Standard Practice for Optimization, Calibration, and Validation of Ion Chromatographic Determination of Heteroatoms and Anions in Petroleum Products and Lubricants

Available format(s)

Hardcopy , PDF

Language(s)

English

Published date

01-07-2020

Publisher

American Society for Testing and Materials

1.1This practice covers the information on calibration, quality control, and operational guidance for anionic measurements using ion chromatography (IC).

1.2IC Related Standards—Chemically or electrolytically regenerated suppressed ion chromatography standards for aqueous matrices include Test Methods D2988, D4327, D5085, D5542, D5827, D5987, D5996, D6581, D7319, D7328, D7359, D7773, D7994, and D8150; IC instrumentation requirements are described in Practices E1151, and E1511.

1.3The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.4This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.

1.5This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

Committee	D 02
DocumentType	Standard Practice
Pages	11
PublisherName	American Society for Testing and Materials
Status	Current
Supersedes	ASTM D 8149 : 2017

ASTM D 4057 : 2019	Standard Practice for Manual Sampling of Petroleum and Petroleum Products
ASTM D 6792 : 2021 : REV A	Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories
ASTM D 7328 : 2022	Standard Test Method for Determination of Existent and Potential Inorganic Sulfate and Total Inorganic Chloride in Fuel Ethanol by Ion Chromatography Using Aqueous Sample Injection
ASTM D 2988 : 1996	Standard Test Methods for Water-Soluble Halide Ion In Halogenated Organic Solvents and Their Admixtures
ASTM D 86 : 2023	Standard Test Method for Distillation of Petroleum Products and Liquid Fuels at Atmospheric Pressure
ASTM E 1151 : 1993	Standard Practice for Ion Chromatography Terms and Relationships
ASTM D 975 : 2022	Standard Specification for Diesel Fuel
ASTM D 86 : 2023 : REV A : EDT 1	Standard Test Method for Distillation of Petroleum Products and Liquid Fuels at Atmospheric Pressure
ASTM D 86 : 2020 : REV A	Standard Test Method for Distillation of Petroleum Products and Liquid Fuels at Atmospheric Pressure
ASTM D 6299 : 2021	Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 975 : 2019 : REV B	Standard Specification for Diesel Fuel
ASTM D 86 : 2018	Standard Test Method for Distillation of Petroleum Products and Liquid Fuels at Atmospheric Pressure
ASTM D 6299 : 2022 : EDT 1	Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 5085 : 2002 : R2013	Standard Test Method for Determination of Chloride, Nitrate, and Sulfate in Atmospheric Wet Deposition by Chemically Suppressed Ion Chromatography
ASTM D 7328 : 2023	Standard Test Method for Determination of Existent and Potential Inorganic Sulfate and Total Inorganic Chloride in Fuel Ethanol by Ion Chromatography Using Aqueous Sample Injection
ASTM D 975 : 2021	Standard Specification for Diesel Fuel
ASTM D 975 : 2023 : REV A	Standard Specification for Diesel Fuel
ASTM D 6792 : 2021 : REV B	Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories
ASTM D 6792 : 2023 : REV C	Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories
ASTM D 6299 : 2023 : REV A	Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 86 : 2019	Standard Test Method for Distillation of Petroleum Products and Liquid Fuels at Atmospheric Pressure
ASTM D 7319 : 2022	Standard Test Method for Determination of Existent and Potential Sulfate and Inorganic Chloride in Fuel Ethanol and Butanol by Direct Injection Suppressed Ion Chromatography
ASTM E 1511 : 1993 : R2017	Standard Practice for Testing Conductivity Detectors Used in Liquid and Ion Chromatography
ASTM D 7359 : 2023	Standard Test Method for Total Fluorine, Chlorine and Sulfur in Aromatic Hydrocarbons and Their Mixtures by Oxidative Pyrohydrolytic Combustion followed by Ion Chromatography Detection (Combustion Ion Chromatography-CIC)
ASTM D 86 : 2012	Standard Test Method for Distillation of Petroleum Products at Atmospheric Pressure
ASTM D 5987 : 1996	Standard Test Method for Total Fluorine in Coal and Coke by Pyrohydrolytic Extraction and Ion Selective Electrode or Ion Chromatograph Methods
ASTM D 975 : 2020 : REV C	Standard Specification for Diesel Fuel
ASTM D 5085 : 2021	Standard Test Method for Determination of Chloride, Nitrate, and Sulfate in Atmospheric Wet Deposition by Suppressed Ion Chromatography
ASTM D 6792 : 2023 : REV B	Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories
ASTM D 5827 : 2022	Standard Test Method for Analysis of Engine Coolant for Chloride and Other Anions by Ion Chromatography
ASTM D 6792 : 2020	Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories
ASTM D 6792 : 2021	Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories
ASTM D 6299 : 2023 : EDT 1	Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 86 : 2020 : REV B	Standard Test Method for Distillation of Petroleum Products and Liquid Fuels at Atmospheric Pressure
ASTM D 7319 : 2017	Standard Test Method for Determination of Existent and Potential Sulfate and Inorganic Chloride in Fuel Ethanol and Butanol by Direct Injection Suppressed Ion Chromatography
ASTM D 7318 : 2019	Standard Test Method for Existent Inorganic Sulfate in Ethanol by Potentiometric Titration
ASTM D 86 : 2016 : REV A	Standard Test Method for Distillation of Petroleum Products and Liquid Fuels at Atmospheric Pressure
ASTM D 4177 : 2022	Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
ASTM D 6751 : 2023 : REV A	Standard Specification for Biodiesel Fuel Blendstock (B100) for Middle Distillate Fuels
ASTM D 6792 : 2021 : REV C	Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories
ASTM D 6299 : 2023	Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 6751 : 2020 : REV A	Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels
ASTM D 7359 : 2018	Standard Test Method for Total Fluorine, Chlorine and Sulfur in Aromatic Hydrocarbons and Their Mixtures by Oxidative Pyrohydrolytic Combustion followed by Ion Chromatography Detection (Combustion Ion Chromatography-CIC)
ASTM D 6792 : 2023 : REV A	Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories
ASTM D 8150 : 2022	Standard Test Method for Determination of Organic Chloride Content in Crude Oil by Distillation Followed by Detection Using Combustion Ion Chromatography
ASTM D 86 : 2023 : REV A	Standard Test Method for Distillation of Petroleum Products and Liquid Fuels at Atmospheric Pressure
ASTM D 975 : 2022 : REV A	Standard Specification for Diesel Fuel
ASTM D 6751 : 2023	Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels
ASTM D 6299 : 2022	Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 6792 : 2022	Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories
ASTM D 86 : 2020	Standard Test Method for Distillation of Petroleum Products and Liquid Fuels at Atmospheric Pressure
ASTM D 4057 : 2022	Standard Practice for Manual Sampling of Petroleum and Petroleum Products
ASTM D 975 : 2023	Standard Specification for Diesel Fuel
ASTM D 7328 : 2017	Standard Test Method for Determination of Existent and Potential Inorganic Sulfate and Total Inorganic Chloride in Fuel Ethanol by Ion Chromatography Using Aqueous Sample Injection
ASTM D 4177 : 2020	Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
ASTM D 5827 : 2009 : R2015	Standard Test Method for Analysis of Engine Coolant for Chloride and Other Anions by Ion Chromatography
ASTM D 86 : 2015	Standard Test Method for Distillation of Petroleum Products and Liquid Fuels at Atmospheric Pressure
ASTM D 8150 : 2017	Standard Test Method for Determination of Organic Chloride Content in Crude Oil by Distillation Followed by Detection Using Combustion Ion Chromatography
ASTM D 6792 : 2023	Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories
ASTM D 6299 : 2020 : REV A	Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 4177 : 2022 : EDT 1	Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
ASTM D 6792 : 2022 : REV A	Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories
ASTM D 86 : 2017	Standard Test Method for Distillation of Petroleum Products and Liquid Fuels at Atmospheric Pressure