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ASTM D 7778 : 2015 : R2022 : EDT 1

Current
Current

The latest, up-to-date edition.

Standard Guide for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
Available format(s)

Hardcopy , PDF

Language(s)

English

Published date

03-06-2022

1.1This guide describes the procedures for planning and conducting an interlaboratory study (ILS) of a test method used in Petroleum Products and Lubricants Committee D02 of ASTM for the purpose of estimating repeatability and reproducibility of the test method in accordance with ASTM Form and Style requirements.

1.2This guide is concerned with the management of the ILS and intended to provide guidance for the planning stage and ensure the process, logistics, and tools are identified and agreed upon in advance.

1.2.1Selection of the samples and the impact of sample selection on the final scope of the test method—both the range of materials covered in the scope and precision sections and the measurement range covered in the precision section—are important, and careful consideration needs to be given to these aspects before an ILS is launched.

1.3This guide does not concern itself with the development of test methods but rather with gathering the information needed for a test method precision statement.

1.4This guide is concerned with test methods which yield a single numerical figure as the test result, although the single figure may be the result of a calculation from a set of measurements.

1.5This guide is designed for tests of properties that are stable, such that bulk samples can be homogenized and sub-samples can be prepared that will be identical and stable for the duration of the ILS testing period. This guide is not designed for unstable properties or for properties that make it difficult to obtain stable, representative samples for an ILS conducted at multiple laboratory sites.

1.6This guide represents the suggested practices for a typical precision study. Individual subcommittees may modify this approach as their expertise directs.

1.7This guide is voluntary, and thus, is not required for an approved precision study.

1.8This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

Committee
D 02
DocumentType
Guide
Pages
10
ProductNote
ε1NOTE—Editorially corrected6.2.2in May 2022.
PublisherName
American Society for Testing and Materials
Status
Current
Supersedes

ASTM D 8110 : 2017 Standard Test Method for Elemental Analysis of Distillate Products by Inductively Coupled Plasma Mass Spectrometry (ICP-MS)
ASTM F 3375 : 2019 Standard Test Method for Assessing Non-Metered Restricted Delivery Systems for Liquid Consumer Products
ASTM C 1926 : 2023 Standard Test Method for Measurement of Glass Dissolution Rate Using Stirred Dilute Reactor Conditions on Monolithic Samples

ASTM E 456 : 2013 : REV A : R2022 Standard Terminology Relating to Quality and Statistics
ASTM E 456 : 2013 : REV A : R2022 : EDT 1 Standard Terminology Relating to Quality and Statistics
ASTM D 5854 : 2019 Standard Practice for Mixing and Handling of Liquid Samples of Petroleum and Petroleum Products
ASTM D 6792 : 2023 : REV C Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories
ASTM D 6708 : 2024 Standard Practice for Statistical Assessment and Improvement of Expected Agreement Between Two Test Methods that Purport to Measure the Same Property of a Material
ASTM D 6300 : 2021 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products, Liquid Fuels, and Lubricants
ASTM D 6300 : 2023 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products, Liquid Fuels, and Lubricants
ASTM D 6792 : 2023 : REV B Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories
ASTM E 691 : 2023 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
ASTM D 6300 : 2023 : REV A Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products, Liquid Fuels, and Lubricants
ASTM E 691 : 2022 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
ASTM D 6708 : 2021 Standard Practice for Statistical Assessment and Improvement of Expected Agreement Between Two Test Methods that Purport to Measure the Same Property of a Material
ASTM D 6792 : 2021 : REV C Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories
ASTM D 6792 : 2023 : REV A Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories
ASTM E 691 : 2021 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
ASTM D 130 : 2018 Standard Test Method for Corrosiveness to Copper from Petroleum Products by Copper Strip Test
ASTM D 6792 : 2022 Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories
ASTM D 4306 : 2020 Standard Practice for Aviation Fuel Sample Containers for Tests Affected by Trace Contamination
ASTM D 6792 : 2023 Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories
ASTM D 6792 : 2022 : REV A Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories
ASTM D 130 : 2012 Standard Test Method for Corrosiveness to Copper from Petroleum Products by Copper Strip Test
ASTM D 6300 : 2024 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products, Liquid Fuels, and Lubricants

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