We noticed you’re not on the correct regional site. Switch to our AMERICAS site for the best experience.
  • ASTM D 974 : 2014 : EDT 2

    Superseded A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.
    Add to Watchlist
    This Standard has been added successfully to your Watchlist.
    Please visit My Watchlist to see all standards that you are watching.
    Please log in or to add this standard to your Watchlist.
    We could not add this standard to your Watchlist.
    Please retry or contact support for assistance.
    You need to be logged in to add this standard to your Watchlist.
    Please log in now or create an account to add.
    You already added this Product in the Watchlist.

    Standard Test Method for Acid and Base Number by Color-Indicator Titration

    Available format(s):  Hardcopy, PDF

    Superseded date:  10-05-2023

    Language(s):  English

    Published date:  26-02-2016

    Publisher:  American Society for Testing and Materials

    Add to Watchlist

    Add To Cart

    Scope - (Show below) - (Hide below)

    1.1This test method covers the determination of acidic or basic constituents (Note 1) in petroleum products2 and lubricants soluble or nearly soluble in mixtures of toluene and isopropyl alcohol. It is applicable for the determination of acids or bases whose dissociation constants in water are larger than 10−9; extremely weak acids or bases whose dissociation constants are smaller than 10−9 do not interfere. Salts react if their hydrolysis constants are larger than 10−9.

    Note 1:In new and used oils, the constituents considered to have acidic characteristics include organic and inorganic acids, esters, phenolic compounds, lactones, resins, salts of heavy metals, and addition agents such as inhibitors and detergents. Similarly, constituents considered to have basic properties include organic and inorganic bases, amino compounds, salts of weak acids (soaps), basic salts of polyacidic bases, salts of heavy metals, and addition agents such as inhibitors and detergents.

    Note 2:This test method is not suitable for measuring the basic constituents of many basic additive-type lubricating oils. Test Method D4739 can be used for this purpose.

    1.2This test method can be used to indicate relative changes that occur in an oil during use under oxidizing conditions. Although the titration is made under definite equilibrium conditions, the method does not measure an absolute acidic or basic property that can be used to predict performance of an oil under service conditions. No general relationship between bearing corrosion and acid or base numbers is known.

    Note 3:Oils, such as many cutting oils, rustproofing oils, and similar compounded oils, or excessively dark-colored oils, that cannot be analyzed for acid number by this test method due to obscurity of the color-indicator end point, can be analyzed by Test Method D664. The acid numbers obtained by this color-indicator test method need not be numerically the same as those obtained by Test Method D664, the base numbers obtained by this color indicator test method need not be numerically the same as those obtained by Test Method D4739, but they are generally of the same order of magnitude.

    1.3The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

    1.4This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

    General Product Information - (Show below) - (Hide below)

    Committee D 02
    Document Type Test Method
    Publisher American Society for Testing and Materials
    Status Superseded
    Superseded By
    Supersedes

    Standards Referenced By This Book - (Show below) - (Hide below)

    ASTM D 4304 : 2022 Standard Specification for Mineral and Synthetic Lubricating Oil Used in Steam or Gas Turbines
    ASTM D 7414 : 2022 Standard Test Method for Condition Monitoring of Oxidation in In-Service Petroleum and Hydrocarbon Based Lubricants by Trend Analysis Using Fourier Transform Infrared (FT-IR) Spectrometry
    ASTM D 6224 : 2022 Standard Practice for In-Service Monitoring of Lubricating Oil for Auxiliary Power Plant Equipment
    ASTM D 6074 : 2015 : R2022 Standard Guide for Characterizing Hydrocarbon Lubricant Base Oils
    ASTM D 4378 : 2022 Standard Practice for In-Service Monitoring of Mineral Turbine Oils for Steam, Gas, and Combined Cycle Turbines
    ASTM D 3394 : 2016 : R2022 Standard Test Methods for Sampling and Testing Electrical Insulating Board
    ASTM D 7415 : 2022 Standard Test Method for Condition Monitoring of Sulfate By-Products in In-Service Petroleum and Hydrocarbon Based Lubricants by Trend Analysis Using Fourier Transform Infrared (FT-IR) Spectrometry
    ASTM D 6823 : 2008 : R2021 Standard Specification for Commercial Boiler Fuels With Used Lubricating Oils
    ASTM D 6710 : 2021 Standard Guide for Evaluation of Hydrocarbon-Based Quench Oil
    ASTM D 5222 : 2023 Standard Specification for Less Flammable High Molecular Weight Hydrocarbon Mineral Electrical Insulating Liquids
    ASTM D 8240 : 2022 : EDT 1 Standard Specification for Less-Flammable Synthetic Ester Liquids Used in Electrical Apparatus
    ASTM D 8045 : 2017 : R2023 Standard Test Method for Acid Number of Crude Oils and Petroleum Products by Catalytic Thermometric Titration
    ASTM D 8180 : 2023 Standard Specification for Rerefined Mineral Insulating Liquid Used in Electrical Apparatus
    ASTM D 3339 : 2021 Standard Test Method for Acid Number of Petroleum Products by Semi-Micro Color Indicator Titration
    ASTM D 4293 : 2022 Standard Specification for Phosphate Ester-Based Fluids for Turbine Lubrication and Steam Turbine Electro-Hydraulic Control (EHC) Applications
    ASTM D 117 : 2022 Standard Guide for Sampling, Test Methods, and Specifications for Electrical Insulating Liquids
    ASTM D 2440 : 2013 : R2021 Standard Test Method for Oxidation Stability of Mineral Insulating Oil
    ASTM D 7720 : 2021 Standard Guide for Statistically Evaluating Measurand Alarm Limits when Using Oil Analysis to Monitor Equipment and Oil for Fitness and Contamination
    ASTM D 2226 : 1993 : R2022 Standard Classification for Various Types of Petroleum Oils for Rubber Compounding Use
    ASTM D 4871 : 2011 : R2022 Standard Guide for Universal Oxidation/Thermal Stability Test Apparatus
    ASTM D 4174 : 2017 Standard Practice for Cleaning, Flushing, and Purification of Petroleum Fluid Hydraulic Systems
    ASTM D 6514 : 2003 : R2019 : EDT 1 Standard Test Method for High Temperature Universal Oxidation Test for Turbine Oils
    ASTM D 8045 : 2017 : EDT 1 Standard Test Method for Acid Number of Crude Oils and Petroleum Products by Catalytic Thermometric Titration
    ASTM D 8032 : 2020 Standard Test Method for Acid Number of Terephthalic Acid by Color-Indicator Titration
    ASTM D 5846 : 2007 : R2017 Standard Test Method for Universal Oxidation Test for Hydraulic and Turbine Oils Using the Universal Oxidation Test Apparatus
    ASTM D 8181 : 2019 Standard Specification for Microemulsion Blendstock for Preparing Microemulsion Test Fuel Oils
    ASTM D 6751 : 2020 : REV A Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels
    ASTM D 7666 : 2012 : R2019 Standard Specification for Triglyceride Burner Fuel
    ASTM D 5282 : 2005 : R2020 Standard Test Methods for Compatibility of Construction Material with Silicone Fluid Used for Electrical Insulation
    ASTM D 5222 : 2016 Standard Specification for High Fire-Point Mineral Electrical Insulating Oils
    ASTM D 4304 : 2017 Standard Specification for Mineral and Synthetic Lubricating Oil Used in Steam or Gas Turbines
    ASTM D 664 : 2018 : EDT 2 Standard Test Method for Acid Number of Petroleum Products by Potentiometric Titration
    ASTM D 3455 : 2011 : R2019 Standard Test Methods for Compatibility of Construction Material with Electrical Insulating Oil of Petroleum Origin
    ASTM D 3339 : 2012 : R2017 Standard Test Method for Acid Number of Petroleum Products by Semi-Micro Color Indicator Titration
    ASTM D 2440 : 2013 Standard Test Method for Oxidation Stability of Mineral Insulating Oil
    ASTM D 6224 : 2016 Standard Practice for In-Service Monitoring of Lubricating Oil for Auxiliary Power Plant Equipment
    ASTM D 117 : 2018 Standard Guide for Sampling, Test Methods, and Specifications for Electrical Insulating Liquids
    ASTM D 1934 : 2020 Standard Test Method for Oxidative Aging of Electrical Insulating Liquids by Open-Beaker Method
    ASTM D 7044 : 2015 Standard Specification for Biodegradable Fire Resistant Hydraulic Fluids
    ASTM D 6469 : 2020 Standard Guide for Microbial Contamination in Fuels and Fuel Systems
    ASTM D 3487 : 2016 : EDT 1 Standard Specification for Mineral Insulating Oil Used in Electrical Apparatus
    ASTM D 6439 : 2011 : R2017 Standard Guide for Cleaning, Flushing, and Purification of Steam, Gas, and Hydroelectric Turbine Lubrication Systems
    ASTM D 2619 : 2021 Standard Test Method for Hydrolytic Stability of Hydraulic Fluids (Beverage Bottle Method)
    ASTM D 4871 : 2011 : R2016 Standard Guide for Universal Oxidation/Thermal Stability Test Apparatus
    ASTM D 5770 : 2011 : R2017 Standard Test Method for Semiquantitative Micro Determination of Acid Number of Lubricating Oils During Oxidation Testing
    ASTM D 7752 : 2018 Standard Practice for Evaluating Compatibility of Mixtures of Hydraulic Fluids
    ASTM D 7414 : 2018 Standard Test Method for Condition Monitoring of Oxidation in In-Service Petroleum and Hydrocarbon Based Lubricants by Trend Analysis Using Fourier Transform Infrared (FT-IR) Spectrometry
    ASTM D 3394 : 2016 Standard Test Methods for Sampling and Testing Electrical Insulating Board
    ASTM D 6823 : 2008 : R2013 Standard Specification for Commercial Boiler Fuels With Used Lubricating Oils
    ASTM D 7720 : 2011 : R2017 Standard Guide for Statistically Evaluating Measurand Alarm Limits when Using Oil Analysis to Monitor Equipment and Oil for Fitness and Contamination
    ASTM D 6871 : 2017 Standard Specification for Natural (Vegetable Oil) Ester Fluids Used in Electrical Apparatus
    ASTM D 6074 : 2015 Standard Guide for Characterizing Hydrocarbon Lubricant Base Oils
    ASTM D 7415 : 2018 Standard Test Method for Condition Monitoring of Sulfate By-Products in In-Service Petroleum and Hydrocarbon Based Lubricants by Trend Analysis Using Fourier Transform Infrared (FT-IR) Spectrometry
    ASTM D 8029 : 2018 Standard Specification for Biodegradable, Low Aquatic Toxicity Hydraulic Fluids
    ASTM D 2225 : 2020 Standard Test Methods for Silicone Liquids Used for Electrical Insulation
    ASTM F 2161 : 2021 Standard Guide for Instrument and Precision Bearing Lubricants—Part 1 Oils
    ASTM D 1534 : 1995 : R2017 Standard Test Method for Approximate Acidity in Electrical Insulating Liquids by Color-Indicator Titration
    ASTM D 7155 : 2020 Standard Practice for Evaluating Compatibility of Mixtures of Turbine Lubricating Oils
    ASTM D 2226 : 1993 : R2018 Standard Classification for Various Types of Petroleum Oils for Rubber Compounding Use
    ASTM D 8324 : 2021 Standard Guide for Selection of Environmentally Acceptable Lubricants for the U.S. Environmental Protection Agency (EPA) Vessel General Permit
    ASTM D 4652 : 2020 Standard Specification for Silicone Liquid Used for Electrical Insulation
    ASTM D 6710 : 2017 Standard Guide for Evaluation of Hydrocarbon-Based Quench Oil
    ASTM D 4293 : 2015 : EDT 1 Standard Specification for Phosphate Ester Based Fluids for Turbine Lubrication and Steam Turbine Electro-Hydraulic Control (EHC) Applications
    ASTM D 4378 : 2020 Standard Practice for In-Service Monitoring of Mineral Turbine Oils for Steam, Gas, and Combined Cycle Turbines
    ASTM D 6158 : 2018 Standard Specification for Mineral Hydraulic Oils

    Standards Referencing This Book - (Show below) - (Hide below)

    ASTM D 4175 : 2020 Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
    ASTM D 4175 : 2014 Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
    ASTM D 4175 : 2009 : REV A : EDT 1 Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
    ASTM D 4175 : 2008 : REV B : EDT 1 Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
    ASTM D 4175 : 2005 Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
    ASTM D 4175 : 2005 : EDT 2 Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
    ASTM D 4175 : 2015 : REV C Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
    ASTM D 4175 : 2017 : REV A : EDT 1 Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
    ASTM D 4739 : 2005 Standard Test Method for Base Number Determination by Potentiometric Titration
    ASTM D 4175 : 2008 : REV A Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
    ASTM D 4175 : 2020 : REV A Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
    ASTM D 4175 : 2017 : REV B Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
    ASTM D 4175 : 2009 Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
    ASTM D 1193 : 1977 : R1983 : EDT 1 Standard Specification for Reagent Water
    ASTM D 4175 : 2009 : REV A : EDT 4 Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
    ASTM D 4175 : 2009 : REV A : EDT 3 Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
    ASTM D 4175 : 2018 Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
    ASTM D 4175 : 2001 : EDT 1 Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
    ASTM D 4175 : 2001 Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
    ASTM D 4175 : 2005 : EDT 1 Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
    ASTM D 4739 : 2008 Standard Test Method for Base Number Determination by Potentiometric Hydrochloric Acid Titration
    ASTM D 4175 : 2002 Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
    ASTM D 4739 : 2017 Standard Test Method for Base Number Determination by Potentiometric Hydrochloric Acid Titration
    ASTM D 4739 : 2006 Standard Test Method for Base Number Determination by Potentiometric Titration
    ASTM D 4175 : 2015 Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
    ASTM D 1193 : 2006 : R2011 Standard Specification for Reagent Water
    ASTM D 4175 : 2002 : REV A : EDT 2 Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
    ASTM D 4739 : 1996 Standard Test Method for Base Number Determination by Potentiometric Titration
    ASTM D 664 : 1995 Standard Test Method for Acid Number of Petroleum Products by Potentiometric Titration
    ASTM D 4175 : 2009 : REV A : EDT 5 Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
    ASTM D 4175 : 2016 : REV C Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
    ASTM D 4175 : 2015 : REV B Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
    ASTM D 4175 : 2015 : REV A Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
    ASTM D 4739 : 2011 : R2017 Standard Test Method for Base Number Determination by Potentiometric Hydrochloric Acid Titration
    ASTM D 1193 : 1991 Standard Specification for Reagent Water
    ASTM D 4175 : 2009 : REV A Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
    ASTM D 4175 : 2016 : REV B Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
    ASTM D 4175 : 2002 : REV A : EDT 1 Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
    ASTM D 4175 : 2008 Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
    ASTM D 4175 : 2002 : REV A Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
    ASTM D 4175 : 2000 : EDT 1 Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
    ASTM D 4175 : 2016 : REV A Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
    ASTM D 4739 : 2008 : EDT 1 Standard Test Method for Base Number Determination by Potentiometric Hydrochloric Acid Titration
    ASTM D 4175 : 2019 : EDT 1 Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
    ASTM D 117 : 1996 Standard Guide for Sampling, Test Methods, Specifications, and Guide for Electrical Insulating Oils of Petroleum Origin
    ASTM D 4175 : 2017 : REV A Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
    ASTM D 4175 : 2009 : REV A : EDT 2 Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
    ASTM D 1193 : 1970 Standard Specification For Reagent Water
    ASTM D 1193 : 2006 Standard Specification for Reagent Water
    ASTM D 4175 : 2018 : EDT 1 Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
    ASTM D 4175 : 2016 Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
    ASTM D 1193 : 1999 Standard Specification for Reagent Water
    ASTM D 4739 : 2011 Standard Test Method for Base Number Determination by Potentiometric Hydrochloric Acid Titration
    ASTM D 4739 : 2002 Standard Test Method for Base Number Determination by Potentiometric Titration
    ASTM D 4739 : 2006 : REV A Standard Test Method for Base Number Determination by Potentiometric Titration
    ASTM D 4175 : 2017 Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
    ASTM D 4175 : 2019 Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
    ASTM D 1193 : 2006 : R2018 Standard Specification for Reagent Water
    ASTM D 4175 : 2015 : REV B : EDT 1 Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
    ASTM D 4175 : 2008 : REV B Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
    • Access your standards online with a subscription

      Features

      • Simple online access to standards, technical information and regulations
      • Critical updates of standards and customisable alerts and notifications
      • Multi - user online standards collection: secure, flexibile and cost effective