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  • ASTM D 7861 : 2014 : R2019

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    Standard Test Method for Determination of Fatty Acid Methyl Esters (FAME) in Diesel Fuel by Linear Variable Filter (LVF) Array Based Mid-Infrared Spectroscopy

    Available format(s):  Hardcopy, PDF

    Language(s):  English

    Published date:  01-05-2019

    Publisher:  American Society for Testing and Materials

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    Abstract - (Show below) - (Hide below)

    This test method determines fatty acid methyl esters (FAME or biodiesel) in diesel fuel oils. FAME can be quantitatively determined from 1.0 % to 30.0 % by volume.

    Scope - (Show below) - (Hide below)

    1.1This test method determines fatty acid methyl esters (FAME or biodiesel) in diesel fuel oils. FAME can be quantitatively determined from 1.0 % to 30.0 % by volume. This test method uses linear variable filter (LVF) array based mid-infrared spectroscopy for monitoring FAME concentration.

    Note 1:See Section 6 for a list of interferences that could affect the results produced from this method.

    1.2This test method uses a horizontal attenuated total reflectance (HATR) crystal and a univariate calibration.

    1.3The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

    1.4This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.

    1.5This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

    General Product Information - (Show below) - (Hide below)

    Committee D 02
    Document Type Test Method
    Publisher American Society for Testing and Materials
    Status Current
    Supersedes

    Standards Referenced By This Book - (Show below) - (Hide below)

    ASTM D 396 : 2019 Standard Specification for Fuel Oils
    ASTM D 7467 : 2019 Standard Specification for Diesel Fuel Oil, Biodiesel Blend (B6 to B20)

    Standards Referencing This Book - (Show below) - (Hide below)

    ASTM D 4057 : 2019 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
    ASTM D 6300 : 2020 : REV A Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products, Liquid Fuels, and Lubricants
    ASTM D 6300 : 2013 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
    ASTM D 4057 : 1995 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
    ASTM D 6299 : 2010 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 6300 : 2014 : REV A : EDT 1 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
    ASTM D 7467 : 2018 : REV A Standard Specification for Diesel Fuel Oil, Biodiesel Blend (B6 to B20)
    ASTM D 1298 : 2012 : REV A Standard Test Method for Density, Relative Density (Specific Gravity), or API Gravity of Crude Petroleum and Liquid Petroleum Products by Hydrometer Method
    ASTM D 6299 : 2013 : EDT 1 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 4177 : 2016 : EDT 1 Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
    ASTM D 6299 : 2017 : REV A Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 6299 : 2017 : REV B Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 4052 : 1996 : R2002 : EDT 1 Standard Test Method for Density and Relative Density of Liquids by Digital Density Meter
    ASTM D 7467 : 2009 Standard Specification for Diesel Fuel Oil, Biodiesel Blend (B6 to B20)
    ASTM D 6300 : 2017 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
    ASTM D 6299 : 2009 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 7371 : 2014 Standard Test Method for Determination of Biodiesel (Fatty Acid Methyl Esters) Content in Diesel Fuel Oil Using Mid Infrared Spectroscopy (FTIR-ATR-PLS Method)
    ASTM D 1298 : 2012 : REV B Standard Test Method for Density, Relative Density, or API Gravity of Crude Petroleum and Liquid Petroleum Products by Hydrometer Method
    ASTM D 7371 : 2014 : R2022 Standard Test Method for Determination of Biodiesel (Fatty Acid Methyl Esters) Content in Diesel Fuel Oil Using Mid Infrared Spectroscopy (FTIR-ATR-PLS Method)
    ASTM D 975 : 2022 Standard Specification for Diesel Fuel
    ASTM D 4177 : 1995 Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
    ASTM D 6751 : 2006 : REV A Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels
    ASTM D 6300 : 2017 : REV A Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
    ASTM D 4057 : 2012 : R2018 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
    ASTM D 4052 : 2018 : REV A Standard Test Method for Density, Relative Density, and API Gravity of Liquids by Digital Density Meter
    ASTM D 6751 : 2007 : REV B Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels
    ASTM E 168 : 2016 : R2023 Standard Practices for General Techniques of Infrared Quantitative Analysis
    ASTM D 6751 : 2006 : EDT 1 Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels
    ASTM D 6299 : 2013 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 6299 : 2021 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 6751 : 2018 Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels
    ASTM D 6751 : 2009 : REV A Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels
    ASTM D 6751 : 2007 : REV B : EDT 1 Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels
    ASTM D 975 : 2019 : REV B Standard Specification for Diesel Fuel
    ASTM D 5854 : 1996 : R2010 Standard Practice for Mixing and Handling of Liquid Samples of Petroleum and Petroleum Products
    ASTM D 6299 : 2010 : EDT 1 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 6299 : 2022 : EDT 1 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 7467 : 2010 Standard Specification for Diesel Fuel Oil, Biodiesel Blend (B6 to B20)
    ASTM D 6300 : 2016 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
    ASTM D 7467 : 2008 Standard Specification for Diesel Fuel Oil, Biodiesel Blend (B6 to B20)
    ASTM D 6751 : 2007 Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels
    ASTM D 1298 : 1999 : R2005 Standard Test Method for Density, Relative Density (Specific Gravity), or API Gravity of Crude Petroleum and Liquid Petroleum Products by Hydrometer Method
    ASTM D 4052 : 2009 Standard Test Method for Density, Relative Density, and API Gravity of Liquids by Digital Density Meter
    ASTM D 4057 : 1981 : EDT 2 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
    ASTM D 6300 : 2004 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
    ASTM D 1298 : 2012 : REV B : R2017 Standard Test Method for Density, Relative Density, or API Gravity of Crude Petroleum and Liquid Petroleum Products by Hydrometer Method
    ASTM D 7467 : 2017 Standard Specification for Diesel Fuel Oil, Biodiesel Blend (B6 to B20)
    ASTM D 1298 : 2012 Standard Test Method for Density, Relative Density (Specific Gravity), or API Gravity of Crude Petroleum and Liquid Petroleum Products by Hydrometer Method
    ASTM D 5854 : 2019 Standard Practice for Mixing and Handling of Liquid Samples of Petroleum and Petroleum Products
    ASTM D 6751 : 2012 Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels
    ASTM E 1655 : 2004 Standard Practices for Infrared Multivariate Quantitative Analysis
    ASTM D 975 : 2021 Standard Specification for Diesel Fuel
    ASTM D 7467 : 2015 Standard Specification for Diesel Fuel Oil, Biodiesel Blend (B6 to B20)
    ASTM D 1298 : 1999 : EDT 2 Standard Test Method for Density, Relative Density (Specific Gravity), or API Gravity of Crude Petroleum and Liquid Petroleum Products by Hydrometer Method
    ASTM D 6300 : 2019 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
    ASTM D 6751 : 2014 Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels
    ASTM D 5854 : 1996 : R2005 Standard Practice for Mixing and Handling of Liquid Samples of Petroleum and Petroleum Products
    ASTM D 7467 : 2015 : REV A Standard Specification for Diesel Fuel Oil, Biodiesel Blend (B6 to B20)
    ASTM D 4307 : 1999 : R2004 Standard Practice for Preparation of Liquid Blends for Use as Analytical Standards
    ASTM D 6300 : 2021 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products, Liquid Fuels, and Lubricants
    ASTM D 6300 : 2019 : REV A Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
    ASTM D 6300 : 2020 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products, Liquid Fuels, and Lubricants
    ASTM D 6299 : 2000 Standard Practice for Applying Statistical Quality Assurance Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 6299 : 2010 : EDT 2 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 1298 : 1999 Standard Test Method for Density, Relative Density (Specific Gravity), or API Gravity of Crude Petroleum and Liquid Petroleum Products by Hydrometer Method
    ASTM D 6751 : 2011 : REV B Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels
    ASTM D 975 : 2020 : REV C Standard Specification for Diesel Fuel
    ASTM D 6299 : 2016 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 6751 : 2015 : REV B Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels
    ASTM D 4057 : 2006 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
    ASTM D 7467 : 2015 : EDT 1 Standard Specification for Diesel Fuel Oil, Biodiesel Blend (B6 to B20)
    ASTM D 4177 : 2015 Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
    ASTM D 7467 : 2015 : REV C Standard Specification for Diesel Fuel Oil, Biodiesel Blend (B6 to B20)
    ASTM D 6751 : 2015 : REV C Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels
    ASTM D 4052 : 2011 Standard Test Method for Density, Relative Density, and API Gravity of Liquids by Digital Density Meter
    ASTM D 6299 : 2019 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 4052 : 2016 Standard Test Method for Density, Relative Density, and API Gravity of Liquids by Digital Density Meter
    ASTM D 6300 : 2020 : REV B Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products, Liquid Fuels, and Lubricants
    ASTM D 6751 : 2015 : REV A Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels
    ASTM D 4057 : 2012 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
    ASTM D 6299 : 2000 : REV A Standard Practice for Applying Statistical Quality Assurance Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 6300 : 2006 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
    ASTM D 4307 : 1999 Standard Practice for Preparation of Liquid Blends for Use as Analytical Standards
    ASTM D 7467 : 2014 Standard Specification for Diesel Fuel Oil, Biodiesel Blend (B6 to B20)
    ASTM D 6300 : 2014 : REV A Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
    ASTM D 6751 : 2002 Standard Specification for Biodiesel Fuel (B100) Blend Stock for Distillate Fuels
    ASTM D 6751 : 2003 : REV A Standard Specification for Biodiesel Fuel (B100) Blend Stock for Distillate Fuels
    ASTM D 6300 : 2015 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
    ASTM D 1298 : 1999 : EDT 1 Standard Test Method for Density, Relative Density (Specific Gravity), or API Gravity of Crude Petroleum and Liquid Petroleum Products by Hydrometer Method
    ASTM D 6300 : 1999 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
    ASTM D 4177 : 2022 Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
    ASTM D 6751 : 2020 Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels
    ASTM D 6299 : 2020 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 4177 : 1995 : R2010 Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
    ASTM D 4307 : 2017 Standard Practice for Preparation of Liquid Blends for Use as Analytical Standards
    ASTM D 6299 : 2008 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 6751 : 2003 Standard Specification for Biodiesel Fuel (B100) Blend Stock for Distillate Fuels
    ASTM E 1655 : 2017 Standard Practices for Infrared Multivariate Quantitative Analysis
    ASTM D 6751 : 2008 Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels
    ASTM D 6751 : 2019 Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels
    ASTM D 4177 : 1995 : R2000 Standard Practice for Automatic Sampling of Peroleum and Petroleum Products
    ASTM D 5854 : 1996 : R2000 Standard Practice for Mixing and Handling of Liquid Samples of Petroleum and Petroleum Products
    ASTM D 6300 : 2013 : REV A Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
    ASTM D 7467 : 2020 Standard Specification for Diesel Fuel Oil, Biodiesel Blend (B6 to B20)
    ASTM D 6299 : 2002 : EDT 1 Standard Practice for Applying Statistical Quality Assurance Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 4052 : 1996 Standard Test Method for Density and Relative Density of Liquids by Digital Density Meter
    ASTM D 7467 : 2018 : REV B Standard Specification for Diesel Fuel Oil, Biodiesel Blend (B6 to B20)
    ASTM D 4307 : 2017 : R2021 Standard Practice for Preparation of Liquid Blends for Use as Analytical Standards
    ASTM E 1655 : 2000 Standard Practices for Infrared Multivariate Quantitative Analysis
    ASTM D 6751 : 2015 : REV C : EDT 1 Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels
    ASTM D 975 : 2022 : REV A Standard Specification for Diesel Fuel
    ASTM D 7467 : 2009 : REV A Standard Specification for Diesel Fuel Oil, Biodiesel Blend (B6 to B20)
    ASTM D 6300 : 2008 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
    ASTM D 4307 : 1999 : R2010 Standard Practice for Preparation of Liquid Blends for Use as Analytical Standards
    ASTM D 6300 : 2003 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
    ASTM D 7371 : 2007 Standard Test Method for Determination of Biodiesel (Fatty Acid Methyl Esters) Content in Diesel Fuel Oil Using Mid Infrared Spectroscopy (FTIR-ATR-PLS Method)
    ASTM D 6300 : 2007 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
    ASTM D 6299 : 2022 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 6751 : 2007 : REV A Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels
    ASTM E 1655 : 2005 Standard Practices for Infrared Multivariate Quantitative Analysis
    ASTM D 7467 : 2015 : REV C : EDT 1 Standard Specification for Diesel Fuel Oil, Biodiesel Blend (B6 to B20)
    ASTM D 6300 : 2002 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
    ASTM D 4057 : 2022 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
    ASTM D 7467 : 2019 Standard Specification for Diesel Fuel Oil, Biodiesel Blend (B6 to B20)
    ASTM D 6751 : 2011 Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels
    ASTM D 4177 : 2016 Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
    ASTM D 7467 : 2015 : REV B Standard Specification for Diesel Fuel Oil, Biodiesel Blend (B6 to B20)
    ASTM D 4052 : 2022 Standard Test Method for Density, Relative Density, and API Gravity of Liquids by Digital Density Meter
    ASTM D 4177 : 2020 Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
    ASTM D 4177 : 1995 : R2005 Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
    ASTM D 1298 : 1985 : R1990 : EDT 1 Standard Practice for Density, Relative Density (Specific Gravity), or API Gravity of Crude Petroleum and Liquid Petroleum Products by Hydrometer Method
    ASTM D 6751 : 2011 : REV A Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels
    ASTM D 6300 : 2016 : REV A Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
    ASTM D 6751 : 2015 Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels
    ASTM D 7371 : 2012 Standard Test Method for Determination of Biodiesel (Fatty Acid Methyl Esters) Content in Diesel Fuel Oil Using Mid Infrared Spectroscopy (FTIR-ATR-PLS Method)
    ASTM D 5854 : 2019 : REV A Standard Practice for Mixing and Handling of Liquid Samples of Petroleum and Petroleum Products
    ASTM D 6299 : 2007 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 7467 : 2013 Standard Specification for Diesel Fuel Oil, Biodiesel Blend (B6 to B20)
    ASTM D 4052 : 2015 Standard Test Method for Density, Relative Density, and API Gravity of Liquids by Digital Density Meter
    ASTM D 6299 : 2007 : EDT 1 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 4057 : 1995 : R2000 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
    ASTM D 6299 : 2020 : REV A Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM E 1655 : 2005 : R2012 Standard Practices for Infrared Multivariate Quantitative Analysis
    ASTM D 7467 : 2018 Standard Specification for Diesel Fuel Oil, Biodiesel Blend (B6 to B20)
    ASTM D 6299 : 2017 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 6751 : 2009 Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels
    ASTM D 4177 : 2015 : REV A Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
    ASTM D 4307 : 1999 : R2015 Standard Practice for Preparation of Liquid Blends for Use as Analytical Standards
    ASTM D 6300 : 2014 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
    ASTM D 4057 : 2006 : R2011 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
    ASTM D 6751 : 2010 Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels
    ASTM D 5854 : 1996 : R2015 Standard Practice for Mixing and Handling of Liquid Samples of Petroleum and Petroleum Products
    ASTM D 4052 : 2018 Standard Test Method for Density, Relative Density, and API Gravity of Liquids by Digital Density Meter
    ASTM D 6751 : 2002 : REV A Standard Specification for Biodiesel Fuel (B100) Blend Stock for Distillate Fuels
    ASTM D 6299 : 2002 Standard Practice for Applying Statistical Quality Assurance Techniques to Evaluate Analytical Measurement System Performance
    ASTM E 168 : 2016 Standard Practices for General Techniques of Infrared Quantitative Analysis
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