specification for Liquefied Petroleum (LP) Gases
    ASTM D 2158 : 2021 Standard Test Method for Residues in Liquefied Petroleum (LP) Gases
    ASTM D 2421 : 2019 Standard Practice for Interconversion of Analysis of C5 and Lighter Hydrocarbons to Gas-Volume, Liquid-Volume, or Mass Basis
    ASTM D 6299 : 2002 Standard Practice for Applying Statistical Quality Assurance Techniques to Evaluate Analytical Measurement System Performance
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